Terahertz transmission-mode near-field scanning-probe microscope based on a flexible sapphire fiber

We present the terahertz (THz) near-field microscope, in which a flexible sapphire fiber serves as a scanning probe. High refractive index of sapphire at THz frequencies allows for a strong confinement of guided modes in a fiber core, and, thus, for a sub-wavelength resolution THz imaging. In turn, low THz-wave absorption in sapphire allows for guiding the THz waves in a fiber over tens of centimeters with rather high energy efficiency. The developed THz microscope operates in a transmission mode and uses a backward wave oscillator, as a continuous-wave THz source with the output wavelength of λ = 1200 µm, a Golay cell, as a detector of THzwave intensity, and a 300 µm-diameter flexible sapphire fiber with at input and output ends, as a scanning probe. In our THz microscope arrangement, the input end of a sapphire fiber is mounted on a motorized translation stage, which yield two- or even three-dimensional imaging of electromagnetic field formed at the shadow side of an object; while the output fiber end is rigidly fixed in front of the detector aperture. The experimental setup was applied for imaging of representative test objects, and the observed results demonstrated its advanced spatial resolution of ~ λ=4, which is beyond the Abbe diffraction limit. In our opinion, the sub-wavelength spatial resolution, along with a high energy throughout, open a wide range of the developed THz microscope applications in material science, non-destructive testing, and biophotonics.

[1]  Masatsugu Yamashita,et al.  Laser terahertz-emission microscope for inspecting electrical faults in integrated circuits. , 2003 .

[2]  Kiarash Ahi,et al.  Quality control and authentication of packaged integrated circuits using enhanced-spatial-resolution terahertz time-domain spectroscopy and imaging , 2017 .

[3]  Daniel M. Mittleman,et al.  Metal wires for terahertz wave guiding , 2004, Nature.

[4]  Warren S Grundfest,et al.  Non-invasive terahertz imaging of tissue water content for flap viability assessment. , 2017, Biomedical optics express.

[5]  Laurent Chusseau,et al.  Near-field wire-based passive probe antenna for the selective detection of the longitudinal electric field at terahertz frequencies , 2009 .

[6]  I. A. Shikunova,et al.  Sapphire Photonic Crystal Waveguides for Terahertz Sensing in Aggressive Environments , 2018, Advanced Optical Materials.

[7]  John L. Reno,et al.  Photoconductive terahertz near-field detector with a hybrid nanoantenna array cavity , 2015 .

[8]  Guglielmo Lanzani,et al.  Photophysics of Molecular Materials From Single Molecules to Single Crystals , 2005 .

[9]  D. Grischkowsky,et al.  Far-infrared time-domain spectroscopy with terahertz beams of dielectrics and semiconductors , 1990 .

[10]  G. S. Kolontaeva,et al.  Reflection-mode continuous-wave 0.15λ-resolution terahertz solid immersion microscopy of soft biological tissues , 2018, Applied Physics Letters.

[11]  O. E. Porodinkov,et al.  BWO Generators for Terahertz Dielectric Measurements , 2013, IEEE Transactions on Terahertz Science and Technology.

[12]  Alexander J. Macfaden,et al.  3 μm aperture probes for near-field terahertz transmission microscopy , 2014 .

[13]  M. Golay,et al.  The theoretical and practical sensitivity of the pneumatic infra-red detector. , 1949, The Review of scientific instruments.

[14]  G. Kino,et al.  Solid immersion microscope , 1990 .

[15]  James Lloyd-Hughes,et al.  A Review of the Terahertz Conductivity of Bulk and Nano-Materials , 2012 .

[16]  R. Leonhardt,et al.  Aspheric lenses for Terahertz imaging , 2008, 2008 Conference on Lasers and Electro-Optics and 2008 Conference on Quantum Electronics and Laser Science.

[17]  Haofei Shi,et al.  Conductivity mapping of graphene on polymeric films by terahertz time-domain spectroscopy. , 2018, Optics express.

[18]  Godehard Wüstefeld,et al.  THz near-field imaging employing synchrotron radiation , 2004 .

[19]  R. Kersting,et al.  Terahertz imaging with nanometer resolution , 2003 .

[20]  Matthew C. Beard,et al.  Transient photoconductivity in GaAs as measured by time-resolved terahertz spectroscopy , 2000 .

