Fabrication of Al7075–Al_2O_3np-based metal matrix composites with a high solid fraction for thixoforming

For thixoforming, it is necessary to have a good microstructure of fine, uniform, and globular grains in a semisolid range. In this study, the nano-Al_2O_3(Al_2O_3np)/Al7075 composites with a high solid fraction were fabricated by specially made Al_2O_3np containing Mg powders and semisolid ultrasonic vibration (SSUV) process. The influence of SSUV technology on primary α-Al grain and second phase in the composites was investigated. Microstructural studies revealed that a good semisolid slurry with an average grain size of 73 μm, a shape factor of 0.84, and a solid fraction of 0.715 could be obtained. Also, it could be shown that SSUV affected largely the size and type of the second phase as well as growth and nucleation of the primary α-Al grain. TEM analysis revealed that there are well-defined crystallographic orientation relationships between the second phases and α-Al, suggesting enhanced heterogeneous nucleation in Al7075 alloys. Moreover, mechanisms involved in the development of microstructure were discussed.

[1]  Bin Liu,et al.  Constitutive behavior of AZ80 M magnesium alloy compressed at elevated temperature and containing a small fraction of liquid , 2018, Vacuum.

[2]  W. Peng,et al.  Al alloy metal matrix composites reinforced by WS2 inorganic nanomaterials , 2018 .

[3]  Hong Yan,et al.  Constitutive behavior of Al 2 O 3np /Al7075 composites with a high solid fraction for thixoforming , 2017 .

[4]  S. Sanjabi,et al.  Synthesis and characterization of nanocrystalline MgAl2O4 spinel via modified sol–gel method , 2015 .

[5]  Hong Yan,et al.  Fabrication of nanosized Al_2O_3 reinforced aluminum matrix composites by subtype multifrequency ultrasonic vibration , 2015 .

[6]  A. J. Knowles,et al.  Microstructure and mechanical properties of 6061 Al alloy based composites with SiC nanoparticles , 2014 .

[7]  H. Atkinson,et al.  Microstructural coarsening of 7005 aluminum alloy semisolid billets with high solid fraction , 2014 .

[8]  Hong Yan,et al.  Morphological evolution of semi-solid Mg2Si/AM60 magnesium matrix composite produced by ultrasonic vibration process , 2014 .

[9]  P. An,et al.  Microstructure and mechanical properties of rheo-diecast hypereutectic Al–Si alloy with 2%Fe assisted with ultrasonic vibration process , 2013 .

[10]  Ping An,et al.  Microstructure and property of rheocasting aluminum-alloy made with indirect ultrasonic vibration process , 2012 .

[11]  W. Gao,et al.  Processing, microstructure and tensile properties of nano-sized Al2O3 particle reinforced aluminum matrix composites , 2012 .

[12]  N. Haghdadi,et al.  Microstructure evolution and mechanical properties of backward thixoextruded 7075 aluminum alloy , 2012 .

[13]  R. Chaim Grain coalescence by grain rotation in nano-ceramics , 2012 .

[14]  Weidong Huang,et al.  Effect of ultrasonic vibration on microstructural evolution of the reinforcements and degassing of in situ TiB2p/Al-12Si-4Cu composites , 2012 .

[15]  P. Rohatgi,et al.  Microstructure and hardness of Al2O3 nanoparticle reinforced Al–Mg composites fabricated by reactive wetting and stir mixing , 2011 .

[16]  Y. Birol Thixoforming of EN AW-2014 alloy at high solid fraction , 2011 .

[17]  C. Kang,et al.  Study on the effects of the compression ratio and mushy zone heating on the thixotropic microstructure of AA 7075 aluminum alloy via SIMA process , 2011 .

[18]  A. Bolouri,et al.  Microstructural evolution during semisolid state strain induced melt activation process of aluminum 7075 alloy , 2010 .

[19]  H. Saghafian,et al.  Study on the effect of prolonged mechanical vibration on the grain refinement and density of A356 aluminum alloy , 2009 .

[20]  M. Nili-Ahmadabadi,et al.  Semi-solid microstructure evolution during reheating of aluminum A356 alloy deformed severely by ECAP , 2008 .

[21]  H. Schuchmann,et al.  Influence of hydrostatic pressure and sound amplitude on the ultrasound induced dispersion and de-agglomeration of nanoparticles. , 2008, Ultrasonics sonochemistry.

[22]  S. E. Offerman,et al.  Nucleation kinetics during the solidification of aluminum alloys , 2007 .

[23]  R. Pérez,et al.  Morphological characteristics of the rapidly and conventionally solidified alloys of the AlCuFe system , 2007 .

[24]  Q. Zhai,et al.  Effects of power ultrasonic treatment on microstructure and mechanical properties of T10 steel , 2007 .

[25]  W. Zhou,et al.  Semisolid microstructure of Mg2Si/Al composite by cooling slope cast and its evolution during partial remelting process , 2007 .

[26]  Q. Meng,et al.  The microstructural evolution of an Al–Zn–Mg–Cu alloy during homogenization , 2006 .

[27]  Y. Chang,et al.  Diffusion coefficients of some solutes in fcc and liquid Al: critical evaluation and correlation , 2003 .

[28]  H. Atkinson,et al.  Microstructural evolution and tensile mechanical properties of thixoformed high performance aluminium alloys , 2003 .

[29]  G. Lu,et al.  Liquidus semi-continuous casting, reheating and thixoforming of a wrought aluminum alloy 7075 , 2003 .

[30]  Patrick S. Grant,et al.  Isothermal grain coarsening of spray formed alloys in the semi-solid state , 2002 .

[31]  Jiehan Wang,et al.  Thixoforming of spray-formed 6066Al/SiCp composites , 2001 .

[32]  G. Éskin Broad prospects for commercial application of the ultrasonic (cavitation) melt treatment of light alloys. , 2001, Ultrasonics sonochemistry.

[33]  Shouxun Ji,et al.  Semi-solid Processing of Engineering Alloys by a Twin-screw Rheomoulding Process , 2001 .

[34]  Mats Johnson,et al.  Thermal Expansion of Al and TiB2 in the Temperature Range 300 to 900 K and Calculated Lattice Fit at the Melting Temperature for Al , 1998 .

[35]  Ho-In Lee,et al.  Microstructure of stir-cast metals , 1984 .

[36]  B. L. Bramfitt The effect of carbide and nitride additions on the heterogeneous nucleation behavior of liquid iron , 1970, Metallurgical and Materials Transactions B.

[37]  D. Kirkwood Semisolid metal processing , 1994 .