Studies in multiple impeller agitated gas–liquid contactors

Experiments have been performed to study the effect of the density and the volume of the tracer pulse on the mixing time for two impeller combinations in the presence of gas in a 0.3 m diameter and 1 m tall cylindrical acrylic vessel. The tall multi-impeller aerobic fermenters, which require periodic dosing of nutrients that are in the form of aqueous solution, is a classic case under consideration. Conductivity measuring method was used to measure the mixing time. Two triple impeller combinations; one containing two pitched blade downflow turbines as upper impellers and disc turbine as the lowermost impeller (2 PBTD-DT) and another containing all pitched blade downflow turbines (3 PBTD) have been used. Other variables covered during experiments were the density and the amount of the tracer pulse, the impeller rotational speed and the gas superficial velocity. Fractional gas hold-up, Power consumption and mass transfer coefficient have also been measured for both the impeller combinations. Influence of aeration and impeller speed on the mixing time has been explained by the interaction of air induced and impeller generated liquid flows. Three different flow regimes have been distinguished to explain the hydrodynamics of the overall vessel (i.e., multiple impeller system). A compartment model with the number of compartments varying with the flow regimes have been used to model liquid phase mixing in these flow regimes. A correlation for the prediction of the dimensionless mixing time in the loading regime has been proposed in order to account the effect of the density and the amount of the tracer pulse on the mixing time. Correlations have also been proposed to predict fractional gas hold-up and k L a.

[1]  J. Rushton,et al.  Holdup and flooding in air liquid mixing , 1968 .

[2]  J. Joshi,et al.  Some design features of radial baffles in sectionalised bubble columns , 1979 .

[3]  Milan Jahoda,et al.  Homogenization of liquids in tanks stirred by multiple impellers , 1994 .

[4]  Milan Jahoda,et al.  Liquid Homogenization in Aerated Multi‐Impeller Stirred Vessel , 2000 .

[5]  A. Nienow,et al.  Comparison of Experimental Techniques for the Measurement of Mixing Time in Gas‐Liquid Systems , 2001 .

[6]  Gogate,et al.  Multiple-impeller systems with a special emphasis on bioreactors: a critical review. , 2000, Biochemical engineering journal.

[7]  Alvin W. Nienow,et al.  Scale‐up of mixing in gassed multi‐turbine agitated vessels , 1998 .

[8]  Jyeshtharaj B. Joshi,et al.  Role of sparger design in mechanically agitated gas‐liquid reactors. Part I: Power consumption , 1991 .

[9]  Jorge M. M. Barata,et al.  Mixing in gas-liquid contactors agitated by multiple turbines , 1995 .

[10]  Franco Magelli,et al.  A fluid-dynamic study of a gas—liquid, non-standard vessel stirred by multiple impellers , 1988 .

[11]  Alvin W. Nienow,et al.  Gas–liquid dispersion with dual Rushton impellers , 1989 .

[12]  P. Gogate,et al.  Mixing of miscible liquids with density differences : Effect of volume and density of the tracer fluid , 1999 .

[13]  P. Beneš,et al.  A critical review and experimental verification of the correct use of the dynamic method for the determination of oxygen transfer in aerated agitated vessels to water, electrolyte solutions and viscous liquids , 1987 .

[14]  Serafim D. Vlaev,et al.  A 3-D Analysis of Gas-Liquid Mixing, Mass Transfer and Bioreaction in a Stirred Bio-Reactor , 2001 .

[15]  Václav Linek,et al.  Gas hold-up, mixing time and gas-liquid volumetric mass transfer coefficient of various multiple-impeller configurations: Rushton turbine, pitched blade and techmix impeller and their combinations , 2003 .

[16]  Jorge M. M. Barata,et al.  Alternative compartment models of mixing in tall tanks agitated by multi-Rushton turbines , 1997 .

[17]  G. Baldi,et al.  Sparged vessels agitated by multiple turbines , 1988 .

[18]  S. A. Miller,et al.  Power requirements of gas‐liquid agitated systems , 1962 .

[19]  Aniruddha B. Pandit,et al.  Mechanically agitated gas-liquid reactors , 1982 .

[20]  Ashwin W. Patwardhan,et al.  MIXING IN TANKS AGITATED BY JETS , 2003 .

[21]  P. Gogate,et al.  Effect of tracer properties (volume, density and viscosity) on mixing time in mechanically agitated contactors , 2000 .

[22]  Alvin W. Nienow,et al.  Mixing in large-scale vessels stirred with multiple radial or radial and axial up-pumping impellers: modelling and measurements , 2000 .

[23]  Alvin W. Nienow,et al.  Gas—liquid mixing studies with multiple up‐ and down‐pumping hydrofoil impellers: Power characteristics and mixing time , 1998 .

[24]  Jorge M. T. Vasconcelos,et al.  Mixing in gas-liquid contactors agitated by multiple turbines in the flooding regime , 1995 .

[25]  Gopal R. Kasat,et al.  Mixing Time Studies in Multiple Impeller Agitated Reactors , 2008 .

[26]  Aniruddha B. Pandit,et al.  Mixing in mechanically agitated gas-liquid contactors, bubble columns and modified bubble columns , 1983 .

[27]  The Mixing of Miscible Liquids with Large Differences in Density and Viscosity , 1992 .

[28]  Peter Vrábel,et al.  Compartment Model Approach: Mixing in Large Scale Aerated Reactors with Multiple Impellers , 1999 .

[29]  H. V. D. Akker,et al.  Blending Liquids of Differing Viscosities and Densities in Stirred Vessels , 1997 .