A. Lesage

发表

Preferential Siting of Aluminum Heteroatoms in the Zeolite Catalyst Al-SSZ-70.

Zachariah J. Berkson, S. Zones, M. Hsieh, 2019, Angewandte Chemie.

Preferential Siting of Aluminum Heteroatoms in the Zeolite Catalyst Al‐SSZ‐70

Zachariah J. Berkson, S. Zones, M. Hsieh, 2019, Angewandte Chemie.

Methane reacts with heteropolyacids chemisorbed on silica to produce acetic acid under soft conditions.

Jizhen Zhang, Miao Sun, E. Abou‐hamad, 2013, Journal of the American Chemical Society.

Atomic-level organization of vicinal acid–base pairs through the chemisorption of aniline and derivatives onto mesoporous SBA15

R. Sougrat, E. Abou‐hamad, D. Gajan, 2016, Chemical science.

Combination of DQ and ZQ coherences for sensitive through-bond NMR correlation experiments in biosolids under ultra-fast MAS.

I. Bertini, Michael J. Knight, I. Felli, 2012, Chemphyschem : a European journal of chemical physics and physical chemistry.

High-resolution and sensitivity through-bond correlations in ultra-fast magic angle spinning (MAS) solid-state NMR

I. Bertini, I. Felli, R. Pierattelli, 2011 .

Transverse-dephasing optimized homonuclear j-decoupling in solid-state NMR spectroscopy of uniformly 13C-labeled proteins.

I. Bertini, I. Felli, R. Pierattelli, 2009, Journal of the American Chemical Society.

Water-protein interactions in microcrystalline crh measured by 1H-13C solid-state NMR spectroscopy.

A. Lesage, A. Böckmann, Anja Böckmann, 2003, Journal of the American Chemical Society.

Gold nanoparticles supported on passivated silica: access to an efficient aerobic epoxidation catalyst and the intrinsic oxidation activity of gold.

C. Copéret, D. Gajan, A. Lesage, 2009, Journal of the American Chemical Society.

Probing surface site heterogeneity through 1D and INADEQUATE31P solid state NMR spectroscopy of silica supported PMe3-Au(I) adducts

Daniel S. Levine, C. Copéret, D. Gajan, 2011 .

Well-defined silica-supported Mo-alkylidene catalyst precursors containing one or substituent: methods of preparation and structure-reactivity relationship in alkene metathesis.

R. Schrock, F. Blanc, C. Copéret, 2009, Chemistry.

Trimeric assembly and three-dimensional structure model of the FACIT collagen COL1-NC1 junction from CD and NMR analysis.

C. Geourjon, F. Penin, D. Marion, 1996, Biochemistry.

Hyperpolarization of Frozen Hydrocarbon Gases by Dynamic Nuclear Polarization at 1.2 K.

G. Bodenhausen, C. Copéret, D. Gajan, 2016, The journal of physical chemistry letters.

Synthesis of deuterium-labeled cryptophane-A and investigation of Xe@cryptophane complexation dynamics by 1D-EXSY-NMR experiments.

A. Lesage, T. Devic, L. Emsley, 2001, Chemistry.

Two-Photon Absorbing AIEgens: Influence of Stereoconfiguration on Their Crystallinity and Spectroscopic Properties and Applications in Bioimaging.

J. Blahůt, A. Lesage, T. Le Bahers, 2020, ACS applied materials & interfaces.

A comparison of proton‐detected 13C local field experiments with deuterium NMR at natural abundance for studying liquid crystals

A. Lesage, G. De Luca, J. Emsley, 2008 .

Atomic-Scale Structure and Its Impact on Chemical Properties of Aluminum Oxide Layers Prepared by Atomic Layer Deposition on Silica

C. Müller, A. Fedorov, C. Copéret, 2021, Chemistry of Materials.

Insights into the structure and dynamics of measles virus nucleocapsids by 1H-detected solid-state NMR.

M. Blackledge, R. Ruigrok, M. R. Jensen, 2014, Biophysical journal.

Proton to carbon-13 INEPT in solid-state NMR spectroscopy.

A. Lesage, A. Böckmann, L. Emsley, 2005, Journal of the American Chemical Society.

Rational design of dinitroxide biradicals for efficient cross-effect dynamic nuclear polarization

Karthikeyan Ganesan, G. Jeschke, C. Copéret, 2015, Chemical science.

Tailored Polarizing Hybrid Solids with Nitroxide Radicals Localized in Mesostructured Silica Walls

G. Bodenhausen, G. Jeschke, C. Copéret, 2017 .

Dynamic nuclear polarization surface enhanced NMR spectroscopy.

C. Copéret, A. Lesage, Aaron J. Rossini, 2013, Accounts of chemical research.

Powder crystallography of pharmaceutical materials by combined crystal structure prediction and solid-state 1H NMR spectroscopy.

E. Salager, G. Day, A. Lesage, 2013, Physical chemistry chemical physics : PCCP.

Fast characterization of functionalized silica materials by silicon-29 surface-enhanced NMR spectroscopy using dynamic nuclear polarization.

V. Vitzthum, G. Bodenhausen, M. Caporini, 2011, Journal of the American Chemical Society.

Molecular Level Characterization of the Structure and Interactions in Peptide-Functionalized Metal-Organic Frameworks.

L. N. Ho, D. Farrusseng, C. Gervais, 2016, Chemistry.

Spectroscopic Signature and Structure of the Active Sites in Ziegler-Natta Polymerization Catalysts Revealed by Electron Paramagnetic Resonance.

