Quantitative Phase Analysis for Carbide Characterization in Steel Using Automated Electron Diffraction

Carbides are critical to many different properties in a steel. In this paper, the quantification of a carbide powder extracted from a stainless steel analyzed with profile refinement of X-ray powde ...

[1]  Yefei Li,et al.  Microstructure and crystallography of M7C3 carbide in chromium cast iron , 2015 .

[2]  D. Bish,et al.  Quantitative phase analysis using the Rietveld method , 1988 .

[3]  T. Lwin,et al.  Outcomes of the International Union of Crystallography Commission on Powder Diffraction Round Robin on Quantitative Phase Analysis: samples 1a to 1h , 2001 .

[4]  P. Luksch,et al.  New developments in the Inorganic Crystal Structure Database (ICSD): accessibility in support of materials research and design. , 2002, Acta crystallographica. Section B, Structural science.

[5]  Yimin Gao,et al.  The electronic, mechanical properties and theoretical hardness of chromium carbides by first-principles calculations , 2011 .

[6]  Sven Hovmöller,et al.  Three-dimensional electron diffraction as a complementary technique to powder X-ray diffraction for phase identification and structure solution of powders , 2015, IUCrJ.

[7]  International Centre for Diffraction Data round robin on quantitative Rietveld phase analysis of pharmaceuticals , 2010, Powder Diffraction.

[8]  M. Sluiter,et al.  Formation, structure and magnetism of the γ-(Fe,M)23C6 (M = Cr, Ni) phases: A first-principles study , 2016 .

[9]  Alan A. Coelho,et al.  TOPAS and TOPAS-Academic: an optimization program integrating computer algebra and crystallographic objects written in C++ , 2018 .

[10]  H. Yakel Atom distributions in tau‐carbide phases: Fe and Cr distributions in (Cr23−xFex)C6 with x = 0, 0·74, 1·70, 4·13 and 7·36 , 1987 .

[11]  E. F. Rauch,et al.  Rapid Diffraction Patterns identification through template matching , 2005 .

[12]  Á. G. Torre,et al.  Round robin on Rietveld quantitative phase analysis of Portland cements , 2009 .

[13]  Stef Smeets,et al.  Serial electron crystallography for structure determination and phase analysis of nanocrystalline materials , 2018, Journal of applied crystallography.

[14]  Ye-hua Jiang,et al.  Mechanical properties and electronic structures of M23C6 (M = Fe, Cr, Mn)-type multicomponent carbides , 2015 .

[15]  H. Rietveld,et al.  The structure of some alkaline‐earth metal uranates , 1969 .

[16]  M. Raven,et al.  Application of the Rietveld Refinement Procedure in Assaying Powdered Mixtures , 1988, Powder Diffraction.

[17]  H. Henein,et al.  Matrix Dissolution Techniques Applied to Extract and Quantify Precipitates from a Microalloyed Steel , 2011 .