Nanoindentation in materials research: Past, present, and future

The method we introduced in 1992 for measuring hardness and elastic modulus by nanoindentation testing has been widely adopted and used in the characterization of mechanical behavior at small scales. Since its original development, the method has undergone numerous refinements and changes brought about by improvements to testing equipment and techniques, as well as advances in our understanding of the mechanics of elastic-plastic contact. In this article, we briefly review the history of the method, comment on its capabilities and limitations, and discuss some of the emerging areas in materials research where it has played, or promises to play, an important role.

[1]  William D. Nix,et al.  A method for interpreting the data from depth-sensing indentation instruments , 1986 .

[2]  David Tabor,et al.  Elastic Recovery of Conical Indentations , 1961 .

[3]  I. N. Sneddon The relation between load and penetration in the axisymmetric boussinesq problem for a punch of arbitrary profile , 1965 .

[4]  Dezba Coughlin,et al.  Nanomechanical properties of calcification, fibrous tissue, and hematoma from atherosclerotic plaques. , 2009, Journal of biomedical materials research. Part A.

[5]  George M. Pharr,et al.  On the generality of the relationship among contact stiffness, contact area, and elastic modulus during indentation , 1992 .

[6]  J. Georges,et al.  Vickers Indentation Curves of Magnesium Oxide (MgO) , 1984 .

[7]  Subra Suresh,et al.  Protection mechanisms of the iron-plated armor of a deep-sea hydrothermal vent gastropod , 2010, Proceedings of the National Academy of Sciences.

[8]  T. Page,et al.  The deformation behavior of ceramic crystals subjected to very low load (nano)indentations , 1992 .

[9]  G. Pharr,et al.  The elastic properties of trabecular and cortical bone tissues are similar: results from two microscopic measurement techniques. , 1999, Journal of biomechanics.

[10]  G. Pharr,et al.  An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments , 1992 .

[11]  Mechanical properties of porous methyl silsesquioxane and nanoclustering silica films using atomic force microscope , 2010 .

[12]  G. Pharr,et al.  Nanoindentation creep of quartz, with implications for rate- and state-variable friction laws relevant to earthquake mechanics , 2004 .

[13]  Felix Riede,et al.  Testing the 'Laacher See hypothesis': tephra as dental abrasive , 2009 .

[14]  W. Oliver,et al.  Hardness measurement at penetration depths as small as 20 nm , 1983 .