J. Blahůt, S. Norsic, V. Monteil, 2020, Journal of the American Chemical Society.

In situ preparation of a multifunctional chiral hybrid organic–inorganic catalyst for asymmetric multicomponent reactions

A. Corma, C. Copéret, A. Lesage, 2013 .

Molecular and Electronic Structure of Isolated Platinum Sites Enabled by the Expedient Measurement of 195Pt Chemical Shift Anisotropy.

C. Copéret, A. Lesage, Aaron J. Rossini, 2022, Journal of the American Chemical Society.

Dynamics of silica-supported catalysts determined by combining solid-state NMR spectroscopy and DFT calculations.

R. Schrock, F. Blanc, C. Copéret, 2008, Journal of the American Chemical Society.

Efficient Dynamic Nuclear Polarization up to 230 K with Hybrid BDPA-Nitroxide Radicals at a High Magnetic Field.

G. Jeschke, D. Gajan, A. Lund, 2021, The journal of physical chemistry. B.

Direct observation of reaction intermediates for a well defined heterogeneous alkene metathesis catalyst

R. Schrock, F. Blanc, C. Copéret, 2008, Proceedings of the National Academy of Sciences.

Well-Defined Surface Tungstenocarbyne Complexes through the Reaction of [W(⋮CtBu)(CH2tBu)3] with Silica

C. Copéret, A. Lesage, D. Alcor, 2005 .

Molecular Understanding of the Formation of Surface Zirconium Hydrides upon Thermal Treatment under Hydrogen of [(=SiO)Zr(CH 2 tBU) 3 ] by Using Advanced Solid-State NMR Techniques

C. Copéret, A. Lesage, F. Rataboul, 2004 .

Detailed structural investigation of the grafting of [Ta(=CHtBu)(CH2tBu)3] and [Cp*TaMe4] on silica partially dehydroxylated at 700 degrees C and the activity of the grafted complexes toward alkane metathesis.

Glenn J. Sunley, W. Lukens, C. Copéret, 2004, Journal of the American Chemical Society.

Expanding the horizons for structural analysis of fully protonated protein assemblies by NMR spectroscopy at MAS frequencies above 100 kHz.

A. Gronenborn, D. Lalli, A. Lesage, 2017, Solid State Nuclear Magnetic Resonance.

Superstructure of a substituted zeolitic imidazolate metal-organic framework determined by combining proton solid-state NMR spectroscopy and DFT calculations.

D. Farrusseng, A. Lesage, J. Canivet, 2015, Angewandte Chemie.

Off-the-Shelf Gd(NO3)3 as an Efficient High-Spin Metal Ion Polarizing Agent for Magic Angle Spinning Dynamic Nuclear Polarization

Adam Brookfield, Subhradip Paul, D. Gajan, 2022, The journal of physical chemistry. B.

Design Principles for the Development of Gd(III) Polarizing Agents for Magic Angle Spinning Dynamic Nuclear Polarization

G. Jeschke, A. Lesage, A. Venkatesh, 2022, The journal of physical chemistry. C, Nanomaterials and interfaces.

Polarization transfer over the water-protein interface in solids.

B. Meier, A. Lesage, A. Loquet, 2008, Angewandte Chemie.

Dynamic nuclear polarization enhanced solid-state NMR spectroscopy of functionalized metal-organic frameworks.

D. Farrusseng, C. Copéret, A. Lesage, 2012, Angewandte Chemie.

19 F Magic Angle Spinning Dynamic Nuclear Polarization Enhanced NMR Spectroscopy.

D. Gajan, A. Lesage, D. Kubicki, 2019, Angewandte Chemie.

19 F Magic Angle Spinning Dynamic Nuclear Polarization Enhanced NMR Spectroscopy

D. Gajan, A. Lesage, D. Kubicki, 2019, Angewandte Chemie.

Open and Closed Radicals: Local Geometry around Unpaired Electrons Governs Magic-Angle Spinning Dynamic Nuclear Polarization Performance

G. Jeschke, A. Lesage, D. Kubicki, 2020, Journal of the American Chemical Society.

Hydrophobic radicals embedded in neutral surfactants for dynamic nuclear polarization of aqueous environments at 9.4 Tesla.

A. Lesage, Aaron J. Rossini, L. Emsley, 2014, Chemical communications.

Endogenous 17O Dynamic Nuclear Polarization of Gd-Doped CeO2 from 100 to 370 K

C. Grey, J. MacManus‐Driscoll, A. Lesage, 2021, The Journal of Physical Chemistry C.

BDPA-Nitroxide Biradicals Tailored for Efficient Dynamic Nuclear Polarization Enhanced Solid-State NMR at Magnetic Fields up to 21.1 T.

G. Jeschke, C. Copéret, D. Gajan, 2018, Journal of the American Chemical Society.

Measuring Nano- to Microstructures from Relayed Dynamic Nuclear Polarization NMR

Mingxue Tang, A. Lesage, Aaron J. Rossini, 2017 .

Multiple Surface Site Three-Dimensional Structure Determination of a Supported Molecular Catalyst.

C. Copéret, D. Gajan, A. Lesage, 2022, Journal of the American Chemical Society.

Dynamic nuclear polarization enhanced NMR spectroscopy for pharmaceutical formulations.

C. Copéret, A. Lesage, Aaron J. Rossini, 2014, Journal of the American Chemical Society.

Surface versus molecular siloxy ligands in well-defined olefin metathesis catalysts: [{(RO)3SiO}Mo(=NAr)(=CHtBu)(CH2tBu)].

R. Schrock, F. Blanc, C. Copéret, 2006, Angewandte Chemie.

Perhydrocarbyl ReVII complexes: comparison of molecular and surface complexes.

