Magnetic resonance imaging of liquid flow and pore structure within packed beds

Magnetic resonance imaging (MRI) volume- and velocity-measurement techniques are used to probe structure-flow correlations within the interparticle space of a packed bed of ballotini. Images of the three mutually orthogonal components of the velocity field are obtained in two perpendicular slices within a bed of 5 mm diameter ballotini packed within a glass column of internal diameter 4.6 cm. Comparison of flow images obtained for two beds of identical column-to-particle diameter ratio but of differing length show that velocity enhancements at the walls of the bed are greater in the shorter, more ordered, bed. A three-dimensional volume image of each bed is also obtained and analysed to partition the interparticle space into individual pores and determine the location of pore necks. Correlations between volume flow rate and the surface area of the constrictions (pore necks) within the interparticle space lie between two limiting behaviours. For pores associated with low local Reynolds number, the volume flow rate through the constrictions scales as the square of the cross-sectional area of the constriction, whereas at the extreme of high local Reynolds number pores show volume flow rates scaling with cross-sectional area.

[1]  F. Dullien Porous Media: Fluid Transport and Pore Structure , 1979 .

[2]  Numerical analysis of near—wall channelling in a packed bed , 1995 .

[3]  L. E. Scriven,et al.  NMR imaging of velocity profiles and velocity distributions in bead packs , 1996 .

[4]  P. Callaghan Principles of Nuclear Magnetic Resonance Microscopy , 1991 .

[5]  J. Lumley,et al.  Fluid Dynamics for Physicists , 1996 .

[6]  P. Callaghan,et al.  Velocity and diffusion imaging in dynamic NMR microscopy , 1991 .

[7]  P. Cheng,et al.  Transverse thermal dispersion and wall channelling in a packed bed with forced convective flow , 1988 .

[8]  Lynn F. Gladden,et al.  Applications of nuclear magnetic resonance imaging in process engineering , 1996 .

[9]  Lynn F. Gladden,et al.  Nuclear magnetic resonance in chemical engineering: Principles and applications , 1994 .

[10]  G. Nesbitt,et al.  Towards validation of porous media models using NMR imaging and image-analysis techniques , 1991 .

[11]  Ajit P. Yoganathan,et al.  Experimental studies of model porous media fluid dynamics , 1989 .

[12]  P. J. Moss,et al.  Fluid Mechanics and Transfer Processes , 1985 .

[13]  J. Pope,et al.  Quantitative magnetic resonance flow and diffusion imaging in porous media. , 1995, Magnetic resonance imaging.

[14]  Pierre M. Adler,et al.  Measurement of two-dimensional velocity fields in porous media by particle image displacement velocimetry , 1992 .

[15]  C. A. Baldwin,et al.  Determination and Characterization of the Structure of a Pore Space from 3D Volume Images , 1996 .