Synthesis of Tin-Containing Heterocyclic Compounds by the Reaction of 1,3,5,2,4,6-Trichalcogenatristannin with 1,3-Dipoles
暂无分享,去创建一个
Reaction of 1,3,5,2,4,6-trithiatristannin with 2,4,6-tri-t-butylbenzonitrile oxide gave the 1,3,5,2-oxathiazastannole quantitatively. Reaction of 1,3,2,4-dithiadistannetane with 2,4,6-tri-t-butylbenzonitrile oxide also quantitatively but slowly afforded the 1,3,5,2-oxathiazastannole. Reaction of 1,3,5,2,4,6-triselenatristannin with 2,4,6-tri-t-butylbenzonitrile oxide gave 1,3,5,2-oxaselenazastannole. The thermal behavior of the oxaselenazastannole was unusual.
[1] N. Tokitoh,et al. Synthesis and reactions of stanneneselone , 1995 .
[2] R. Hundt,et al. Structure of the First Four‐Membered Cyclic Diorganyltin Chalcogenides , 1977 .
[3] N. Sugiyama,et al. Photochemical Reactions of Some Thiocarbonyl Trimers , 1973 .