W. Lukens, C. Copéret, A. Lesage, 2003, Journal of the American Chemical Society.

Deuterium-carbon NMR correlation spectroscopy in oriented materials

A. Lesage, C. Auger, S. Caldarelli, 1997 .

A highly ordered mesostructured material containing regularly distributed phenols: preparation and characterization at a molecular level through ultra-fast magic angle spinning proton NMR spectroscopy.

C. Copéret, D. Gajan, A. Lesage, 2011, Physical chemistry chemical physics : PCCP.

Molecular-level characterization of the structure and the surface chemistry of periodic mesoporous organosilicates using DNP-surface enhanced NMR spectroscopy.

C. Copéret, D. Gajan, A. Lesage, 2013, Physical chemistry chemical physics : PCCP.

Iridium(I)/N-Heterocyclic Carbene Hybrid Materials: Surface Stabilization of Low-Valent Iridium Species for High Catalytic Hydrogenation Performance.

I. Romanenko, R. Sayah, D. Gajan, 2015, Angewandte Chemie.

A well-defined Pd hybrid material for the Z-selective semihydrogenation of alkynes characterized at the molecular level by DNP SENS.

W. T. Franks, H. Oschkinat, C. Copéret, 2013, Chemistry.

Improved dynamic nuclear polarization surface-enhanced NMR spectroscopy through controlled incorporation of deuterated functional groups.

W. T. Franks, H. Oschkinat, C. Copéret, 2013, Angewandte Chemie.

A slowly relaxing rigid biradical for efficient dynamic nuclear polarization surface-enhanced NMR spectroscopy: expeditious characterization of functional group manipulation in hybrid materials.

C. Copéret, D. Gajan, A. Lesage, 2012, Journal of the American Chemical Society.

Surface enhanced NMR spectroscopy by dynamic nuclear polarization.

V. Vitzthum, G. Bodenhausen, M. Caporini, 2010, Journal of the American Chemical Society.

Atomistic Description of Reaction Intermediates for Supported Metathesis Catalysts Enabled by DNP SENS.

C. Copéret, V. Mougel, D. Gajan, 2016, Angewandte Chemie.

Well-defined surface imido amido tantalum(v) species from ammonia and silica-supported tantalum hydrides.

E. A. Quadrelli, A. Lesage, L. Emsley, 2007, Journal of the American Chemical Society.

Phenylazide Hybrid-Silica – Polarization Platform for Dynamic Nuclear Polarization at Cryogenic Temperatures

G. Bodenhausen, C. Copéret, D. Gajan, 2017 .

Homonuclear dipolar decoupling with very large scaling factors for high-resolution ultrafast magic angle spinning 1H solid-state NMR spectroscopy

E. Salager, B. Elena-Herrmann, A. Lesage, 2010 .

Motional heterogeneity in single-site silica-supported species revealed by deuteron NMR.

C. Copéret, A. Lesage, R. Vold, 2009, Physical chemistry chemical physics : PCCP.

Oxygen-17 dynamic nuclear polarisation enhanced solid-state NMR spectroscopy at 18.8 T.

F. Blanc, D. Gajan, A. Lesage, 2017, Chemical communications.

Large molecular weight nitroxide biradicals providing efficient dynamic nuclear polarization at temperatures up to 200 K.

G. Jeschke, C. Copéret, A. Lesage, 2013, Journal of the American Chemical Society.

Solid-state NMR of a paramagnetic DIAD-FeII catalyst: sensitivity, resolution enhancement, and structure-based assignments.

E. Oldfield, C. Copéret, A. Lesage, 2006, Journal of the American Chemical Society.

Speciation and Structures in Pt Surface Sites Stabilized by N-Heterocyclic Carbene Ligands Revealed by Dynamic Nuclear Polarization Enhanced Indirectly Detected 195Pt NMR Spectroscopic Signatures and Fingerprint Analysis.

C. Copéret, D. Gajan, A. Lesage, 2022, Journal of the American Chemical Society.

NMR signatures of the active sites in Sn-β zeolite.

I. Hermans, A. Comas‐Vives, C. Copéret, 2014, Angewandte Chemie.

Frozen Acrylamide Gels as Dynamic Nuclear Polarization Matrices.

D. Gajan, A. Lesage, L. Emsley, 2017, Angewandte Chemie.

Structural Characterization of the EtOH-TiCl4-MgCl2 Ziegler-Natta Precatalyst

P. Sautet, S. Norsic, V. Monteil, 2016 .

Assigning powders to crystal structures by high-resolution (1)H-(1)H double quantum and (1)H-(13)C J-INEPT solid-state NMR spectroscopy and first principles computation. A case study of penicillin G.

C. Pickard, A. Lesage, L. Emsley, 2006, Physical chemistry chemical physics : PCCP.

Predicting the DNP-SENS efficiency in reactive heterogeneous catalysts from hydrophilicity

Manoja K. Samantaray, L. Cavallo, Zhen Cao, 2018, Chemical science.

Specific Localization of Aluminum Sites Favors Ethene-to-Propene Conversion on (Al)MCM-41-Supported Ni(II) Single Sites

A. Fedorov, C. Copéret, D. Gajan, 2019, ACS Catalysis.

Evidence for metal-surface interactions and their role in stabilizing well-defined immobilized Ru-NHC alkene metathesis catalysts.

Lyndon Emsley, Anne Lesage, David Gajan, 2013, Journal of the American Chemical Society.

Local Structures and Heterogeneity of Silica-Supported M(III) Sites Evidenced by EPR, IR, NMR, and Luminescence Spectroscopies.

