Predicting Fracture in Micrometer-Scale Polycrystalline Silicon MEMS Structures

Designing reliable MEMS structures presents numerous challenges. Polycrystalline silicon fractures in a brittle manner with considerable variability in measured strength. Furthermore, it is not clear how to use measured tensile strength data to predict the strength of a complex MEMS structure. To address such issues, two recently developed high-throughput MEMS tensile test techniques have been used to estimate strength distribution tails by testing approximately 1500 tensile bars. There is strong evidence that the micromachined polycrystalline silicon that was tested in this paper has a lower bound to its tensile strength (i.e., a strength threshold). Process-induced sidewall flaws appear to be the main source of the variability in tensile strength. Variations in as-fabricated dimensions, stress inhomogeneity within a polycrystal, and variations in the apparent fracture toughness do not appear to be dominant contributors to tensile strength variability. The existence of a strength threshold implies that there is maximum flaw size, which consequently enables a linear elastic fracture mechanics flaw-tolerance analysis. This approach was used to estimate a lower bound for the strength of a double edge-notched specimen that compared favorably with our measured values.

[1]  C. P. Chen,et al.  Fracture toughness of silicon , 1980 .

[2]  Michael S. Baker,et al.  Demonstration of an in situ on-chip tensile tester , 2009 .

[3]  C. Comi,et al.  Mechanical characterization of polysilicon through on-chip tensile tests , 2004, Journal of Microelectromechanical Systems.

[4]  L. Breiman Statistics: with a view toward applications , 1969 .

[5]  E. Reedy Singular Stress Fields at the Intersection of a Grain Boundary and a Stress-Free Edge in a Columnar Polycrystal , 2011 .

[6]  R. Mullen,et al.  The effects of heterogeneity and anisotropy on the size effect in cracked polycrystalline films , 1999 .

[7]  Alan T. Zehnder,et al.  Methyl monolayers improve the fracture strength and durability of silicon nanobeams , 2006 .

[8]  J. Hutchinson,et al.  The influence of plasticity on mixed mode interface toughness , 1993 .

[9]  B. Boyce,et al.  Strength Distributions in Polycrystalline Silicon MEMS , 2007, Journal of Microelectromechanical Systems.

[10]  M. Williams,et al.  Stress Singularities Resulting From Various Boundary Conditions in Angular Corners of Plates in Extension , 1952 .

[11]  A. Saada Elasticity : theory and applications , 1993 .

[12]  O. Tabata,et al.  Specimen size effect on tensile strength of surface-micromachined polycrystalline silicon thin films , 1998 .

[13]  T. Kitamura,et al.  Ab initio study of the surface properties and ideal strength of (100)silicon thin films , 2005 .

[14]  Xiang Chen,et al.  Fracture toughness improvement of austempered high silicon steel by titanium, vanadium and rare earth elements modification , 2007 .

[15]  T. C. T. Ting,et al.  Anisotropic Elasticity: Theory and Applications , 1996 .

[16]  R. C. Picu,et al.  Singularities at Grain Triple Junctions in Two-Dimensional Polycrystals With Cubic and Orthotropic Grains , 1996 .

[17]  B. Boyce A Sequential Tensile Method for Rapid Characterization of Extreme-value Behavior in Microfabricated Materials , 2010 .

[18]  N. H. Macmillan,et al.  The theoretical strength of solids , 1972 .

[19]  M. Umeno,et al.  Crack healing and fracture strength of silicon crystals , 1986 .

[20]  Ioannis Chasiotis,et al.  Description of brittle failure of non-uniform MEMS geometries , 2007 .

[21]  W. Sharpe,et al.  Fracture strength of silicon carbide microspecimens , 2005, Journal of Microelectromechanical Systems.

[22]  Ioannis Chasiotis,et al.  Fracture Toughness and Subcritical Crack Growth in Polycrystalline Silicon , 2006 .

[23]  Stefan Johansson,et al.  In situ tensile strength measurement and Weibull analysis of thick film and thin film micromachined polysilicon structures , 1997 .

[24]  Ioannis Chasiotis,et al.  The mechanical strength of polysilicon films: Part 2. Size effects associated with elliptical and circular perforations , 2003 .

[25]  J. Sniegowski,et al.  IC-Compatible Polysilicon Surface Micromachining , 2000 .