Interband cascade laser based quartz-enhanced photoacoustic sensor for multiple hydrocarbons detection

Hydrocarbon detection in the gas phase can be a powerful tool to guide downstream operations for the oil & gas industry. This application requires highly sensitive, selective and robust spectroscopic techniques. In this work, a quartz-enhanced photoacoustic sensor system designed to detect methane and ethane concentration levels in the part-per billion concentration range by employing a single interband cascade laser emitting at 3345 nm is reported. Measurements at both low and high pressure were carried out and mixtures simulating typical downhole compositions were analyzed.

[1]  J. Speight The Chemistry and Technology of Petroleum , 1980 .

[2]  Yao-Ming Mu,et al.  Interband cascade lasers , 2000, Photonics West - Optoelectronic Materials and Devices.

[3]  A. Kosterev,et al.  Quartz-enhanced photoacoustic spectroscopy. , 2002, Optics letters.

[4]  C. Webster,et al.  Measuring methane and its isotopes 12CH4, 13CH4, and CH3D on the surface of Mars with in situ laser spectroscopy. , 2005, Applied optics.

[5]  A. Kosterev,et al.  Applications of quartz tuning forks in spectroscopic gas sensing , 2005 .

[6]  Federico Capasso,et al.  High-performance midinfrared quantum cascade lasers , 2010 .

[7]  Jerry R. Meyer,et al.  Special Section Guest Editorial: Quantum and Interband Cascade Lasers , 2010 .

[8]  M. Fischer,et al.  Continuous-wave operation of type-I quantum well DFB laser diodes emitting in 3.4 μm wavelength range around room temperature , 2011 .

[9]  S. Borri,et al.  Molecular gas sensing below parts per trillion: radiocarbon-dioxide optical detection. , 2011, Physical review letters.

[10]  Markus-Christian Amann,et al.  Single mode and tunable GaSb-based VCSELs for wavelengths above 2 μm , 2011, OPTO.

[11]  Daqiang Zhang,et al.  A Survey on Gas Sensing Technology , 2012, Sensors.

[12]  G. Scamarcio,et al.  Part-per-trillion level SF6 detection using a quartz enhanced photoacoustic spectroscopy-based sensor with single-mode fiber-coupled quantum cascade laser excitation. , 2012, Optics letters.

[13]  R. Tatam,et al.  Optical gas sensing: a review , 2012 .

[14]  Frank K. Tittel,et al.  Quartz-Enhanced Photoacoustic Spectroscopy: A Review , 2014, Sensors.

[15]  Xukun Yin,et al.  Quartz enhanced photoacoustic H2S gas sensor based on a fiber-amplifier source and a custom tuning fork with large prong spacing , 2015 .

[16]  G. Scamarcio,et al.  Quartz-enhanced photoacoustic spectroscopy exploiting tuning fork overtone modes , 2015 .

[17]  Huadan Zheng,et al.  Single-tube on-beam quartz-enhanced photoacoustic spectroscopy. , 2016, Optics letters.

[18]  Frank K. Tittel,et al.  Analysis of the electro-elastic properties of custom quartz tuning forks for optoacoustic gas sensing , 2016 .

[19]  Angelo Sampaolo,et al.  Compact TDLAS based sensor design using interband cascade lasers for mid-IR trace gas sensing. , 2016, Optics express.

[20]  Vincenzo Spagnolo,et al.  Analysis of overtone flexural modes operation in quartz-enhanced photoacoustic spectroscopy. , 2016, Optics express.

[21]  Frank K. Tittel,et al.  Allan Deviation Plot as a Tool for Quartz-Enhanced Photoacoustic Sensors Noise Analysis , 2016, IEEE Transactions on Ultrasonics, Ferroelectrics, and Frequency Control.

[22]  Frank K. Tittel,et al.  Infrared Dual-Gas CH4/C2H6 Sensor Using Two Continuous-Wave Interband Cascade Lasers , 2016, IEEE Photonics Technology Letters.

[23]  Huadan Zheng,et al.  Overtone resonance enhanced single-tube on-beam quartz enhanced photoacoustic spectrophone , 2016 .

[24]  Frank K. Tittel,et al.  Improved Tuning Fork for Terahertz Quartz-Enhanced Photoacoustic Spectroscopy , 2016, Sensors.

[25]  Xian Zhao,et al.  Photoacoustic trace detection of gases at the parts-per-quadrillion level with a moving optical grating , 2017, Proceedings of the National Academy of Sciences.

[26]  Huadan Zheng,et al.  Quartz–enhanced photoacoustic spectrophones exploiting custom tuning forks: a review , 2017 .

[27]  Frank K. Tittel,et al.  Recent advances in quartz enhanced photoacoustic sensing , 2018 .

[28]  Igor Vurgaftman,et al.  Quantum and Interband Cascade Lasers , 2019 .