A. Comas‐Vives, M. Walter, G. Jeschke, 2017, Journal of the American Chemical Society.

Silica‐Grafted Tris(neopentyl)aluminum: A Monomeric Aluminum Solid Co‐catalyst for Efficient Nickel‐Catalyzed Ethene Dimerization

C. Copéret, A. Lesage, C. Gordon, 2020, Angewandte Chemie.

Silica-grafted Tris(neopentyl)aluminum: A Monomeric Aluminum Solid Co-Catalyst for Efficient Nickel-Catalyzed Ethene Dimerization.

C. Copéret, A. Lesage, C. Gordon, 2020, Angewandte Chemie.

Metal-Metal Synergy in Well-Defined Surface Tantalum-Iridium Heterobimetallic Catalysts for H/D Exchange Reactions.

D. Gajan, A. Lesage, L. Veyre, 2019, Journal of the American Chemical Society.

Nature and structure of aluminum surface sites grafted on silica from a combination of high-field aluminum-27 solid-state NMR spectroscopy and first-principles calculations.

P. Sautet, R. Kerber, C. Copéret, 2012, Journal of the American Chemical Society.

Stepwise construction of silica-supported tantalum/iridium heteropolymetallic catalysts using surface organometallic chemistry

D. Gajan, A. Lesage, E. Fonda, 2020, Journal of Catalysis.

Synthesis and reactivity of molybdenum imido alkylidene bis-pyrazolide complexes.

R. Schrock, C. Copéret, D. Gajan, 2010, Dalton transactions.

The chirality of a twist-bend nematic phase identified by NMR spectroscopy.

G. R. Luckhurst, B. A. Timimi, H. Zimmermann, 2012, The journal of physical chemistry. B.

The Nature of Secondary Interactions at Electrophilic Metal Sites of Molecular and Silica-Supported Organolutetium Complexes from Solid-State NMR Spectroscopy.

W. Lukens, C. Copéret, D. Gajan, 2016, Journal of the American Chemical Society.

Tetrahydrofuran in TiCl4/THF/MgCl2: a Non-Innocent Ligand for Supported Ziegler–Natta Polymerization Catalysts

P. Sautet, É. Grau, S. Norsic, 2013 .

Title Structural Characterization of the EtOH-TiCl 4-MgCl 2 Ziegler-Natta Precatalyst Permalink

P. Sautet, S. Norsic, V. Monteil, 2016 .

Supported Ru olefin metathesis catalysts via a thiolate tether.

Vidar R. Jensen, V. R. Jensen, R. Sayah, 2019, Dalton transactions.

Three-Dimensional Structure Determination of Surface Sites

C. Copéret, D. Gajan, A. Lesage, 2016, Journal of the American Chemical Society.

A well-defined silica-supported tungsten oxo alkylidene is a highly active alkene metathesis catalyst.

R. Schrock, C. Copéret, V. Mougel, 2013, Journal of the American Chemical Society.

Homonuclear dipolar decoupling in solid-state NMR using continuous phase modulation

Dimitris Sakellariou, Lyndon Emsley, Anne Lesage, 2000 .

Through-Bond Carbon−Carbon Connectivities in Disordered Solids by NMR

Lyndon Emsley, Anne Lesage, A. Lesage, 1999 .

Determination of Through-Bond Carbon−Carbon Connectivities in Solid-State NMR Using the INADEQUATE Experiment

A. Lesage, C. Auger, S. Caldarelli, 1997 .

Spin Hyperpolarization in Modern Magnetic Resonance

D. Budker, S. Cavagnero, J. Reimer, 2023, Chemical reviews.

129Xe NMR Spectroscopy of Deuterium-Labeled Cryptophane-A Xenon Complexes: Investigation of Host−Guest Complexation Dynamics

A. Lesage, A. Collet, T. Brotin, 2000 .

Observation of a H-agostic bond in a highly active rhenium-alkylidene olefin metathesis heterogeneous catalyst by two-dimensional solid-state NMR spectroscopy.

C. Copéret, A. Lesage, L. Emsley, 2002, Angewandte Chemie.

The Structure of Molecular and Surface Platinum Sites Determined by DNP-SENS and Fast MAS 195Pt Solid-State NMR Spectroscopy.

C. Copéret, D. Gajan, A. Lund, 2020, Journal of the American Chemical Society.

Open and Closed Radicals: Local Geometry Around Unpaired Electrons Governs MAS DNP Performance.

G. Jeschke, A. Lesage, D. Kubicki, 2020, Journal of the American Chemical Society.

Atomic-Scale Description of Interfaces between Antigen and Aluminum-Based Adjuvants used in Vaccines by DNP Enhanced NMR Spectroscopy.

F. Ronzon, D. Gajan, A. Lesage, 2020, Chemistry.

Dynamic Nuclear Polarization Magic-Angle Spinning Nuclear Magnetic Resonance Combined with Molecular Dynamics Simulations Permits Detection of Order and Disorder in Viral Assemblies.

A. Gronenborn, H. Oschkinat, M. Caporini, 2019, The journal of physical chemistry. B.

DNP NMR of biomolecular assemblies.

H. Oschkinat, A. Lesage, T. Polenova, 2019, Journal of structural biology.

One- and Two-Dimensional High-Resolution NMR from Flat Surfaces

C. Copéret, A. Lesage, Aaron J. Rossini, 2019, ACS central science.

Dynamic Nuclear Polarization-Enhanced Biomolecular NMR Spectroscopy at High Magnetic Field with Fast Magic-Angle Spinning.

