Structural characterization of (3-aminopropyl)triethoxysilane-modified silicas by silicon-29 and carbon-13 nuclear magnetic resonance

[1]  W. Hertl,et al.  Acidity of surface hydroxyl groups , 1970 .

[2]  G. Maciel,et al.  Spin dynamics in the carbon-13 nuclear magnetic resonance spectrometric analysis of coal by cross polarization and magic-angle spinning , 1982 .

[3]  J. Koenig,et al.  The structure of γ-aminopropyltriethoxysilane on glass surfaces , 1980 .

[4]  G. Maciel,et al.  Setting the magic angle using a quadrupolar nuclide , 1982 .

[5]  J. Koenig,et al.  Magic-angle cross-polarization carbon 13 NMR study of aminosilane coupling agents on silica surfaces , 1982 .

[6]  G. Maciel,et al.  Silicon-29 NMR study of the surface of silica gel by cross polarization and magic-angle spinning , 1980 .

[7]  Michael Mehring,et al.  Principles of high-resolution NMR in solids , 1982 .

[8]  G. Maciel,et al.  Silicon-29 nuclear magnetic resonance study of hydroxyl sites on dehydrated silica gel surfaces, using silylation as a probe , 1983 .

[9]  SOLID‐STATE NMR STUDIES OF THE REACTIONS OF SILICA SURFACES WITH POLYFUNCTIONAL CHLOROMETHYLSILANES AND ETHOXYMETHYLSILANES , 1983 .

[10]  G. Maciel,et al.  Cross-polarization magic-angle-spinning silicon-29 nuclear magnetic resonance study of silica gel using trimethylsilane bonding as a probe of surface geometry and reactivity , 1982 .

[11]  G. Maciel,et al.  Carbon-13 CP/MAS NMR study of molecular motion in n-alkylsilane bonded to the silica surface , 1983 .

[12]  U. Haeberlen,et al.  Cross polarization in solids with flip-back of I-spin magnetization , 1979 .

[13]  T. Zeegers-Huyskens Influence des liaisons hydrogène sur les vibrations de valence NH2 des amines aliphatiques , 1965 .

[14]  V. Bartuska,et al.  Characterization of silica-attached systems by 29Si and 13C cross-polarization and magic-angle spinning nuclear magnetic resonance , 1981 .

[15]  C. N. Reilley,et al.  Chemical shifts and protonation shifts in carbon-13 nuclear magnetic resonance studies of aqueous amines , 1975 .

[16]  J. G. Batchelor 13C protonation shifts: Steric dependence on β-methyl groups , 1977 .

[17]  D. Leyden,et al.  Preconcentration of trace metals using chelating groups immobilized via silylation , 1975 .

[18]  G. R. Hays,et al.  Solid-state silicon-29 and carbon-13 NMR spectroscopy using cross-polarization and magic-angle-spinning techniques to characterize 3-chloropropyl and 3-aminopropyl-modified silica gels , 1985 .

[19]  E. Stejskal,et al.  Removal of artifacts from cross-polarization NMR experiments , 1975 .