Scanning transmission X-ray microscopy with a fast framing pixel detector.

Scanning transmission X-ray microscopy (STXM) is a powerful imaging technique, in which a small X-ray probe is raster scanned across a specimen. Complete knowledge of the complex-valued transmission function of the specimen can be gained using detection schemes whose every-day use, however, is often hindered by the need of specialized configured detectors or by slow or noisy readout of area detectors. We report on sub-50 nm-resolution STXM studies in the hard X-ray regime using the PILATUS, a fully pixelated fast framing detector operated in single-photon counting mode. We demonstrate a range of imaging modes, including phase contrast and dark-field imaging.

[1]  P. Charalambous,et al.  TwinMic : A European Twin X-ray Microscopy Station Commissioned at ELETTRA , 2006 .

[2]  P W Hawkes,et al.  Half-plane apertures in TEM, split detectors in STEM and psychography , 1978 .

[3]  Chris Jacobsen,et al.  Integrating Silicon detector with segmentation for scanning transmission X-ray microscopy , 2006 .

[4]  Franz Pfeiffer,et al.  Fabrication of Fresnel zone plates for hard X-rays , 2007 .

[5]  J. M. Cowley Configured detectors for STEM imaging of thin specimens , 1993 .

[6]  M. D. de Jonge,et al.  Quantitative phase imaging with a scanning transmission x-ray microscope. , 2008, Physical Review Letters.

[7]  S. Wilkins,et al.  X‐ray omni microscopy , 2004, Journal of microscopy.

[8]  B. Schmitt,et al.  Performance of single-photon-counting PILATUS detector modules , 2009, Journal of synchrotron radiation.

[9]  O. Bunk,et al.  High-Resolution Scanning X-ray Diffraction Microscopy , 2008, Science.

[10]  Graeme Morrison,et al.  Dark-field imaging with the scanning transmission x-ray microscope , 1992 .

[11]  G. Schmahl,et al.  X-ray microscopy and spectromicroscopy , 1998 .

[12]  M R Arnison,et al.  Linear phase imaging using differential interference contrast microscopy , 2004, Journal of microscopy.

[13]  A. G. Cullis,et al.  Hard-x-ray lensless imaging of extended objects. , 2007, Physical review letters.

[14]  Graeme Morrison,et al.  STXM imaging with a configured detector , 2003 .

[15]  H N Chapman,et al.  Dark field X-ray microscopy: the effects of condenser/detector aperture. , 2001, Ultramicroscopy.

[16]  Franz Pfeiffer,et al.  Multimodal x-ray scatter imaging , 2009 .

[17]  B. Niemann,et al.  Differential Phase Contrast X-Ray Microscopy , 1998 .

[18]  C. David,et al.  Zone-doubling technique to produce ultrahigh-resolution x-ray optics. , 2007, Physical review letters.

[19]  O. Bunk,et al.  A two-directional approach for grating based differential phase contrast imaging using hard x-rays. , 2007, Optics express.

[20]  C. Jacobsen,et al.  SCANNING TRANSMISSION X-RAY MICROSCOPY WITH A SEGMENTED DETECTOR , 2003 .

[21]  J. Rodenburg,et al.  A phase retrieval algorithm for shifting illumination , 2004 .

[22]  William H. Press,et al.  Numerical recipes in C , 2002 .

[23]  O. Bunk,et al.  Contrast mechanisms in scanning transmission x-ray microscopy , 2009 .