I. Akopjana, K. Tārs, A. Pica, 2018, Angewandte Chemie.

Dynamic Nuclear Polarization Efficiency Increased by Very Fast Magic Angle Spinning

C. Copéret, D. Gajan, A. Lesage, 2017, Journal of the American Chemical Society.

Solid-State Dynamic Nuclear Polarization at 9.4 and 18.8 T from 100 K to Room Temperature

D. Gajan, A. Lesage, Aaron J. Rossini, 2015, Journal of the American Chemical Society.

Hybrid polarizing solids for pure hyperpolarized liquids through dissolution dynamic nuclear polarization

Geoffrey Bodenhausen, Lyndon Emsley, Anne Lesage, 2014, Proceedings of the National Academy of Sciences.

Predictive morphology, stoichiometry and structure of surface species in supported Ru nanoparticles under H2 and CO atmospheres from combined experimental and DFT studies.

F. Ribeiro, A. Comas‐Vives, C. Copéret, 2016, Physical chemistry chemical physics : PCCP.

The conformation and orientational order of a 1,2-disubstituted ethane nematogenic molecule (I22) in liquid crystalline and isotropic phases studied by NMR spectroscopy.

A. Lesage, G. De Luca, J. Emsley, 2010, Physical chemistry chemical physics : PCCP.

Structure of fully protonated proteins by proton-detected magic-angle spinning NMR

T. Herrmann, I. Akopjana, K. Tārs, 2016, Proceedings of the National Academy of Sciences.

Indirect Coupling and Connectivity

A. Lesage, 2008 .

The refocused INADEQUATE MAS NMR experiment in multiple spin-systems: interpreting observed correlation peaks and optimising lineshapes.

A. Lesage, L. Duma, L. Emsley, 2007, Journal of magnetic resonance.

NMR measurements of scalar-coupling distributions in disordered solids.

A. Lesage, L. Heux, M. Trierweiler, 2007, Physical chemistry chemical physics : PCCP.

Recent advances in solid-state NMR spectroscopy of spin I=1/2 nuclei.

A. Lesage, 2009, Physical chemistry chemical physics : PCCP.

Water–Protein Hydrogen Exchange in the Micro-Crystalline Protein Crh as Observed by Solid State NMR Spectroscopy

F. Penin, A. Galinier, A. Lesage, 2005, Journal of biomolecular NMR.

Spin-state selection in solid-state NMR.

Lyndon Emsley, Anne Lesage, Luminita Duma, 2003, Journal of magnetic resonance.

Dynamic nuclear polarization NMR spectroscopy of microcrystalline solids.

C. Copéret, D. Gajan, A. Lesage, 2012, Journal of the American Chemical Society.

Transverse dephasing optimised NMR spectroscopy in solids: natural-abundance 13C correlation spectra.

A. Lesage, L. Emsley, G. De Paëpe, 2004, Chemphyschem : a European journal of chemical physics and physical chemistry.

High-resolution NMR correlation spectra of disordered solids.

A. Pines, D. Sakellariou, M. Bardet, 2003, Journal of the American Chemical Society.

Structural description of surfaces and interfaces in biominerals by DNP SENS.

T. Azaïs, N. Nassif, D. Gajan, 2019, Solid state nuclear magnetic resonance.

Unraveling the core-shell structure of ligand-capped Sn/SnOx nanoparticles by surface-enhanced nuclear magnetic resonance, Mössbauer, and X-ray absorption spectroscopies.

Marc D. Walter, M. Kovalenko, K. Kravchyk, 2014, ACS nano.

Carbon-proton chemical shift correlation in solid-state NMR by through-bond multiple-quantum spectroscopy

D. Sakellariou, A. Lesage, L. Emsley, 1998 .

Structural Characterization of Phosphate Species Adsorbed on γ-Alumina by Combining DNP Surface Enhanced NMR Spectroscopy and DFT Calculations

A. Lesage, P. Raybaud, C. Michel, 2021, ACS Catalysis.

Dendritic polarizing agents for DNP SENS† †Electronic supplementary information (ESI) available. See DOI: 10.1039/c6sc03139k Click here for additional data file.

M. Buchmeiser, G. Jeschke, C. Copéret, 2016, Chemical science.

Reactive surface organometallic complexes observed using dynamic nuclear polarization surface enhanced NMR spectroscopy

Manoja K. Samantaray, D. Anjum, E. Abou‐hamad, 2016, Chemical science.

Dynamic nuclear polarization at 40 kHz magic angle spinning† †Electronic supplementary information (ESI) available: Experimental details, with supplementary tables and figures. See DOI: 10.1039/c6cp00839a Click here for additional data file.

C. Copéret, D. Gajan, A. Lesage, 2016, Physical chemistry chemical physics : PCCP.

Backbone assignment of fully protonated solid proteins by 1H detection and ultrafast magic-angle-spinning NMR spectroscopy.

Lyndon Emsley, Michele Felletti, Anne Lesage, 2012, Angewandte Chemie.

Probing proton-proton proximities in the solid state: high-resolution two-dimensional 1H-1H double-quantum CRAMPS NMR spectroscopy.

A. Lesage, L. Emsley, B. Eléna, 2004, Journal of the American Chemical Society.

One hundred fold overall sensitivity enhancements for Silicon-29 NMR spectroscopy of surfaces by dynamic nuclear polarization with CPMG acquisition

C. Copéret, D. Gajan, A. Lesage, 2012 .

Dynamic nuclear polarization of quadrupolar nuclei using cross polarization from protons: surface-enhanced aluminium-27 NMR.

Geoffrey Bodenhausen, Lyndon Emsley, Anne Lesage, 2012, Chemical communications.

Correlating Synthetic Methods, Morphology, Atomic-Level Structure, and Catalytic Activity of Sn-β Catalysts

I. Hermans, A. Comas‐Vives, C. Copéret, 2016 .

Direct measure of the tilt angle in de Vries-type liquid crystals through NMR spectroscopy.

