Fast Synchrotron X‐Ray Tomography of Dynamic Processes in Liquid Aluminium Alloy Foam  

Series of fast synchrotron X-ray tomographies are taken continuously at a rate of up to 5 Hz, while aluminium alloy precursors are foamed in an X-ray transparent setup for several minutes using infra-red (IR) lasers for heating. The entire foaming process from the solid precursor to the expanded liquid foam is captured. The analysis of the sequence of tomographies is done with an emphasis on nucleation and bubble growth. In early stages of foaming, bubble and crack formation and evolution are observed. We analyze the nucleation stage and obtain quantitative results for the number of nucleation centers and their distribution and derive the nucleation rate as a function of time.

[1]  John Banhart,et al.  On the Road Again: Metal Foams Find Favor , 2002 .

[2]  A. Rack,et al.  Synchrotron-based radioscopy employing spatio-temporal micro-resolution for studying fast phenomena in liquid metal foams , 2009, Journal of synchrotron radiation.

[3]  R. Flumerfelt,et al.  Bubble size distributions in freely expanded polymer foams , 1997 .

[4]  V. Gergely,et al.  The FORMGRIP Process: Foaming of Reinforced Metals by Gas Release in Precursors , 2000 .

[5]  John Banhart,et al.  Viewing the early stage of metal foam formation by computed tomography using synchrotron radiation , 2002 .

[6]  J. Banhart,et al.  Kinetics of coalescence in liquid aluminium foams , 2011 .

[7]  E. Solórzano,et al.  Early anisotropic expansion of aluminium foam precursors , 2013, Journal of Materials Science.

[8]  J. Banhart,et al.  White-beam X-ray radioscopy and tomography with simultaneous diffraction at the EDDI beamline. , 2013, Journal of synchrotron radiation.

[9]  Andreas Mortensen,et al.  20 Hz X-ray tomography during an in situ tensile test , 2016, International Journal of Fracture.

[10]  Marco Stampanoni,et al.  Quantitative 3D characterization of cellular materials: Segmentation and morphology of foam , 2012 .

[11]  M. Amon,et al.  A study of the dynamics of foam growth: Analysis of the growth of closely spaced spherical bubbles , 1984 .

[12]  P. Withers,et al.  Quantitative X-ray tomography , 2014 .

[13]  J. Banhart,et al.  Al and Zn Foams Blown by an Intrinsic Gas Source , 2010 .

[14]  Jiansheng Lu,et al.  Bubble Nucleation of PM Al-9Si Foam , 2011 .

[15]  J. Banhart,et al.  Fatigue of a laterally constrained closed cell aluminum foam , 2008 .

[16]  F. García‐Moreno Commercial Applications of Metal Foams: Their Properties and Production , 2016, Materials.

[17]  J. Banhart,et al.  Real‐time X‐ray Radioscopy on Metallic Foams Using a Compact Micro‐Focus Source , 2004 .

[18]  John Banhart,et al.  Early pore formation in aluminium foams studied by synchrotron-based microtomography and 3-D image analysis , 2009 .

[19]  John Banhart,et al.  Why are metal foams stable , 2006 .

[20]  Holger G. Krapp,et al.  Four-dimensional in vivo X-ray microscopy with projection-guided gating , 2015, Scientific Reports.

[21]  P. Cloetens,et al.  Investigation of pore initiation in metal foams by synchrotron-radiation tomography , 2005 .

[22]  A. Saint-Jalmes,et al.  Physical chemistry in foam drainage and coarsening. , 2006, Soft matter.

[23]  A. Mehra,et al.  Modeling nucleation and growth of bubbles during foaming of molten aluminum with high initial gas supersaturation , 2014 .

[24]  J. Banhart,et al.  Particle-stabilised foams: structure and aging , 2011 .