An ultra-high temperature testing instrument under oxidation environment up to 1800 °C.

A new testing instrument was developed to measure the high-temperature constitutive relation and strength of materials under an oxidative environment up to 1800 °C. A high temperature electric resistance furnace was designed to provide a uniform temperature environment for the mechanical testing, and the temperature could vary from room temperature (RT) to 1800 °C. A set of semi-connected grips was designed to reduce the stress. The deformation of the specimen gauge section was measured by a high temperature extensometer. The measured results were acceptable compared with the results from the strain gauge method. Meanwhile, tensile testing of alumina was carried out at RT and 800 °C, and the specimens showed brittle fracture as expected. The obtained Young's modulus was in agreement with the reported value. In addition, tensile experiment of ZrB2-20%SiC ceramic was conducted at 1700 °C and the high-temperature tensile stress-strain curve was first obtained. Large plastic deformation up to 0.46% and the necking phenomenon were observed before the fracture of specimen. This instrument will provide a powerful research tool to study the high temperature mechanical property of materials under oxidation and is benefit for the engineering application of materials in aerospace field.

[1]  Guo‐Jun Zhang,et al.  Changed oxidation behavior of ZrB2–SiC ceramics with the addition of ZrC , 2015 .

[2]  William E Lee,et al.  Effect of La2O3 addition on long-term oxidation kinetics of ZrB2-SiC and HfB2-SiC ultra-high temperature ceramics , 2014 .

[3]  William E Lee,et al.  Thermal properties of La2O3-doped ZrB2- and HfB2-based ultra-high temperature ceramics , 2013 .

[4]  Yuan Tian,et al.  Evaluation of Impact Bending Strength of Ceramic Composites at Ultra-High Temperatures from 1500-2000 °C in Air , 2013 .

[5]  W. Mao,et al.  Nanoindentation Study of Pop-in Phenomenon Characteristics and Mechanical Properties of Sapphire (101¯2) Crystal , 2012 .

[6]  R. Savino,et al.  ZrB2 – SiC Sharp Leading Edges in High Enthalpy Supersonic Flows , 2012 .

[7]  T. Detzel,et al.  Novel temperature dependent tensile test of freestanding copper thin film structures. , 2012, The Review of scientific instruments.

[8]  Raffaele Savino,et al.  Plasma wind tunnel testing of ultra-high temperature ZrB2-SiC composites under hypersonic re-entry conditions , 2010 .

[9]  Andrei Kotousov,et al.  Induction heating apparatus for high temperature testing of thermo-mechanical properties , 2009 .

[10]  C. Hong,et al.  Ablation behavior of ZrB2–SiC–ZrO2 ceramic composites by means of the oxyacetylene torch , 2009 .

[11]  Fernando Guiberteau,et al.  Effect of temperature on the pre-creep mechanical properties of silicon nitride , 2009 .

[12]  J. Zaykoski,et al.  Flexural Creep Deformation of ZrB2/SiC Ceramics in Oxidizing Atmosphere , 2008 .

[13]  Y. Bao,et al.  Mechanical Properties Evaluation of Ultra-High Temperature Ceramics , 2008 .

[14]  S. Hardy,et al.  A new model for the time-dependent behaviour of polycrystalline ceramic materials with metallic inter-granular layers under tension , 2006 .

[15]  A. Bellosi,et al.  Development and characterization of metal-diboride-based composites toughened with ultra-fine SiC particulates , 2005 .

[16]  D. Munz,et al.  Differences in Tensile and Bending Strength for Knoop‐Cracked Lead Zirconate Titanate Specimens , 2004 .

[17]  R. Völkl,et al.  Mechanical testing of ultra-high temperature alloys , 2004 .

[18]  Mahen Mahendran,et al.  Mechanical Properties of Light Gauge Steels at Elevated Temperatures , 2003 .

[19]  B. Zagar,et al.  Noncontacting strain measurements at high temperatures by the digital laser speckle technique , 2000 .

[20]  Theo Fett,et al.  Determination of Room-temperature Tensile Creep of PZT , 1998 .

[21]  Theo Fett,et al.  Deformation and strength behavior of a soft PZT ceramic , 1998, Smart Structures.

[22]  M. G. Castelli,et al.  Comparison testings between two high-temperature strain measurement systems , 1996 .

[23]  Richard O. Claus,et al.  High-temperature fiber optic strain sensors in fatigue-loading conditions , 1996, Smart Structures and Materials + Nondestructive Evaluation and Health Monitoring.

[24]  S. Nasu,et al.  High-Temperature Creep of Pure Platinum , 1996 .

[25]  M. Sutton,et al.  High-temperature deformation measurements using digital-image correlation , 1996 .

[26]  J. Holmes A Technique for Tensile Fatigue and Creep Testing of Fiber-Reinforced Ceramics , 1992 .

[27]  E. Lara‐Curzio,et al.  A high-temperature fibre testing facility , 1991 .

[28]  D. E. Roberts,et al.  Technique for Tensile Creep Testing of Ceramics , 1989 .

[29]  David J. Quesnel,et al.  Extensometer extender for conversion of room‐temperature extensometers for high‐temperature applications , 1983 .

[30]  L. F. Sturgeon,et al.  The use of interrupted resistance heating to perform elevated temperature tensile tests , 1974 .

[31]  J. B. Wachtman,et al.  Strength of Synthetic Single Crystal Sapphire and Ruby as a Function of Temperature and Orientation , 1959 .

[32]  William G. Fahrenholtz,et al.  Strength of Zirconium Diboride to 2300°C , 2013 .

[33]  †. J.J.Meléndez-Martínez,et al.  Temperature dependence of mechanical properties of alumina up to the onset of creep , 2007 .

[34]  R. Savino,et al.  Stability of ultra-high-temperature ZrB2–SiC ceramics under simulated atmospheric re-entry conditions , 2007 .

[35]  William G. Fahrenholtz,et al.  Thermodynamic Analysis of ZrB2–SiC Oxidation: Formation of a SiC‐Depleted Region , 2007 .

[36]  Bernd Fischer,et al.  Economical Creep Testing of Ultrahigh-temperature Alloys , 2003 .