A. Lesage, M. Lelli, V. Domenici, 2010, Chemphyschem : a European journal of chemical physics and physical chemistry.

Beyond γ-Al2O3 crystallite surfaces: The hidden features of edges revealed by solid-state 1H NMR and DFT calculations

D. Gajan, A. Lesage, C. Chizallet, 2019, Journal of Catalysis.

Uncovering selective and active Ga surface sites in gallia–alumina mixed-oxide propane dehydrogenation catalysts by dynamic nuclear polarization surface enhanced NMR spectroscopy

C. Müller, A. Fedorov, C. Copéret, 2021, Chemical science.

DNP in Materials Science: Touching the Surface

A. Lesage, L. Emsley, Pierrick Berruyer, 2018 .

TinyPols: a family of water-soluble binitroxides tailored for dynamic nuclear polarization enhanced NMR spectroscopy at 18.8 and 21.1 T†

D. Gajan, A. Lund, A. Lesage, 2020, Chemical science.

Influences of Dilute Organic Adsorbates on the Hydration of Low-Surface-Area Silicates.

L. Roberts, D. Gajan, A. Lesage, 2015, Journal of the American Chemical Society.

Refocused linewidths less than 10 Hz in 1H solid-state NMR.

M. Halse, A. Lesage, L. Emsley, 2018, Journal of magnetic resonance.

Assignment and Measurement of Deuterium Quadrupolar Couplings in Liquid Crystals by Deuterium−Carbon NMR Correlation Spectroscopy

A. Lesage, C. Auger, S. Caldarelli, 1998 .

Atomic Description of the Interface between Silica and Alumina in Aluminosilicates through Dynamic Nuclear Polarization Surface-Enhanced NMR Spectroscopy and First-Principles Calculations

Céline Chizallet, Jeroen A. van Bokhoven, Lyndon Emsley, 2015, Journal of the American Chemical Society.

High resolution solid state NMR spectroscopy in surface organometallic chemistry: access to molecular understanding of active sites of well-defined heterogeneous catalysts.

F. Blanc, C. Copéret, A. Lesage, 2008, Chemical Society reviews.

High-resolution NMR of hydrogen in organic solids by DNP enhanced natural abundance deuterium spectroscopy.

A. Lesage, Aaron J. Rossini, L. Emsley, 2015, Journal of magnetic resonance.

Heteronuclear proton double quantum-carbon single quantum scalar correlation in solids.

A. Lesage, L. Emsley, Vipin Agarwal, 2014, Journal of magnetic resonance.

13C-detected through-bond correlation experiments for protein resonance assignment by ultra-fast MAS solid-state NMR.

I. Felli, R. Pierattelli, A. Lesage, 2013, Chemphyschem : a European journal of chemical physics and physical chemistry.

A comparison of the conformational distributions of the achiral symmetric liquid crystal dimer CB7CB in the achiral nematic and chiral twist-bend nematic phases.

G. R. Luckhurst, A. Lesage, M. Lelli, 2013, The journal of physical chemistry. B.

1H detection and dynamic nuclear polarization–enhanced NMR of Aβ1-42 fibrils

R. Griffin, S. Linse, D. Lalli, 2021, Proceedings of the National Academy of Sciences.

Solvent suppression in DNP enhanced solid state NMR.

A. Lesage, Aaron J. Rossini, L. Emsley, 2017, Journal of magnetic resonance.

Rapid Proton-Detected NMR Assignment for Proteins with Fast Magic Angle Spinning

Paul Guerry, Torsten Herrmann, Lyndon Emsley, 2014, Journal of the American Chemical Society.

Fast resonance assignment and fold determination of human superoxide dismutase by high-resolution proton-detected solid-state MAS NMR spectroscopy.

Torsten Herrmann, Ivano Bertini, Roberta Pierattelli, 2011, Angewandte Chemie.

Dynamic Nuclear Polarization Magic Angle Spinning NMR Combined with MD Simulations Permits Detection of Order and Disorder in Viral Assemblies

A. Gronenborn, H. Oschkinat, M. Caporini, 2019 .

Dynamic Nuclear Polarization Enhanced MAS NMR Spectroscopy for Structural Analysis of HIV-1 Protein Assemblies.

A. Gronenborn, W. T. Franks, H. Oschkinat, 2016, The journal of physical chemistry. B.

Dynamic Nuclear Polarization Enhanced MAS NMR for Structural Analysis of HIV-1 Protein Assemblies

A. Gronenborn, W. T. Franks, H. Oschkinat, 2016 .

Monolayer Doping of Silicon through Grafting a Tailored Molecular Phosphorus Precursor onto Oxide-Passivated Silicon Surfaces

R. Wischert, C. Copéret, A. Lesage, 2016 .

Characterization of different water pools in solid-state NMR protein samples

B. Meier, A. Lesage, A. Loquet, 2009, Journal of biomolecular NMR.

Amplifying Dynamic Nuclear Polarization of Frozen Solutions by Incorporating Dielectric Particles

A. Lesage, D. Kubicki, Aaron J. Rossini, 2014, Journal of the American Chemical Society.

Chemical shift correlations in disordered solids.

A. Lesage, L. Emsley, S. Cadars, 2005, Journal of the American Chemical Society.

Investigation of dipolar-mediated water-protein interactions in microcrystalline Crh by solid-state NMR spectroscopy.

F. Penin, A. Lesage, A. Böckmann, 2006, Journal of the American Chemical Society.

The performance of phase modulated heteronuclear dipolar decoupling schemes in fast magic-angle-spinning nuclear magnetic resonance experiments

A. Lesage, L. Emsley, G. D. Paëpe, 2003 .

A general strategy for obtaining 19F-19F and 13C-19F residual dipolar couplings in perfluorocarbons from the NMR spectroscopy of liquid crystalline samples.

