Home-Made Temperature-Control Unit for the Waters Quanta 4000 Capillary Electrophoresis System

A home-made temperature control unit has been developed for a commercial capillary electrophoresis apparatus, the Waters Quanta 4000. The effect of the unit on the absolute migration times and peak areas of nine β-blockers is described. It was found that this homemade temperature control unit considerably (≥ 100 %) improved the repeatability of the separation.

[1]  M. Riekkola,et al.  Determination of nine β-blockers in serum by micellar electrokinetic capillary chromatography , 1994 .

[2]  M. Riekkola,et al.  Effects of organic mobile phase modifiers on elution and separation of beta-blockers in micellar electrokinetic capillary chromatography. , 1993, Journal of chromatography. A.

[3]  M. Riekkola,et al.  Screening for diuretics in urine and blood serum by capillary zone electrophoresis. , 1993, Journal of chromatography. A.

[4]  M. Riekkola,et al.  Effect of buffer solution pH on the elution and separation of beta-blockers by micellar electrokinetic capillary chromatography. , 1993, Journal of chromatography. A.

[5]  M. Riekkola,et al.  Effect of Temperature, Effective Capillary Length, and Applied Voltage on the Migration of Nine P-Blockers in Micellar Electrokinetic Capillary Chromatography , 1993 .

[6]  M. Riekkola,et al.  Determination of ten β-blockers in urine by micellar electrokinetic capillary chromatography , 1993 .

[7]  S. Petersen,et al.  Effects of capillary temperature control and electrophoretic heterogeneity on parameters characterizing separations of particles by capillary zone electrophoresis , 1992 .

[8]  G. Heo,et al.  Separation of theophylline and its analogues by micellar electrokinetic chromatography: application to the determination of theophylline in human plasma. , 1992, Journal of chromatography.

[9]  E. Yeung,et al.  Temperature programming in capillary zone electrophoresis , 1992 .

[10]  A. Vinther,et al.  Temperature elevations of the sample zone in free solution capillary electrophoresis under stacking conditions , 1991 .

[11]  B. Karger,et al.  Influence of column temperature on the electrophoretic behavior of myoglobin and alpha-lactalbumin in high-performance capillary electrophoresis. , 1991, Analytical chemistry.

[12]  M. Saito,et al.  Influence of temperature control in capillary electrophoresis , 1991 .

[13]  K. Otsuka,et al.  Effects of pH on electrokinetic velocities in micellar electrokinetic chromatography , 1989 .

[14]  S. Terabe Electrokinetic chromatography: An interface between electrophoresis and chromatography , 1989 .

[15]  Eli Grushka,et al.  Effect of temperature gradients on the efficiency of capillary zone electrophoresis separations , 1989 .

[16]  J. Knox Thermal effects and band spreading in capillary electro-separation , 1988 .

[17]  A. Paulus,et al.  Use of peltier thermoelectric devices to control column temperature in high-performance capillary electrophoresis , 1989 .