Crack-healing ability of structural ceramics and a new methodology to guarantee the structural integrity using the ability and proof-test

Abstract Recently, the authors developed Si 3 N 4 , Al 2 O 3 and mullite ceramics with good self-crack-healing abilities. It was shown that the optimized crack-healing condition to get high temperature strength was: 1573 K, 1 h, in air, and the healed zone exhibited the same strength as the base material up to about 1573 K (Si 3 N 4 and Al 2 O 3 ) and 1473 K (mullite), respectively. Using this good crack-healing ability, a new methodology to guarantee the reliability of ceramic components [crack-healing + proof test] was proposed. It was shown that reliability could be guaranteed before service by this technique, using about 200 samples. However, if a crack initiated during service, reliability would be severely impaired. Therefore, if a material can heal a crack during service, and if the healed zone has enough strength at the temperature of healing, it would be very desirable for structural integrity. From the above points of view, a new methodology to guarantee the structural integrity of ceramic components using in situ crack-healing ability was proposed and the usefulness is discussed using the test results in terms of crack-healing behavior and proof test theory by the authors.

[1]  S. Usami,et al.  Flaw size dependence in fracture stress of glass and polycrystalline ceramics. , 1985 .

[2]  Shigemi Sato,et al.  (Crack-healing+proof test): a new methodology to guarantee the structural integrity of a ceramics component , 2002 .

[3]  繁美 佐藤,et al.  炭化物粒子分散によるムライトの高強度化に関する研究 : 第1報,SiCおよびTiC粒子分散の効果 , 1994 .

[4]  J. J. Petrovic,et al.  Controlled Surface Flaws in Hot‐Pressed SiC , 1975 .

[5]  敏彦 星出,et al.  セラミックスの保証試験後の疲労特性に関する研究 : 第2報, 実験的検討 , 1990 .

[6]  Sung R. Choi,et al.  Crack healing behavior of hot pressed silicon nitride due to oxidation , 1992 .

[7]  Kotoji Ando,et al.  Crack-Healing Behavior of Liquid-Phase-Sintered Silicon Carbide Ceramics , 2003 .

[8]  F. Lange,et al.  Healing of Surface Cracks in Polycrystalline Al2O3 , 1970 .

[9]  S. Wiederhorn,et al.  Proof-testing of hot-pressed silicon nitride , 1978 .

[10]  Byung-Soo Kim,et al.  Crack-Healing Behavior of Monolithic Alumina and Strength of Crack-Healed Member , 2003 .

[11]  Shigemi Sato,et al.  Crack-healing behavior under stress of mullite/silicon carbide ceramics and the resultant fatigue strength , 2004 .

[12]  Kotoji Ando,et al.  Crack-healing behavior, high temperature and fatigue strength of SiC-reinforced silicon nitride composite , 2000 .

[13]  Kotoji Ando,et al.  Fatigue strength of crack‐healed Si3N4/SiC composite ceramics , 1999 .

[14]  T. K. Gupta,et al.  Crack Healing and Strengthening of Thermally Shocked Alumina , 1976 .

[15]  Sheldon M. Wiederhorn,et al.  Proof testing of ceramics , 1980 .

[16]  K. Ando,et al.  Strength Properties of Crack-Healed Silicon-Carbide Ceramics , 2003 .

[17]  Shigemi Sato,et al.  Fatigue Strength Properties of Crack Healed Mullite/SiC Composite Ceramics. , 1999 .

[18]  F. F. Lange,et al.  Crack Healing by Heat Treatment , 1970 .

[19]  M. Chu,et al.  Crack Healing Behavior and High Temperature Strength of Mullite/SiC Composite Ceramics. , 1999 .

[20]  Shigemi Sato,et al.  Static and cyclic fatigue behaviour of crack-healed Si3N4/SiC composite ceramics , 2001 .

[21]  K. Houjou,et al.  Crack-healing and oxidation behavior of silicon nitride ceramics , 2004 .

[22]  Kotoji Ando,et al.  EFFECTS OF CRACK LENGTH, NOTCH ROOT RADIUS AND GRAIN SIZE ON FRACTURE TOUGHNESS OF FINE CERAMICS , 1993 .

[23]  P. B. Oates,et al.  Proof testing of ceramics , 1980 .

[24]  Kotoji Ando,et al.  Crack‐Healing Behavior of Si3N4/SiC Ceramics under Cyclic Stress and Resultant Fatigue Strength at the Healing Temperature , 2002 .

[25]  Shigemi Sato,et al.  Crack-Healing Behavior of Structural Ceramics under Constant and Cyclic Stress at Elevated Temperature , 2002 .

[26]  敏彦 星出,et al.  セラミックスの保証試験後の疲労特性に関する研究 : 第1報, 理論的解析 , 1990 .

[27]  Shigemi Sato,et al.  Crack healing behaviour and high-temperature strength of mullite/SiC composite ceramics , 2002 .

[28]  M. Chu,et al.  Crack healing behavior of silicon carbide ceramics , 2004 .

[29]  Shigemi Sato,et al.  The Study on Crack Healing Behaviour of Silicon Nitride Ceramics. , 1998 .

[30]  Kotoji Ando,et al.  PROCESS ZONE SIZE FAILURE CRITERION AND PROBABILISTIC FRACTURE ASSESSMENT CURVES FOR CERAMICS , 1992 .

[31]  Shigemi Sato,et al.  Crack-healing behavior of Si3N4/SiC ceramics under stress and fatigue strength at the temperature of healing (1000 °C) , 2002 .

[32]  Kotoji Ando,et al.  A PRELIMINARY STUDY ON CRACK HEALING BEHAVIOUR OF Si3 N4 /SiC COMPOSITE CERAMICS , 1998 .