E. Salager, A. Lesage, G. De Luca, 2010, Physical Chemistry, Chemical Physics - PCCP.

The structure and conformation of a mesogenic compound between almost zero and almost complete orientational order

A. Lesage, G. De Luca, J. Emsley, 2007 .

The indirect through-space F-F coupling in peri-difluoronaphthalene: is it anisotropic?

C. W. Mallory, A. Lesage, G. De Luca, 2008, Physical chemistry chemical physics : PCCP.

Experimental aspects of proton NMR spectroscopy in solids using phase-modulated homonuclear dipolar decoupling.

D. Sakellariou, A. Lesage, L. Emsley, 2003, Journal of magnetic resonance.

Spectroscopic Expression of the External Surface Sites of H-ZSM-5

A. Lesage, C. Chizallet, T. Bruin, 2021, The Journal of Physical Chemistry C.

Donor – acceptor stacking arrangements in bulk and thin- ﬁ lm high-mobility conjugated polymers characterized using molecular modelling and MAS and surface-enhanced solid-state NMR spectroscopy † EDGE ARTICLE

H. Sirringhaus, A. Lesage, V. Lemaur, 2017 .

Complete (1)H resonance assignment of beta-maltose from (1)H-(1)H DQ-SQ CRAMPS and (1)H (DQ-DUMBO)-(13)C SQ refocused INEPT 2D solid-state NMR spectra and first principles GIPAW calculations.

J. Yates, F. Mauri, A. M. Gil, 2010, Physical chemistry chemical physics : PCCP.

Enhanced sensitivity in high-resolution 1H solid-state NMR spectroscopy with DUMBO dipolar decoupling under ultra-fast MAS

E. Salager, A. Lesage, L. Emsley, 2009 .

Structure, Location, and Spatial Proximities of Hydroxyls on γ-Alumina Crystallites by High-Resolution Solid-State NMR and DFT Modeling: Why Edges Hold the Key

D. Gajan, A. Lesage, C. Chizallet, 2023, ACS Catalysis.

How Halogenation Impacts the Polymer Backbone Conformation: Learning from Combination of Solid‐State MAS NMR and X‐Ray Scattering

A. Lesage, D. Jacquemin, B. Heinrich, 2022, Advanced Functional Materials.

On the orientational dependence of resolution in 1H solid‐state NMR, and its role in MAS, CRAMPS and delayed‐acquisition experiments

A. Lesage, L. Emsley, P. Hodgkinson, 2007, Magnetic resonance in chemistry : MRC.

Dynamics and disorder in surfactant-templated silicate layers studied by solid-state NMR dephasing times and correlated line shapes

J. Epping, N. Hedin, A. Lesage, 2008 .

Band-selective 1H-13C cross-polarization in fast magic angle spinning solid-state NMR spectroscopy.

Roberta Pierattelli, Lyndon Emsley, Anne Lesage, 2008, Journal of the American Chemical Society.

Better characterization of surface organometallic catalysts through resolution enhancement in proton solid state NMR spectra.

R. Schrock, F. Blanc, C. Copéret, 2006, Inorganic Chemistry.

Carbon-13 lineshapes in solid-state NMR of labeled compounds. Effects of coherent CSA-dipolar cross-correlation.

D. Sakellariou, A. Lesage, L. Duma, 2003, Journal of magnetic resonance.

Out-and-back 13C–13C scalar transfers in protein resonance assignment by proton-detected solid-state NMR under ultra-fast MAS

W. T. Franks, I. Akopjana, K. Tārs, 2013, Journal of Biomolecular NMR.

Out-and-back 13C–13C scalar transfers in protein resonance assignment by proton-detected solid-state NMR under ultra-fast MAS

Lyndon Emsley, Emeline Barbet-Massin, Andrew J. Pell, 2013, Journal of biomolecular NMR.

Complete Resonance Assignment of a Natural Abundance Solid Peptide by Through-Bond Heteronuclear Correlation Solid-State NMR

A. Lesage, L. Emsley, S. Steuernagel, 2000 .

The structures and conformations of mesogenic molecules in the pre-transitional region of the isotropic phase: 5OCB and MBBA and their mixtures

A. Lesage, G. De Luca, J. Emsley, 2012 .

Magnetic field induced dipolar couplings in the pretransitional region of a nematic liquid crystal.

A. Lesage, J. Emsley, D. Merlet, 2005, Journal of Physical Chemistry A.

Quantitative analysis of backbone dynamics in a crystalline protein from nitrogen-15 spin-lattice relaxation.

M. Blackledge, F. Penin, A. Lesage, 2005, Journal of the American Chemical Society.

Site-specific backbone dynamics from a crystalline protein by solid-state NMR spectroscopy.

M. Blackledge, F. Penin, A. Lesage, 2004, Journal of the American Chemical Society.

Dinitrogen Dissociation on an Isolated Surface Tantalum Atom

E. A. Quadrelli, A. Lesage, L. Emsley, 2007, Science.

Solid-phase polarization matrixes for dynamic nuclear polarization from homogeneously distributed radicals in mesostructured hybrid silica materials.

Gunnar Jeschke, Lyndon Emsley, Anne Lesage, 2013, Journal of the American Chemical Society.

Characterizing slight structural disorder in solids by combined solid-state NMR and first principles calculations.

