Cross-Correlation for Automated Stitching of Two-Dimensional Multi-Tile Electron Backscatter Diffraction Data (Preprint)

Abstract : A method for automatically aligning consecutive datasets of large, two-dimensional multi-tile electron backscatter diffraction (EBSD) scans with high accuracy was developed. The method involves first locating grain and phase boundaries within search regions containing overlapping data in adjacent scan tiles, and subsequently using cross-correlation algorithms to determine the relative position of the individual scan tiles which maximizes the fraction of overlapping boundaries. Savitzky-Golay filtering in two dimensions was used to estimate the background, which was then subtracted from the cross-correlation to enhance the peak signal in samples with a high density of interfaces. The technique was demonstrated on datasets with a range of grain boundary densities. The equations were implemented as enhancements to a recently published open source code for automated stitching of multi-tile datasets.

[1]  M. Mills,et al.  Determination of crystallographic orientation of dwell-fatigue fracture facets in Ti-6242 alloy , 2007 .

[2]  A. Authier,et al.  Physical properties of crystals , 2007 .

[3]  S. Daly,et al.  Small-scale patterning methods for digital image correlation under scanning electron microscopy , 2011 .

[4]  G. Nolze Image distortions in SEM and their influences on EBSD measurements. , 2007, Ultramicroscopy.

[5]  K. Kunze,et al.  The characterisation of microtexture by orientation mapping , 1994 .

[6]  D. Dimiduk,et al.  3D microstructural characterization of nickel superalloys via serial-sectioning using a dual beam FIB-SEM , 2006 .

[7]  M. Mills,et al.  In-Situ Mechanical Testing for Characterizing Strain Localization During Deformation at Elevated Temperatures , 2012 .

[8]  A L Pilchak,et al.  A novel method for acquiring large‐scale automated scanning electron microscope data , 2011, Journal of microscopy.

[9]  A. Savitzky,et al.  Smoothing and Differentiation of Data by Simplified Least Squares Procedures. , 1964 .

[10]  T. Bieler,et al.  The origins of heterogeneous deformation during primary hot working of Ti–6Al–4V , 2002 .

[11]  Somnath Ghosh,et al.  3D reconstruction and characterization of polycrystalline microstructures using a FIB-SEM system , 2006 .

[12]  M. Graef,et al.  Application and further development of advanced image processing algorithms for automated analysis of serial section image data , 2009 .

[13]  H. H. Madden Comments on the Savitzky-Golay convolution method for least-squares-fit smoothing and differentiation of digital data , 1976 .

[14]  S. Dey,et al.  Determination of parent orientation maps in advanced titanium‐based alloys , 2007, Journal of microscopy.

[16]  A L Pilchak,et al.  AnyStitch: a tool for combining electron backscatter diffraction data sets , 2011, Journal of microscopy.