Experimental investigation of porosities evolution in a bonded assembly by means of X-ray tomography

ABSTRACT Structral bonding is a very advantageous technique for lots of application fields such as aeronautics or marine industry, which require both advanced performances and lightweight structures. Nonetheless, adhesive joints are often subject to bonding defects: kissing bonds, uneven polymerisation, or pores within the material, for instance. These pores, depending on their sizes and distributions, could jeopardise the mechanical strength of the assembly. Moreover, it is legitimate to hypothesise that these voids in the medium could be influenced by the application of a mechanical stress. In order to investigate this assertion, bonded samples are loaded by various tensile stress levels, and the pores within the joint are visualised and characterised using in-situ X-ray microtomography. This paper deals with the evolutions of various quantities such as the number of pores or their volumetric ratio along with the increasing load and with the diverse phenomena (nucleation, growth, coalescence, etc.) experienced during the testings. These results are extracted from the microtomographic data using a custom processing tool, whose parameters and performances are discussed.

[1]  Victoria Burt Adhesive Bonding , 2018, Aluminum Science and Technology.

[2]  C. Bădulescu,et al.  A viscoelastic-viscoplastic model to describe creep and strain rate effects on the mechanical behaviour of adhesively-bonded assemblies , 2017 .

[3]  S. Adamopoulos,et al.  Study of adhesive bondlines in modified wood with fluorescence microscopy and X-ray micro-computed tomography , 2016 .

[4]  C. Bădulescu,et al.  3D models of specimens with a scarf joint to test the adhesive and cohesive multi-axial behavior of adhesives , 2015 .

[5]  F. Kamke,et al.  Quantitative wood–adhesive penetration with X-ray computed tomography , 2015 .

[6]  S. Mahdi,et al.  Characterization and modelling of the 3D elastic–plastic behaviour of an adhesively bonded joint under monotonic tension/compression-shear loads: influence of three cure cycles , 2013 .

[7]  C. Bădulescu,et al.  Analysis of the low temperature-dependent behaviour of a ductile adhesive under monotonic tensile/compression–shear loads , 2012 .

[8]  Johannes E. Schindelin,et al.  Fiji: an open-source platform for biological-image analysis , 2012, Nature Methods.

[9]  M. Stampanoni,et al.  3D-characterization of three-phase systems using X-ray tomography: tracking the microstructural evolution in ice cream , 2012 .

[10]  David Legland,et al.  Efficient N-Dimensional surface estimation using Crofton formula and run-length encoding , 2012, The Insight Journal.

[11]  J. Cognard,et al.  Numerical analysis of the stress distribution in single-lap shear tests under elastic assumption—Application to the optimisation of the mechanical behaviour , 2011 .

[12]  Eric Maire,et al.  In situ observation of ductile fracture using X-ray tomography technique , 2011 .

[13]  T. Senden,et al.  Visualization and numerical analysis of adhesive distribution in particleboard using X-ray micro-computed tomography , 2010 .

[14]  E. Maire,et al.  In Situ Experiments with X ray Tomography: an Attractive Tool for Experimental Mechanics , 2010 .

[15]  Peter Davies,et al.  Analysis of the nonlinear behavior of adhesives in bonded assemblies—Comparison of TAST and Arcan tests , 2008 .

[16]  I. Sinclair,et al.  Evolution of voids during ductile crack propagation in an aluminium alloy sheet toughness test studied by synchrotron radiation computed tomography , 2008 .

[17]  S. Roux,et al.  Three dimensional image correlation from X-Ray computed tomography of solid foam , 2007, 0712.2642.

[18]  Peter Davies,et al.  A study of the non-linear behaviour of adhesively-bonded composite assemblies , 2006 .

[19]  R. Mahnken,et al.  Simulation of strength difference in elasto‐plasticity for adhesive materials , 2005 .

[20]  Viggo Tvergaard,et al.  Void growth and coalescence in metals deformed at elevated temperature , 2000 .

[21]  L. Feldkamp,et al.  Practical cone-beam algorithm , 1984 .

[22]  G. Wise,et al.  A theoretical analysis of the properties of median filters , 1981 .

[23]  B. Pollak Experiences with planography. , 1953, Diseases of the chest.

[24]  H. Wadell,et al.  Volume, Shape, and Roundness of Quartz Particles , 1935, The Journal of Geology.

[25]  Stéphane Roux,et al.  Identification of the crushing behavior of brittle foam: From indentation to oedometric tests , 2017 .

[26]  Andreas Öchsner,et al.  Modeling of Adhesively Bonded Joints , 2008 .

[27]  R. Adams Adhesive bonding : science, technology and applications , 2005 .

[28]  M. Glas,et al.  Principles of Computerized Tomographic Imaging , 2000 .

[29]  Jorge Herbert de Lira,et al.  Two-Dimensional Signal and Image Processing , 1989 .