Specific-heat measurement of single metallic, carbon, and ceramic fibers at very high temperature

The main objective of this work is to present a method for measuring the specific heat of single metallic, carbon, and ceramic fibers at very high temperature. The difficulty of the measurement is due to the microscale of the fiber (≈10μm) and the important range of temperature (700–2700K). An experimental device, a modelization of the thermal behavior, and an analytic model have been developed. A discussion on the measurement accuracy yields a global uncertainty lower than 10%. The characterization of a tungsten filament with thermal properties identical to those of the bulk allows the validation of the device and the thermal estimation method. Finally, measurements on carbon and ceramic fibers have been done at very high temperature.