Note: precision viscosity measurement using suspended microchannel resonators.

We report the characterization of a suspended microchannel resonator (SMR) for viscosity measurements in a low viscosity regime (<10 mPa s) using two measurement schemes. First, the quality factor (Q-factor) of the SMR was characterized with glycerol-water mixtures. The measured Q-factor at 20 °C exhibits a bilinear behavior with the sensitivity of 1281 (mPa s)(-1) for a lower (1-4 mPa s) and 355 (mPa s)(-1) for a higher viscosity range (4-8 mPa s), respectively. The second scheme is the vibration amplitude monitoring of the SMR running in a closed loop feedback. When compared in terms of the measurement time, the amplitude-based measurement takes only 0.1 ~ 1 ms while the Q-factor-based measurement takes ~30 s. However, the viscosity resolution of the Q-factor-based measurement is at least three times better than the amplitude-based measurement. By comparing the Q-factors of heavy water and 9.65 wt.% glycerol-water mixture that have very similar viscosities but different densities, we confirmed that the SMR can measure the dynamic viscosity without the density correction. The obtained results demonstrate that the SMR can measure the fluid viscosity with high precision and even real-time monitoring of the viscosity change is possible with the amplitude-based measurement scheme.

[1]  K. Hane,et al.  Analysis of the resonance characteristics of a cantilever vibrated photothermally in a liquid , 1993 .

[2]  Bruno Mercier,et al.  MEMS sensors for density–viscosity sensing in a low-flow microfluidic environment , 2008 .

[3]  D. Bucknall,et al.  High-shear-rate capillary viscometer for inkjet inks. , 2010, The Review of scientific instruments.

[4]  J. Kister,et al.  The evaluation of cosmetic and pharmaceutical emulsions aging process using classical techniques and a new method: FTIR. , 2005, International journal of pharmaceutics.

[5]  O. Brand,et al.  An iterative curve fitting method for accurate calculation of quality factors in resonators. , 2009, The Review of scientific instruments.

[6]  B. Jakoby,et al.  Evaluation of a vibrating micromachined cantilever sensor for measuring the viscosity of complex organic liquids , 2005 .

[7]  John E Sader,et al.  Nonmonotonic energy dissipation in microfluidic resonators. , 2009, Physical review letters.

[8]  Mark A Burns,et al.  Analysis of non-Newtonian liquids using a microfluidic capillary viscometer. , 2006, Analytical chemistry.

[9]  N. Najafi,et al.  Dynamic and kinematic viscosity measurements with a resonating microtube , 2009 .

[10]  S. Manalis,et al.  Weighing of biomolecules, single cells and single nanoparticles in fluid , 2007, Nature.

[11]  Jungchul Lee,et al.  Measurement uncertainties in resonant characteristics of MEMS resonators , 2013 .

[12]  Sehyun Shin,et al.  Viscosity measurement of non-Newtonian fluid foods with a mass-detecting capillary viscometer , 2003 .