Performance Evaluation and Comparison between Direct and Chemical-Assisted Picosecond Laser Micro-Trepanning of Single Crystalline Silicon

The fabrication of micro-holes in silicon substrates that have a proper taper, higher depth-to-diameter ratio, and better surface quality has been attracting intense interest for a long time due to its importance in the semiconductor and MEMS (Micro-Electro-Mechanical System) industry. In this paper, an experimental investigation of the machining performance of the direct and chemical-assisted picosecond laser trepanning of single crystalline silicon is conducted, with a view to assess the two machining methods. The relevant parameters affecting the trepanning process are considered, employing the orthogonal experimental design scheme. It is found that the direct laser trepanning results are associated with evident thermal defects, while the chemical-assisted method is capable of machining micro-holes with negligible thermal damage. Range analysis is then carried out, and the effects of the processing parameters on the hole characteristics are amply discussed to obtain the recommended parameters. Finally, the material removal mechanisms that are involved in the two machining methods are adequately analyzed. For the chemical-assisted trepanning case, the enhanced material removal rate may be attributed to the serious mechanical effects caused by the liquid-confined plasma and cavitation bubbles, and the chemical etching effect provided by NaOH solution.

[1]  Jun Wang,et al.  A study of hybrid laser–waterjet micromachining of crystalline germanium , 2018 .

[2]  Jun Wang,et al.  Analysis of the machining performance and surface integrity in laser milling of polycrystalline diamonds , 2014 .

[3]  A. Vogel,et al.  Laser-induced plasma formation in water at nanosecond to femtosecond time scales: Calculation of thresholds, absorption coefficients, and energy density , 1999 .

[4]  C. Leone,et al.  Experimental study of fibre laser microdrilling of aerospace superalloy by trepanning technique , 2017 .

[5]  Yoshiro Ito,et al.  Trepanning drilling of microholes on cemented tungsten carbide using femtosecond laser pulses , 2012 .

[6]  R. Clady,et al.  Crossing the threshold of ultrafast laser writing in bulk silicon , 2017, Nature Communications.

[7]  J. Mazumder,et al.  Modelling of high-density laser-material interaction using fast level set method , 2001 .

[8]  Laser-induced chemical etching of silicon in chlorine atmosphere , 1987 .

[9]  P. Mannion,et al.  STEM (scanning transmission electron microscopy) analysis of femtosecond laser pulse induced damage to bulk silicon , 2005 .

[10]  Stefan Nolte,et al.  Laser helical drilling of silicon wafers with ns to fs pulses: Scanning electron microscopy and transmission electron microscopy characterization of drilled through-holes , 2006 .

[11]  Y. Shin,et al.  A self-closed thermal model for laser shock peening under the water confinement regime configuration and comparisons to experiments , 2005 .

[12]  A. Tünnermann,et al.  Femtosecond, picosecond and nanosecond laser ablation of solids , 1996 .

[13]  N. Ren,et al.  Effects of ultrasonic assistance on microhole drilling based on Nd:YAG laser trepanning , 2018, Optics & Laser Technology.

[14]  D. Kray,et al.  Comparison of Laser Chemical Processing and LaserMicroJet for structuring and cutting silicon substrates , 2009 .

[15]  P. Corkum,et al.  Influence of laser parameters and material properties on micro drilling with femtosecond laser pulses , 1999 .

[16]  K. Ehmann,et al.  High throughput microfabrication using laser induced plasma in saline aqueous medium , 2015 .

[17]  Hans Joachim Eichler,et al.  Laser Trepanning for Industrial Applications , 2011 .

[18]  Klaus Sokolowski-Tinten,et al.  The physical mechanisms of short-pulse laser ablation , 2000 .

[19]  I. Choudhury,et al.  Hole qualities in laser trepanning of polymeric materials , 2012 .

[20]  Zhaoyang Zhang,et al.  An experimental study of micro-machining of hydroxyapatite using an ultrashort picosecond laser , 2018, Precision Engineering.

[21]  H. Zheng,et al.  Micro-machining of silicon wafer in air and under water , 2011 .

[22]  R. Fabbro,et al.  Experimental determination by PVDF and EMV techniques of shock amplitudes induced by 0.6-3 ns laser pulses in a confined regime with water , 2000 .

[23]  D. Ehrlich,et al.  Laser chemical technique for rapid direct writing of surface relief in silicon , 1981 .

[24]  Nagahanumaiah,et al.  Comparative Assessment of the Laser Induced Plasma Micromachining and the Micro-EDM Processes , 2014 .

[25]  Kun Xu,et al.  An Investigation into Picosecond Laser Micro-Trepanning of Alumina Ceramics Employing a Semi-Water-Immersed Scheme , 2019, Materials.

[26]  Benxin Wu High-intensity nanosecond-pulsed laser-induced plasma in air, water, and vacuum: A comparative study of the early-stage evolution using a physics-based predictive model , 2008 .

[27]  Jun Wang,et al.  An investigation of hybrid laser–waterjet ablation of silicon substrates , 2012 .

[28]  David J. Hwang,et al.  Femtosecond laser drilling of crystalline and multicrystalline silicon for advanced solar cell fabrication , 2012 .

[29]  Bo Tan,et al.  Deep micro hole drilling in a silicon substrate using multi-bursts of nanosecond UV laser pulses , 2005 .

[30]  B. Yilbas,et al.  Laser trepanning of a small diameter hole in titanium alloy: Temperature and stress fields , 2011 .

[31]  G. Willeke,et al.  Comparative Study of Laser Induced Damage in Silicon Wafers , 2006, 2006 IEEE 4th World Conference on Photovoltaic Energy Conference.

[32]  Yong Liu,et al.  Fabrication of Taper Free Micro-Holes Utilizing a Combined Rotating Helical Electrode and Short Voltage Pulse by ECM , 2019, Micromachines.

[33]  Kyung-Jin Choi,et al.  Analysis of silicon via hole drilling for wafer level chip stacking by UV laser , 2010 .

[34]  Kurt W. Kolasinski,et al.  Ultrafast-laser-assisted chemical restructuring of silicon and germanium surfaces , 2007 .

[35]  A. Welch,et al.  Shielding properties of laser-induced breakdown in water for pulse durations from 5 ns to 125 fs. , 1997, Applied Optics.

[36]  Bo Chen,et al.  Laser repeat drilling of alumina ceramics in static water , 2018 .

[37]  Seung Ki Moon,et al.  Influence of substrate heating on hole geometry and spatter area in femtosecond laser drilling of silicon , 2014 .

[38]  J. Kaakkunen,et al.  Water-Assisted Femtosecond Laser Pulse Ablation of High Aspect Ratio Holes , 2011 .

[39]  A. Diaspro,et al.  Very large spot size effect in nanosecond laser drilling efficiency of silicon. , 2010, Optics express.

[40]  Yves Bellouard,et al.  A Monolithic Micro-Tensile Tester for Investigating Silicon Dioxide Polymorph Micromechanics, Fabricated and Operated Using a Femtosecond Laser , 2015, Micromachines.

[41]  Hongyu Zheng,et al.  Role of volatile liquids in debris and hole taper angle reduction during femtosecond laser drilling of silicon , 2011 .

[42]  Lin Li,et al.  Chemical Assisted Laser Machining for The Minimisation of Recast and Heat Affected Zone , 2004 .

[43]  Jun Wang,et al.  Heat transfer and material ablation in hybrid laser-waterjet microgrooving of single crystalline germanium , 2017 .