Numerical prediction and experimental characterisation of meso-scale-voids in liquid composite moulding

Pressure gradients that drive the resin flow during liquid composite moulding (LCM) processes can be very low while manufacturing large composite parts. Capillary pressure becomes the predominant force for tow impregnation and thus meso-scale-voids can be generated, reducing the part quality. In contrast, micro-voids are created at high resin pressure gradients. In this work, a numerical method is presented to predict the creation of meso-scale-voids and their evolution. Experimental validation is conducted by measuring void content of produced composite parts with micro-computed tomography (μ-CT). Additionally, the void content as a function of the modified capillary number Ca∗ is determined and the influence of the fibre volume content in the bundles on the meso-scale- and micro-void content is studied.

[1]  K. Pillai,et al.  Experimental Investigation of the Effect of Fiber-mat Architecture on the Unsaturated Flow in Liquid Composite Molding , 2004 .

[2]  M. Altan,et al.  Three-dimensional features of void morphology in resin transfer molded composites , 2005 .

[3]  Christophe Binetruy,et al.  A new numerical procedure to predict dynamic void content in liquid composite molding , 2006 .

[4]  Geon‐Woong Lee,et al.  Mechanism of Void Formation in Composite Processing with Woven Fabrics , 2003 .

[5]  George H. Staab,et al.  A Note on the Effects of Voids Upon the Hygral and Mechanical Properties of AS4/3502 Graphite/Epoxy , 1987 .

[6]  B. R. Gebart,et al.  Permeability of Unidirectional Reinforcements for RTM , 1992 .

[7]  Suresh G. Advani,et al.  A numerical model to predict fiber tow saturation during liquid composite molding , 2003 .

[8]  W. Young The Effect of Surface Tension on Tow Impregnation of Unidirectional Fibrous Preform in Resin Transfer Molding , 1996 .

[9]  L. J. Lee,et al.  Experimental investigation of flow-induced microvoids during impregnation of unidirectional stitched fiberglass mat , 1996 .

[10]  Analysis of void removal in liquid composite molding using microflow models , 2002 .

[11]  Shawn M. Walsh,et al.  Analytic characterization of the permeability of dual-scale fibrous porous media , 2006 .

[12]  L. J. Lee,et al.  Effects of fiber mat architecture on void formation and removal in liquid composite molding , 1995 .

[13]  S. Advani,et al.  Investigation of unsaturated flow in woven, braided and stitched fiber mats during mold‐filling in resin transfer molding , 2001 .

[14]  Krishna M. Pillai,et al.  Modeling the Unsaturated Flow in Liquid Composite Molding Processes: A Review and Some Thoughts , 2004 .

[15]  Rikard Gebart,et al.  Influence from process parameters on void formation in resin transfer molding , 1994 .

[16]  Joël Bréard,et al.  Void fraction prevision in LCM parts , 2001 .

[17]  S. R. Ghiorse,et al.  Effect of void content on the mechanical properties of carbon/epoxy laminates , 1993 .

[18]  L. Hourng,et al.  Numerical Study on the Capillary Effect of Resin Transfer Molding , 1997 .

[19]  S. Advani,et al.  Correlation of void distribution to VARTM manufacturing techniques , 2007 .

[20]  Paolo Ermanni,et al.  Micro-computed tomography determination of glass fibre reinforced polymer meso structure , 2006 .

[21]  C. Macosko,et al.  Wetting of fiber mats for composites manufacturing: I. Visualization experiments , 1995 .

[22]  L. Hourng,et al.  Study on void formation in resin transfer molding , 1998 .

[23]  Yunguang Chen,et al.  Capillary Impregnation of Aligned Fibrous Beds: Experiments and Model , 1996 .

[24]  C. Binetruy,et al.  Tow Impregnation Model and Void Formation Mechanisms during RTM , 1998 .

[25]  A. Saouab,et al.  Numerical simulation of void formation in LCM , 2003 .

[26]  Suresh G. Advani,et al.  The interaction between micro- and macro-scopic flow in RTM preforms , 1994 .

[27]  F. Trochu,et al.  Optimization of injection flow rate to minimize micro/macro-voids formation in resin transfer molded composites , 2006 .

[28]  J. Gillespie,et al.  Modeling the Effect of Fiber Diameter and Fiber Bundle Count on Tow Impregnation during Liquid Molding Processes , 2005 .

[29]  P. Ermanni,et al.  Experimental Determination of the Transversal and Longitudinal Fibre Bundle Permeability , 2007 .

[30]  Liu Yi,et al.  Study on void formation in multi-layer woven fabrics , 2004 .

[31]  L. J. Lee,et al.  Micro scale flow behavior and void formation mechanism during impregnation through a unidirectional stitched fiberglass mat , 1995 .

[32]  James Glimm,et al.  Case Study from Industry: Process Modeling in Resin Transfer Molding as a Method to Enhance Product Quality , 1997, SIAM Rev..

[33]  B. Gebart,et al.  Void Formation in RTM , 1993 .

[34]  Woo Il Lee,et al.  Formation of microvoids during resin-transfer molding process , 2000 .

[35]  Frederick R. Phelan,et al.  Modeling void formation dynamics in fibrous porous media with the lattice Boltzmann method , 1998 .

[36]  R. J. Morgan,et al.  Tow impregnation during resin transfer molding of bi-directional nonwoven fabrics , 1993 .

[37]  Shawn M. Walsh,et al.  Permeability characterization of dual scale fibrous porous media , 2006 .

[38]  T. Lundström Measurement of void collapse during resin transfer moulding , 1997 .

[39]  C. Kaynak,et al.  Effects of Injection Pressure in Resin Transfer Moulding (RTM) of Woven Carbon Fibre/Epoxy Composites , 2006 .