Toward a further understanding of size effects in the torsion of thin metal wires: An experimental and theoretical assessment

Abstract Both torsion and tensile tests are performed on polycrystalline copper wires with diameters in the range 20–50 μm. A significant size effect in both the initial yielding and the plastic flow is observed in torsion. In contrast, only a minor effect is seen in tension. The physical basis of the size effects in wire torsion is elucidated in the light of the geometrically necessary dislocation argument and of the critical thickness effect. Three phenomenological theories of strain gradient plasticity, due to Fleck and Hutchinson, to Chen and Wang and to Aifantis and co-workers, are assessed within the context of wire torsion, and the corresponding rigid-plastic solutions are derived. Distinctions between the theories are highlighted through comparison with experiment, emphasizing the difference in predicted trends in the size dependence of initial yielding and of hardening rate. Additionally, the key aspects of a new torsion balance technique for wire torsion are presented. An in-situ torsional vibration method for calibrating the torque meter with precision is addressed. The systematic experimental and theoretical assessment suggests that the size effect in the initial yielding is mainly due to the constraints that the external geometrical size put on a finite strained volume, while the size dependence in the plastic flow is principally owing to the geometrically necessary dislocations associated with the plastic strain gradients.

[1]  Dierk Raabe,et al.  Mechanical and microstructural single-crystal Bauschinger effects: Observation of reversible plasticity in copper during bending , 2010 .

[2]  George Z. Voyiadjis,et al.  Gradient plasticity theory with a variable length scale parameter , 2005 .

[3]  M. Saif,et al.  Strain gradient effect in nanoscale thin films , 2003 .

[4]  M. Ashby The deformation of plastically non-homogeneous materials , 1970 .

[5]  George Z. Voyiadjis,et al.  A physically based gradient plasticity theory , 2006 .

[6]  Amit Acharya,et al.  On Non-Local Flow Theories that Preserve the Classical Structure of Incremental Boundary Value Problems , 1996 .

[7]  John W. Hutchinson,et al.  The mechanics of size-dependent indentation , 1998 .

[8]  A. Mortensen,et al.  Geometrically necessary dislocations and strain-gradient plasticity: a few critical issues , 2003 .

[9]  Anthony G. Evans,et al.  A critical assessment of theories of strain gradient plasticity , 2009 .

[10]  C. F. Niordson,et al.  BASIC STRAIN GRADIENT PLASTICITY THEORIES WITH APPLICATION TO CONSTRAINED FILM DEFORMATION , 2011 .

[11]  P. J. Guruprasad,et al.  Size effects under homogeneous deformation of single crystals: A discrete dislocation analysis , 2008 .

[12]  P. Moreau,et al.  Measurement of the size effect in the yield strength of nickel foils , 2005 .

[13]  N. Schmitt,et al.  Micromechanical testing with microstrain resolution. , 2011, The Review of scientific instruments.

[14]  E. Aifantis Strain gradient interpretation of size effects , 1999 .

[15]  T. Siegmund,et al.  A dislocation density based strain gradient model , 2006 .

[16]  B. Song,et al.  Quasi-Static Torsion Characterization of Micro-diameter Copper Wires , 2011 .

[17]  E. Aifantis On the Microstructural Origin of Certain Inelastic Models , 1984 .

[18]  M. Kuroda,et al.  Strain hardening in bent copper foils , 2011 .

[19]  Xutao Tang,et al.  Size effects in the torsion of microscale copper wires: Experiment and analysis , 2012 .

[20]  A. Bushby,et al.  Theory of deformation in small volumes of material , 2004, Proceedings of the Royal Society of London. Series A: Mathematical, Physical and Engineering Sciences.

[21]  E. Aifantis Update on a class of gradient theories , 2003 .

[22]  T. Tsui,et al.  Increased time-dependent room temperature plasticity in metallic glass nanopillars and its size-dependency , 2012 .

