A single-scan method for NMR 2D J-resolved spectroscopy.

A single-scan method is proposed to shorten the acquisition time for an NMR 2D J-resolved spectrum to 1 second. With high SNRs and acceptable resolutions, it constitutes an effective tool for obtaining decoupled proton spectra and fine scalar-coupling splitting patterns.

[1]  Krzysztof Kazimierczuk,et al.  Causality principle in reconstruction of sparse NMR spectra , 2014, Chemical communications.

[2]  R. Fu,et al.  Identifying inter-residue resonances in crowded 2D 13C–13C chemical shift correlation spectra of membrane proteins by solid-state MAS NMR difference spectroscopy , 2013, Journal of Biomolecular NMR.

[3]  Fan Luo,et al.  NASR: an effective approach for simultaneous noise and artifact suppression in NMR spectroscopy. , 2013, Analytical chemistry.

[4]  V. Orekhov,et al.  Analysis of non-uniformly sampled spectra with multi-dimensional decomposition. , 2011, Progress in nuclear magnetic resonance spectroscopy.

[5]  Xu Zhang,et al.  Gridding and fast Fourier transformation on non-uniformly sparse sampled multidimensional NMR data. , 2010, Journal of magnetic resonance.

[6]  Y. Choi,et al.  NMR-based metabolomic analysis of plants , 2010, Nature Protocols.

[7]  Mark R Viant,et al.  Two-dimensional J-resolved NMR spectroscopy: review of a key methodology in the metabolomics toolbox. , 2010, Phytochemical analysis : PCA.

[8]  Daniel J. Hibbard,et al.  High resolution heteronuclear correlation NMR spectroscopy of an antimicrobial peptide in aligned lipid bilayers: peptide-water interactions at the water-bilayer interface. , 2009, Journal of the American Chemical Society.

[9]  S. Akoka,et al.  Resolution and sensitivity aspects of ultrafast J-resolved 2D NMR spectra. , 2008, Journal of magnetic resonance.

[10]  J. Keeler,et al.  Two-dimensional J-spectra with absorption-mode lineshapes. , 2007, Journal of magnetic resonance.

[11]  C. Legein,et al.  Accurate heteronuclear J-coupling measurements in dilute spin systems using the multiple-quantum filtered J-resolved experiment. , 2007, Chemical communications.

[12]  Patrick Giraudeau,et al.  A new detection scheme for ultrafast 2D J-resolved spectroscopy. , 2007, Journal of magnetic resonance.

[13]  Blaise deB. Frederick,et al.  Grey and white matter GABA level differences in the human brain using two‐dimensional, J‐resolved spectroscopic imaging , 2005, NMR in biomedicine.

[14]  P. Renshaw,et al.  Two‐dimensional, J‐resolved spectroscopic imaging of GABA at 4 Tesla in the human brain , 2005, Magnetic resonance in medicine.

[15]  M. Nilsson,et al.  Improving pulse sequences for 3D diffusion-ordered NMR spectroscopy: 2DJ-IDOSY. , 2004, Analytical chemistry.

[16]  Ray Freeman,et al.  Projection-reconstruction technique for speeding up multidimensional NMR spectroscopy. , 2004, Journal of the American Chemical Society.

[17]  R. Freeman,et al.  Hadamard NMR Spectroscopy , 2003 .

[18]  Lucio Frydman,et al.  The acquisition of multidimensional NMR spectra within a single scan , 2002, Proceedings of the National Academy of Sciences of the United States of America.

[19]  V. Mandelshtam FDM: The Filter Diagonalization Method for Data Processing in NMR Experiments , 2001 .

[20]  R. Bartlett,et al.  NMR Spin−Spin Coupling Constants for Hydrogen Bonds of [F(HF)n]-, n = 1−4, Clusters , 2000 .

[21]  Henrik Gesmar,et al.  Application of the Linear Prediction Method to NMR Spectroscopy , 1991 .

[22]  A. Bax,et al.  A simple method for suppressing dispersion-mode contributions in NMR spectra: The “pseudo echo” , 1981 .

[23]  Richard R. Ernst,et al.  Homonuclear broad band decoupling and two-dimensional J-resolved NMR spectroscopy , 1976 .