P. Sautet, C. Pickard, A. Lesage, 2009, The journal of physical chemistry. A.

THE STRUCTURE, CONFORMATION AND ORIENTATIONAL ORDER OF FLUORINATED LIQUID CRYSTALS DETERMINED FROM CARBON-13 NMR SPECTROSCOPY

A. Lesage, L. Emsley, L. Brennan, 1999 .

Carbon-13 spectral editing in solid-state NMR using heteronuclear scalar couplings

A. Lesage, L. Emsley, S. Steuernagel, 1998 .

Hammett Parameter in Microporous Solids as Macroligands for Heterogenized Photocatalysts

D. Farrusseng, E. A. Quadrelli, A. Lesage, 2018 .

Molecular Insight Into Surface Organometallic Chemistry Through the Combined Use of 2D HETCOR Solid‐State NMR Spectroscopy and Silsesquioxane Analogues

C. Copéret, E. A. Quadrelli, A. Lesage, 2002 .

Weak and Transient Protein Interactions Determined by Solid-State NMR.

N. Dixon, A. Lesage, Stefan Jehle, 2016, Angewandte Chemie.

Non-aqueous solvents for DNP surface enhanced NMR spectroscopy.

C. Copéret, D. Gajan, A. Lesage, 2012, Chemical communications.

Trehalose matrices for high temperature dynamic nuclear polarization enhanced solid state NMR.

A. Lesage, M. Lelli, O. Ouari, 2022, Physical chemistry chemical physics : PCCP.

Structural Analysis of an Antigen Chemically-Coupled on Virus-Like Particles in Vaccine Formulation.

A. Kazaks, K. Tārs, A. Lesage, 2021, Angewandte Chemie.

Dynamic nuclear polarization enhanced solid-state NMR spectroscopy of functionalized metal-organic frameworks.

D. Farrusseng, C. Copéret, A. Lesage, 2012, Angewandte Chemie.

Dynamic nuclear polarization at 40 kHz magic angle spinning

C. Copéret, D. Gajan, A. Lesage, 2016, Physical chemistry chemical physics : PCCP.

Silica-surface reorganization during organotin grafting evidenced by ¹¹⁹Sn DNP SENS: a tandem reaction of gem-silanols and strained siloxane bridges.

A. Comas‐Vives, C. Copéret, A. Lesage, 2014, Physical chemistry chemical physics : PCCP.

Polarizing agents for efficient high field DNP solid-state NMR spectroscopy under magic-angle spinning: from design principles to formulation strategies

D. Gajan, A. Lesage, O. Ouari, 2023, Chemical science.

Backbone assignment of fully protonated solid proteins by 1H detection and ultrafast magic-angle-spinning NMR spectroscopy.

N. Dixon, G. Otting, A. Park, 2012, Angewandte Chemie.

Methyl proton contacts obtained using heteronuclear through-bond transfers in solid-state NMR spectroscopy.

A. Lesage, A. Loquet, A. Böckmann, 2008, Journal of the American Chemical Society.

Dynamic nuclear polarization surface enhanced NMR spectroscopy.

C. Copéret, A. Lesage, Aaron J. Rossini, 2013, Accounts of chemical research.

Motional heterogeneity in single-site silica-supported species revealed by deuteron NMR.

C. Copéret, A. Lesage, R. Vold, 2009, Physical chemistry chemical physics : PCCP.

NMR signatures of the active sites in Sn-β zeolite.

A. Comas‐Vives, C. Copéret, A. Lesage, 2014, Angewandte Chemie.

The Molecular and Electronic Structure of Isolated Platinum Sites Enabled by Expedient Measurement of 195Pt Chemical Shift Anisotropy

C. Copéret, A. Lesage, Aaron J. Rossini, 2022 .

Reactive surface organometallic complexes observed using dynamic nuclear polarization surface enhanced NMR spectroscopy

Manoja K. Samantaray, D. Anjum, E. Abou‐hamad, 2016, Chemical science.

Gold nanoparticles supported on passivated silica: access to an efficient aerobic epoxidation catalyst and the intrinsic oxidation activity of gold.

C. Copéret, D. Gajan, A. Lesage, 2009, Journal of the American Chemical Society.

Characterization of surface organometallic complexes using high resolution 2D solid-state NMR spectroscopy. Application to the full characterization of a silica supported metal carbyne: (triple bond)SiO-Mo((triple bond)C-Bu-t)(CH(2)-Bu-t)(2).

C. Copéret, A. Lesage, L. Emsley, 2001, Journal of the American Chemical Society.

Sample restriction using magnetic field gradients in high-resolution solid-state NMR

Steuernagel, A. Lesage, L. Emsley, 2000, Journal of magnetic resonance.

Silica-surface reorganization during organotin grafting evidenced by ¹¹⁹Sn DNP SENS: a tandem reaction of gem-silanols and strained siloxane bridges.

A. Comas‐Vives, C. Copéret, A. Lesage, 2014, Physical chemistry chemical physics : PCCP.

Methane reacts with heteropolyacids chemisorbed on silica to produce acetic acid under soft conditions.

Jizhen Zhang, Miao Sun, E. Abou‐hamad, 2013, Journal of the American Chemical Society.

Solid-phase polarization matrixes for dynamic nuclear polarization from homogeneously distributed radicals in mesostructured hybrid silica materials.

G. Jeschke, C. Copéret, D. Gajan, 2013, Journal of the American Chemical Society.

Donor–acceptor stacking arrangements in bulk and thin-film high-mobility conjugated polymers characterized using molecular modelling and MAS and surface-enhanced solid-state NMR spectroscopy

A. Lesage, Y. Olivier, L. Emsley, 2017, Chemical science.

Cubic three-dimensional hybrid silica solids for nuclear hyperpolarization

G. Bodenhausen, C. Copéret, D. Gajan, 2016, Chemical science.