[21]  Zengbo Wang,et al.  Refractive index less than two: photonic nanojets yesterday, today and tomorrow [Invited] , 2017 .

[22]  A. A. Konovko,et al.  Terahertz biophotonics as a tool for studies of dielectric and spectral properties of biological tissues and liquids , 2018, Progress in Quantum Electronics.

[23]  Yang Hao,et al.  Magnification of subwavelength field distributions at microwave frequencies using a wire medium slab operating in the canalization regime , 2007, 0705.3183.

[24]  Paul C. M. Planken,et al.  Electro-optic detection of subwavelength terahertz spot sizes in the near field of a metal tip , 2002 .

[25]  E. Hendry,et al.  Carrier dynamics in semiconductors studied with time-resolved terahertz spectroscopy , 2011 .

[26]  Valery V. Tuchin,et al.  The progress and perspectives of terahertz technology for diagnosis of neoplasms: a review , 2019, Journal of Optics.

[27]  I. A. Shikunova,et al.  Sapphire shaped crystals for waveguiding, sensing and exposure applications , 2018, Progress in Crystal Growth and Characterization of Materials.

[28]  Kirill I. Zaytsev,et al.  Solid immersion terahertz imaging with sub-wavelength resolution , 2017 .

[29]  Jianquan Yao,et al.  High-sensitivity terahertz imaging of traumatic brain injury in a rat model , 2018, Journal of biomedical optics.

[30]  Kathirvel Nallappan,et al.  Toward real-time terahertz imaging , 2018, Advances in Optics and Photonics.

[31]  Tadao Nagatsuma,et al.  Enhancement of spatial resolution of terahertz imaging systems based on terajet generation by dielectric cube , 2017 .

[32]  Yuh-Jing Hwang,et al.  All-terahertz fiber-scanning near-field microscopy. , 2009, Optics letters.

[33]  Aurèle J. L. Adam,et al.  Review of Near-Field Terahertz Measurement Methods and Their Applications , 2011 .

[34]  Martin Dressel,et al.  THz-micro-spectroscopy with backward-wave oscillators , 2006 .

[35]  K. M. Malakhov,et al.  Terahertz spectroscopy of gelatin-embedded human brain gliomas of different grades: a road toward intraoperative THz diagnosis , 2019, Journal of biomedical optics.

[36]  J. Aizpurua,et al.  Terahertz near-field nanoscopy of mobile carriers in single semiconductor nanodevices. , 2008, Nano letters.

[37]  Igor V. Minin,et al.  Photonic Hook Plasmons: A New Curved Surface Wave , 2018, Annalen der Physik.

[38]  I. V. Minin,et al.  Experimental observation of a photonic hook , 2018, Applied Physics Letters.

[39]  Igal Brener,et al.  Collection-mode near-field imaging with 0.5-THz pulses , 2001 .

[40]  V. V. Tuchin,et al.  Multimodal Optical Diagnostics of Glycated Biological Tissues , 2019, Biochemistry (Moscow).

[41]  D. Smith,et al.  Electromagnetic wave propagation in media with indefinite permittivity and permeability tensors. , 2002, Physical Review Letters.

[42]  Michael Nagel,et al.  Tapered Sommerfeld wire terahertz near-field imaging , 2009 .

[43]  Hak-Sung Kim,et al.  Non-destructive evaluation of the hidden voids in integrated circuit packages using terahertz time-domain spectroscopy , 2015 .

[44]  Alexander Argyros,et al.  A prism based magnifying hyperlens with broad-band imaging , 2017 .

[45]  Robert L. Byer,et al.  Characterization of single‐crystal sapphire fibers for optical power delivery systems , 1989 .

[46]  Vladimir N. Kurlov,et al.  A review of developments in shaped crystal growth of sapphire by the Stepanov and related techniques , 2002 .

[47]  M. E. Frolov,et al.  Wide-aperture aspherical lens for high-resolution terahertz imaging. , 2017, The Review of scientific instruments.

[48]  N. Abrosimovi Automated control of Czochralski and shaped crystal growth processes using weighing techniques , 2003 .

[49]  P. Bøggild,et al.  Graphene conductance uniformity mapping. , 2012, Nano letters.

[50]  David G. Cooke,et al.  Probing Organic Semiconductors with Terahertz Pulses , 2006 .

[51]  Eui Su Lee,et al.  Enhancement of the detection of THz Sommerfeld wave using a conical wire waveguide. , 2008, Optics express.