[23]  C. Weinberger,et al.  Orientation-dependent plasticity in metal nanowires under torsion: twist boundary formation and Eshelby twist. , 2010, Nano letters.

[24]  J. Nye Some geometrical relations in dislocated crystals , 1953 .

[25]  G. Voyiadjis,et al.  Nonlocal gradient-dependent modeling of plasticity with anisotropic hardening , 2010 .

[26]  Lallit Anand,et al.  Thermodynamics applied to gradient theories involving the accumulated plastic strain : The theories of Aifantis and Fleck and Hutchinson and their generalization , 2009 .

[27]  D. Dimiduk,et al.  Sample Dimensions Influence Strength and Crystal Plasticity , 2004, Science.

[28]  N. Fleck,et al.  Strain gradient plasticity , 1997 .

[29]  Norman A. Fleck,et al.  Size effects in the torsion of thin metal wires , 2009 .

[30]  N. Moody,et al.  The role of dislocation walls for nanoindentation to shallow depths , 2009 .

[31]  Reinhard Pippan,et al.  A further step towards an understanding of size-dependent crystal plasticity: In situ tension experiments of miniaturized single-crystal copper samples , 2008 .

[32]  W. Curtin,et al.  Stress-gradient plasticity , 2011, Proceedings of the National Academy of Sciences.

[33]  Anthony G. Evans,et al.  A microbend test method for measuring the plasticity length scale , 1998 .

[34]  P. Gumbsch,et al.  Dislocation microstructure evolution in cyclically twisted microsamples: a discrete dislocation dynamics simulation , 2011 .

[35]  N. Wu,et al.  Length scale effect on mechanical behavior due to strain gradient plasticity , 2001 .

[36]  J. Greer,et al.  Microstructure versus size: mechanical properties of electroplated single crystalline Cu nanopillars. , 2010, Physical review letters.

[37]  D. McDowell A perspective on trends in multiscale plasticity , 2010 .

[38]  R. P. Skelton,et al.  The Bauschinger effect, Masing model and the Ramberg–Osgood relation for cyclic deformation in metals , 1997 .

[39]  Hans Muhlhaus,et al.  A variational principle for gradient plasticity , 1991 .

[40]  S. Lee,et al.  Higher Compressive Strengths and Bauschinger Effect in Conformally-Passivated Copper Nanopillars. , 2012 .

[41]  R. LeSar,et al.  Dislocation dynamics simulations of the Bauschinger effect in metallic thin films , 2012 .

[42]  J. Weertman,et al.  Non‐redundant dislocation density field of a circular bar deformed in torsion and the stress gradient hardening effect , 1995 .

[43]  Huajian Gao,et al.  Geometrically necessary dislocation and size-dependent plasticity , 2003 .

[44]  Peter Gumbsch,et al.  Micro-bending tests: A comparison between three-dimensional discrete dislocation dynamics simulations and experiments , 2008 .

[45]  David J. Dunstan,et al.  Size effect in the initiation of plasticity for ceramics in nanoindentation , 2008 .

[46]  Horacio Dante Espinosa,et al.  Discrete dislocation dynamics simulations to interpret plasticity size and surface effects in freestanding FCC thin films , 2006 .

[47]  M. Ashby,et al.  Strain gradient plasticity: Theory and experiment , 1994 .

[48]  George T. Gillies,et al.  Torsion balances, torsion pendulums, and related devices , 1993 .

[49]  O. Kraft,et al.  Size dependent mechanical behaviour of tantalum , 2011 .

[50]  Viggo Tvergaard,et al.  An alternative treatment of phenomenological higher-order strain-gradient plasticity theory , 2010 .

[51]  Norman A. Fleck,et al.  A reformulation of strain gradient plasticity , 2001 .

[52]  G. Voyiadjis,et al.  Analytical and experimental determination of the material intrinsic length scale of strain gradient plasticity theory from micro- and nano-indentation experiments , 2004 .

[53]  R. Pippan,et al.  Cyclic response of copper single crystal micro-beams , 2010 .

