Combined Additive and Laser-Induced Processing of Functional Structures for Monitoring under Deformation

This research introduces a readily available and non-chemical combinatorial production approach, known as the laser-induced writing process, to achieve laser-processed conductive graphene traces. The laser-induced graphene (LIG) structure and properties can be improved by adjusting the laser conditions and printing parameters. This method demonstrates the ability of laser-induced graphene (LIG) to overcome the electrothermal issues encountered in electronic devices. To additively process the PEI structures and the laser-induced surface, a high-precision laser nScrypt printer with different power, speed, and printing parameters was used. Raman spectroscopy and scanning electron microscopy analysis revealed similar results for laser-induced graphene morphology and structural chemistry. Significantly, the 3.2 W laser-induced graphene crystalline size (La; 159 nm) is higher than the higher power (4 W; 29 nm) formation due to the surface temperature and oxidation. Under four-point probe electrical property measurements, at a laser power of 3.8 W, the resistivity of the co-processed structure was three orders of magnitude larger. The LIG structure and property improvement are possible by varying the laser conditions and the printing parameters. The lowest gauge factor (GF) found was 17 at 0.5% strain, and the highest GF found was 141.36 at 5%.

[1]  Tarik J. Dickens,et al.  Dynamic bond exchangeable thermoset vitrimers in 3D‐printing , 2022, Journal of Applied Polymer Science.

[2]  Dereje Berihun Sitotaw,et al.  Investigation of Parameters of Fused Deposition Modelling 3D Prints with Compression Properties , 2022, Advances in Materials Science and Engineering.

[3]  Xilun Ding,et al.  Combined extrusion-printed and laser-induced graphene enabled self-sensing composites with a strategic roadmap toward optimization of piezoresistivity , 2021 .

[4]  Md. Saifur Rahman,et al.  One-Step Fabrication of Low-Resistance Conductors on 3D-Printed Structures by Laser-Induced Graphene , 2021, ACS Applied Electronic Materials.

[5]  Xilun Ding,et al.  Multifunctional laser-induced graphene enabled polymeric composites , 2021 .

[6]  Haichang Guo,et al.  Highly Thermally Conductive 3D Printed Graphene Filled Polymer Composites for Scalable Thermal Management Applications. , 2021, ACS nano.

[7]  Tarik J. Dickens,et al.  Thermomechanical Multifunctionality in 3D-Printed Polystyrene-Boron Nitride Nanotubes (BNNT) Composites , 2021, Journal of Composites Science.

[8]  Yiliang Wang,et al.  Fabrication of Smart Components by 3D Printing and Laser-scribing Technologies. , 2019, ACS applied materials & interfaces.

[9]  G. Ding,et al.  Micro Heat Sink Structure with High Thermal Conductive Composite via Micromachining Process , 2019, 2019 20th International Conference on Solid-State Sensors, Actuators and Microsystems & Eurosensors XXXIII (TRANSDUCERS & EUROSENSORS XXXIII).

[10]  K. Al-Ghamdi,et al.  On the Free-Surface Roughness in Incremental Forming of a Sheet Metal: A Study from the Perspective of ISF Strain, Surface Morphology, Post-Forming Properties, and Process Conditions , 2019, Metals.

[11]  Qiu Jiang,et al.  Laser-derived graphene: A three-dimensional printed graphene electrode and its emerging applications , 2019, Nano Today.

[12]  J. Koo,et al.  Laser-Induced Graphene on Additive Manufacturing Parts , 2019, Nanomaterials.

[13]  P. Milani,et al.  Embedding electronics in 3D printed structures by combining fused filament fabrication and supersonic cluster beam deposition , 2018, Additive Manufacturing.

[14]  Cátia Leitão,et al.  Laser‐Induced Graphene Strain Sensors Produced by Ultraviolet Irradiation of Polyimide , 2018, Advanced Functional Materials.

[15]  Lisheng Cheng,et al.  Laser induced graphitization of PAN-based carbon fibers , 2018, RSC advances.

[16]  J. Tour,et al.  Laser-Induced Graphene by Multiple Lasing: Toward Electronics on Cloth, Paper, and Food. , 2018, ACS nano.

[17]  James M Tour,et al.  Laser-Induced Conversion of Teflon into Fluorinated Nanodiamonds or Fluorinated Graphene. , 2018, ACS nano.

