Selective laser melting of AlSi10Mg: Influence of post-processing on the microstructural and tensile properties development

Abstract The study looks into the impact of thermal post-processing using Hot Isostatic Pressing (HIPping) and/or T6-peak aging treatment, post-process machining, as well as the build orientation on the microstructural and mechanical properties development in AlSi10Mg alloy fabricated using Selective Laser Melting (SLM). The builds contained fine columnar grains, with a fine Si-enriched cellular dendritic network, resulting in tensile strengths exceeding the castings. To elucidate the as-fabricated microstructure and strength, thermal modelling was employed, predicting cooling rates of 105–106 °C/s. Voids, mostly due to oxide films, were observed using Micro-CT in the as-fabricated condition. HIPping collapsed most voids, showing virtually no trace even after a further T6 treatment. Generally, the tensile properties of the majority of conditions were significantly better than in the cast + T6 equivalent alloy. Post-process machining was also found to improve the strength (compared to the as-fabricated surface). However, HIPping + T6 allowed the builds to achieve the required tensile properties, without surface machining. By assessing the influence of powder recycling, it was found that the void content linked to oxide layer formation increased following powder recycling, resulting in a drop in tensile properties. The interaction between the microstructure, surface condition, thermal post-processing, and fracture mode is discussed.

[1]  Ma Qian,et al.  Effect of Powder Reuse Times on Additive Manufacturing of Ti-6Al-4V by Selective Electron Beam Melting , 2015 .

[2]  J. Kruth,et al.  Fine-structured aluminium products with controllable texture by selective laser melting of pre-alloyed AlSi10Mg powder , 2013 .

[3]  E. Brandl,et al.  Additive manufactured AlSi10Mg samples using Selective Laser Melting (SLM): Microstructure, high cycle fatigue, and fracture behavior , 2012 .

[4]  E. Sjölander,et al.  The heat treatment of Al–Si–Cu–Mg casting alloys , 2010 .

[5]  Y. Birol AlB3 master alloy to grain refine AlSi10Mg and AlSi12Cu aluminium foundry alloys , 2012 .

[6]  A. Rubenchik,et al.  Laser powder-bed fusion additive manufacturing: Physics of complex melt flow and formation mechanisms of pores, spatter, and denudation zones , 2015, 1512.02593.

[7]  Moataz M. Attallah,et al.  Microstructural control during direct laser deposition of a β-titanium alloy , 2015 .

[8]  J. Kruth,et al.  Mechanical Properties of AlSi10Mg Produced by Selective Laser Melting , 2012 .

[9]  J. Kruth,et al.  A study of the microstructural evolution during selective laser melting of Ti–6Al–4V , 2010 .

[10]  David W. Rosen,et al.  Additive Manufacturing Technologies: Rapid Prototyping to Direct Digital Manufacturing , 2009 .

[11]  Claus Emmelmann,et al.  Investigation of Aging Processes of Ti-6Al-4 V Powder Material in Laser Melting , 2012 .

[12]  K. Kunze,et al.  Texture, anisotropy in microstructure and mechanical properties of IN738LC alloy processed by selective laser melting (SLM) , 2015 .

[13]  E. Sjölander,et al.  Artificial ageing of Al–Si–Cu–Mg casting alloys , 2011 .

[14]  P. Alvarez,et al.  Effect of IN718 Recycled Powder Reuse on Properties of Parts Manufactured by Means of Selective Laser Melting , 2014 .

[15]  Wei Wang,et al.  Selective laser melting of AlSi10Mg alloy: Process optimisation and mechanical properties development , 2015, Materials & Design (1980-2015).

[16]  Q. Wang,et al.  The effect of hot isostatic pressing on the microstructure and tensile properties of an unmodified A356-T6 cast aluminum alloy , 2006 .

[17]  E. Lee,et al.  The effect of hot isostatic pressing on cast aluminum , 1997 .

[18]  R. Chou,et al.  Additive Manufacturing of Al-12Si Alloy Via Pulsed Selective Laser Melting , 2015 .

[19]  Nachum Frage,et al.  Microstructure and Mechanical Properties of AlSi10Mg Parts Produced by the Laser Beam Additive Manufacturing (AM) Technology , 2014, Metallography, Microstructure, and Analysis.

[20]  K. E. Nilsen,et al.  Assessment of different techniques for quantification of α-Al(FeMn)Si and β-AlFeSi intermetallics in AA 6xxx alloys , 2002 .

[21]  Moataz M. Attallah,et al.  The influence of the laser scan strategy on grain structure and cracking behaviour in SLM powder-bed fabricated nickel superalloy , 2014 .

[22]  A. Zaldívar-Cadena,et al.  Addition of iron for the removal of the β-AlFeSi intermetallic by refining of α-AlFeSi phase in an Al–7.5Si–3.6Cu alloy , 2010 .