[54]  Andrew M Minor,et al.  Mechanical annealing and source-limited deformation in submicrometre-diameter Ni crystals. , 2008, Nature materials.

[55]  D. Dunstan,et al.  Strain and strain relaxation in semiconductors , 1997 .

[56]  Shefford P. Baker,et al.  Bauschinger effect and anomalous thermomechanical deformation induced by oxygen in passivated thin Cu films on substrates , 2003 .

[57]  J. Segurado,et al.  Micropillar compression of LiF [111] single crystals: Effect of size, ion irradiation and misorientation , 2012 .

[58]  Joost J. Vlassak,et al.  Bauschinger and size effects in thin-film plasticity , 2006 .

[59]  J. Greer,et al.  Crystallographic orientation and size dependence of tension–compression asymmetry in molybdenum nano-pillars , 2012 .

[60]  David J. Dunstan,et al.  Grain size and sample size interact to determine strength in a soft metal , 2008 .

[61]  C. Weinberger,et al.  Plasticity of metal wires in torsion: Molecular dynamics and dislocation dynamics simulations , 2010 .

[62]  John W. Hutchinson,et al.  On lower order strain gradient plasticity theories , 2003 .

[63]  C. Motz,et al.  Observation of the critical thickness phenomenon in dislocation dynamics simulation of microbeam bending , 2012 .

[64]  Shaohua Chen,et al.  Size effect in micro-scale cantilever beam bending , 2011 .

[65]  B. Ehrler,et al.  Elastic limit and strain hardening of thin wires in torsion. , 2009, Physical review letters.

[66]  A. Ngan,et al.  Specimen size and grain size effects on tensile strength of Ag microwires , 2011 .

[67]  D. Dunstan Critical Thickness Theory Applied to Micromechanical Testing , 2012 .

[68]  George Z. Voyiadjis,et al.  Thermo-mechanical strain gradient plasticity with energetic and dissipative length scales , 2012 .

[69]  Shaohua Chen,et al.  A new hardening law for strain gradient plasticity , 2000 .

[70]  D. Dunstan,et al.  Size effects in yield and plasticity under uniaxial and non-uniform loading: experiment and theory , 2011 .

[71]  G. Pharr,et al.  The correlation of the indentation size effect measured with indenters of various shapes , 2002 .

[72]  Huajian Gao,et al.  Indentation size effects in crystalline materials: A law for strain gradient plasticity , 1998 .

[73]  Zengsheng Ma,et al.  On the intrinsic hardness of a metallic film/substrate system: Indentation size and substrate effects , 2012 .

[74]  Peter Gudmundson,et al.  A unified treatment of strain gradient plasticity , 2004 .

[75]  M. Walter,et al.  A new method to measure torsion moments on small-scaled specimens. , 2011, The Review of scientific instruments.

[76]  E. Aifantis,et al.  Recent Developments in Gradient Plasticity—Part I: Formulation and Size Effects , 2002 .

[77]  William Cawthorne Unwin The Testing of Materials of Construction: A Text-Book for the Engineering Laboratory and a Collection of the Results of Experiment , 2012 .

[78]  Y. Milman,et al.  Microindentations on W and Mo oriented single crystals: An STM study , 1993 .

[79]  John L. Bassani,et al.  Incompatibility and a simple gradient theory of plasticity , 2001 .

[80]  Huajian Gao,et al.  A conventional theory of mechanism-based strain gradient plasticity , 2004 .

[81]  J. Weertman,et al.  Anomalous work hardening, non-redundant screw dislocations in a circular bar deformed in torsion, and non-redundant edge dislocations in a bent foil , 2002 .

[82]  Huajian Gao,et al.  Mechanism-based strain gradient plasticity— I. Theory , 1999 .

[83]  Norman A. Fleck,et al.  A mathematical basis for strain-gradient plasticity theory. Part II: Tensorial plastic multiplier , 2009 .