[18]  Andrea Ehrmann,et al.  Three-Dimensional (3D) Printing of Polymer-Metal Hybrid Materials by Fused Deposition Modeling , 2017, Materials.

[19]  Stefano Bianco,et al.  All-SPEEK flexible supercapacitor exploiting laser-induced graphenization , 2017 .

[20]  He Tian,et al.  Self-adapted and tunable graphene strain sensors for detecting both subtle and large human motions. , 2017, Nanoscale.

[21]  E. García-Plaza,et al.  Additive manufacturing of PLA structures using fused deposition modelling: Effect of process parameters on mechanical properties and their optimal selection , 2017 .

[22]  Xiaoming Wu,et al.  High-performance graphene-based flexible heater for wearable applications , 2017 .

[23]  N. A. Ochoa,et al.  Improved gas selectivity of polyetherimide membrane by the incorporation of PIM polyimide phase , 2017 .

[24]  Babak Ziaie,et al.  Direct Laser Writing of Porous-Carbon/Silver Nanocomposite for Flexible Electronics. , 2016, ACS applied materials & interfaces.

[25]  J. Tour,et al.  Flexible Boron-Doped Laser-Induced Graphene Microsupercapacitors. , 2015, ACS nano.

[26]  Z. Çıplak,et al.  Investigation of Graphene/Ag Nanocomposites Synthesis Parameters for Two Different Synthesis Methods , 2015 .

[27]  T. Ren,et al.  A Graphene-Based Resistive Pressure Sensor with Record-High Sensitivity in a Wide Pressure Range , 2015, Scientific Reports.

[28]  Babak Ziaie,et al.  Highly stretchable and sensitive unidirectional strain sensor via laser carbonization. , 2015, ACS applied materials & interfaces.

[29]  Guangting Han,et al.  Functionalization of cotton fabric at low graphene nanoplate content for ultrastrong ultraviolet blocking , 2014 .

[30]  J. Tour,et al.  Laser-induced porous graphene films from commercial polymers , 2014, Nature Communications.

[31]  Woo-Gwang Jung,et al.  Facile and safe graphene preparation on solution based platform , 2014 .

[32]  Chee Kai Chua,et al.  3D Printing and Additive Manufacturing: Principles and Applications (with Companion Media Pack) - Fourth Edition of Rapid Prototyping , 2014 .

[33]  H. Wong,et al.  Cost-effective, transfer-free, flexible resistive random access memory using laser-scribed reduced graphene oxide patterning technology. , 2014, Nano letters.

[34]  Sida Luo,et al.  Structure–property–processing relationships of single-wall carbon nanotube thin film piezoresistive sensors , 2013 .

[35]  J. Tour,et al.  Large-area Bernal-stacked bi-, tri-, and tetralayer graphene. , 2012, ACS nano.

[36]  M. El‐Kady,et al.  Laser Scribing of High-Performance and Flexible Graphene-Based Electrochemical Capacitors , 2012, Science.

[37]  Jean-Yves Hascoët,et al.  A new DFM approach to combine machining and additive manufacturing , 2011, ArXiv.

[38]  G. Wallace,et al.  Processable aqueous dispersions of graphene nanosheets. , 2008, Nature nanotechnology.

[39]  Andre K. Geim,et al.  Raman spectrum of graphene and graphene layers. , 2006, Physical review letters.

[40]  D. Chung,et al.  Composite Materials: Functional Materials for Modern Technologies , 2003 .

[41]  Hon Wah Wai,et al.  RP in art and conceptual design , 2001 .

[42]  J. Korvink,et al.  Unraveling the dependency on multiple passes in laser-induced graphene electrodes for supercapacitor and H2O2 sensing , 2021, Materials Science for Energy Technologies.

[43]  Sang‐Woo Kim,et al.  Graphene Tribotronics for Electronic Skin and Touch Screen Applications , 2017, Advanced materials.

[44]  Sida Luo,et al.  Direct laser writing for creating porous graphitic structures and their use for flexible and highly sensitive sensor and sensor arrays , 2016 .

[45]  Sida Luo Processing-structure-property relationships of carbon nanotube and nanoplatelet enabled piezoresistive sensors , 2013 .

[46]  Claus Emmelmann,et al.  Laser Additive Manufacturing and Bionics: Redefining Lightweight Design , 2011 .

[47]  I. Mita,et al.  Molecular aggregation and fluorescence spectra of aromatic polyimides , 1989 .