Ion beam sputtering of x-ray multilayer mirrors

Ion beam sputtering has been applied for polishing, figuring and multilayer coating on silicon and quartz glass substrates for the fabrication of x-ray mirrors. For high-performance x-ray optics extremely low microroughnesses of the substrates have to be achieved. Particularly for low d-spacing multilayers (d = 1...2 nm) even small improvements of the surface quality result in significant performance gains of the mirrors. By ion beam polishing silicon substrate surfaces could be smoothed from 0.18 nm rms to 0.11 nm rms (AFM scan length = 5 μm). Furthermore figuring of spherical substrates into elliptical or parabolic surface contours has been developed and applied. Spherical quartz glass substrates with initial rms roughnesses of 0.73 nm and 0.52 nm show reduced roughnesses after figuring and multilayer coating of 0.26 nm and 0.10 nm using AFM scan lengths of 20 μm and 5 μm, respectively. The testing of the ion beam figured mirrors for the application as parallel beam and focussing optics shows very promising results: The comparison of collimating mirrors, produced either by ion beam figuring or bending, shows very similar x-ray intensities. However, the ion beam figured mirrors open the perspective for further reduced figure errors, improved long-term stability and 2-dimensional focusing.

[1]  Katsuhiko Murakami,et al.  Tungsten/Carbon Multilayers Prepared by Ion-Beam Sputtering, , 1992 .

[2]  Torsten Feigl,et al.  Magnetron sputtered EUV mirrors with high-thermal stability , 2000, Advanced Lithography.

[3]  Eric Ziegler,et al.  Design and performance of graded multilayers as focusing elements for x-ray optics , 1999 .

[4]  F. Frost,et al.  Ion beam assisted smoothing of optical surfaces , 2004 .

[5]  Fiona A. Harrison,et al.  X-ray reflectivity and mechanical stress in W/Si multilayers deposited on thin substrates of glass, epoxy-replicated aluminum foil, and Si wafer , 1997, Optics & Photonics.

[6]  Metin Tolan,et al.  X-Ray Scattering from Soft-Matter Thin Films: Materials Science and Basic Research , 1998 .

[7]  H. Takenaka,et al.  Heat resistance of Mo/Si, MoSi2/Si, and Mo5Si3/Si multilayer soft x‐ray mirrors , 1995 .

[8]  A. Kloidt,et al.  Enhancement of the reflectivity of Mo/Si multilayer x‐ray mirrors by thermal treatment , 1991 .

[9]  R. Dietsch,et al.  Application of Ni/C Göbel Mirrors , 2000 .

[10]  Aden B. Meinel,et al.  Controlled Figuring of Optical Surfaces by Energetic Ionic Beams , 1965 .

[11]  Olivier Hignette,et al.  X-ray focusing using elliptically bent multilayers , 1996, Optics & Photonics.

[12]  R. Scholz,et al.  Mo/Si Multilayers with Different Barrier Layers for Applications as Extreme Ultraviolet Mirrors , 2002 .

[13]  T. Barbee,et al.  Molybdenum-silicon multilayer mirrors for the extreme ultraviolet. , 1985, Applied optics.

[14]  Raymond G. Wilson Ionic polishing of fused silica and glass , 1970 .

[15]  Eric Louis,et al.  Interface roughness in Mo/Si multilayers , 2006 .

[16]  Hermann Mai,et al.  Laterally graded multilayer optics for x-ray analysis , 1999, Optics & Photonics.

[17]  E. Spiller,et al.  Smooth multilayer films suitable for x‐ray mirrors , 1979 .

[18]  D. Windt,et al.  Surface finish requirements for soft x-ray mirrors. , 1994, Applied optics.

[19]  J. Kortright,et al.  Focusing x‐rays to a 1 μm spot using elastically bent, graded multilayer‐coated mirrors , 1996 .

[20]  Eberhard Spiller,et al.  High-performance Mo-Si multilayer coatings for extreme-ultraviolet lithography by ion-beam deposition. , 2003, Applied optics.

[21]  Andreas Leson,et al.  Ion-beam sputter deposition of x-ray multilayer optics on large areas , 2006, SPIE Optics + Photonics.

[22]  E. Spiller Low-Loss Reflection Coatings Using Absorbing Materials , 1972 .

[23]  R. Scholz,et al.  High precision large area PLD of X-ray optical multilayers , 1998 .