Density and Thermal Expansion of High Purity Nickel over the Temperature Range from 150 K to 2030 K

The paper presents the results of an investigation of the nickel density and thermal expansion over the temperature range from 145 K to 2030 K. The measurements have been carried out by using the dilatometer method and the $$\upgamma $$γ-ray attenuation technique (gamma method). The errors of the density and coefficients of thermal expansion measurements are estimated to be within 0.05 % to 0.25 % and 1 % to 2.5 %, respectively. The accuracy of determination of the volumetric thermal expansion coefficient of the melt by the $$\upgamma $$γ-ray attenuation technique is substantiated. The density change on melting ($$4.70 \pm 0.15$$4.70±0.15) % has been directly measured. The temperature dependences and reference tables of the volumetric properties of solid and liquid nickel have been developed. A comparison of the obtained results with literature data has been made.

[1]  S. Stankus,et al.  Density and phase diagram of the magnesium–lead system in the region of Mg2Pb intermetallic compound , 2008 .

[2]  R. G. Ward,et al.  The Density of Nickel in the Superheated and Supercooled Liquid States , 1964 .

[3]  Y. Tanji Thermal Expansion Coefficient and Spontaneous Volume Magnetostriction of Fe-Ni (fcc) Alloys , 1971 .

[4]  S. Stankus,et al.  Measurement of the thermal properties of platinum in the temperature interval 293-2300 K by the method of penetrating radiation , 1992 .

[5]  Y. Sakuma,et al.  Density Measurement of Molten Metals by Levitation Technique at Temperatures between 1800° and 2200℃ , 1969 .

[6]  S. Steinemann,et al.  Density and Thermal Expansion of Molten Manganese, Iron, Nickel, Copper, Aluminum and Tin by Means of the Gamma-Ray Attenuation Technique , 1995 .

[7]  S. I. Novikova Thermal expansion of solids , 1974 .

[8]  F. R. Kroeger,et al.  Absolute linear thermal‐expansion measurements on copper and aluminum from 5 to 320 K , 1977 .

[9]  Y. F. Wang,et al.  Density and molar volume of liquid Ni–Co binary alloys , 2006 .

[10]  D. Thiessen,et al.  Erratum: A noncontact measurement technique for the density and thermal expansion coefficient of solid and liquid materials [Rev. Sci. Instrum. 67, 3175 (1996)] , 1997 .

[11]  J. Brillo,et al.  Density Determination of Liquid Copper, Nickel, and Their Alloys , 2003 .

[12]  S. Stankus,et al.  Thermal expansion of beryllium oxide in the temperature interval 20–1550°C , 2014 .

[13]  T. G. Kollie,et al.  Measurement of the thermal-expansion coefficient of nickel from 300 to 1000 K and determination of the power-law constants near the Curie temperature , 1977 .

[14]  Y. Sakuma,et al.  Densities of Pure Iron, Cobalt and Nickel in the Molten State , 1967 .

[15]  L. D. Zagrebin,et al.  Quasistationary measurement of thermophysical properties at high temperatures and high pressures , 1989 .

[16]  D. Thiessen,et al.  A noncontact measurement technique for the density and thermal expansion coefficient of solid and liquid materials , 1996 .

[17]  R. K. Kirby Platinum—A thermal expansion reference material , 1991 .