Motivation Identification from metabolomics mass spectrometry experiments requires comparison of fragmentation spectra from experimental samples to spectra from analytical standards. As the quality of identification depends directly on the quality of the reference spectra, manual curation is routine during the selection of reference spectra to include in a spectral library. Whilst building our own in-house spectral library we realised that there is currently no vendor neutral open access tool for for facilitating manual curation of spectra from raw LC-MS data into a custom spectral library. Results We developed a web application curatr for the rapid generation of high quality mass spectral fragmentation libraries for liquid-chromatography mass spectrometry analysis. Curatr handles datasets from single or multiplexed standards, automatically extracting chromatographic profiles and potential fragmentation spectra for multiple adducts. These are presented through an intuitive interface for manual curation before being documented in a custom spectral library. Searchable molecular information and the providence of each standard is stored along with metadata on the experimental protocol. Curatr support the export of spectral libraries in several standard formats for easy use with third party software or submission to community databases, maximising the return on investment for these costly measurements. We demonstrate the use of curatr to generate the EMBL Metabolomics Core Facility spectral library which is publicly available at http://curatr.mcf.embl.de. Availability The source code is freely available at http://github.com/alexandrovteam/curatr/ along with example data. Supplementary information A step-by step user manual is available in the supplementary information
[1]
Robert Burke,et al.
ProteoWizard: open source software for rapid proteomics tools development
,
2008,
Bioinform..
[2]
Kristian Fog Nielsen,et al.
Sharing and community curation of mass spectrometry data with Global Natural Products Social Molecular Networking
,
2016,
Nature Biotechnology.
[3]
Caroline H. Johnson,et al.
Metabolomics: beyond biomarkers and towards mechanisms
,
2016,
Nature Reviews Molecular Cell Biology.
[4]
Christoph Steinbeck,et al.
MetaboLights—an open-access general-purpose repository for metabolomics studies and associated meta-data
,
2012,
Nucleic Acids Res..
[5]
O. Fiehn,et al.
FiehnLib: mass spectral and retention index libraries for metabolomics based on quadrupole and time-of-flight gas chromatography/mass spectrometry.
,
2009,
Analytical chemistry.
[6]
Emma L. Schymanski,et al.
Automatic recalibration and processing of tandem mass spectra using formula annotation.
,
2013,
Journal of mass spectrometry : JMS.
[7]
Nigel W. Hardy,et al.
Proposed minimum reporting standards for chemical analysis
,
2007,
Metabolomics.
[8]
Tobias Schulze,et al.
SPLASH, a hashed identifier for mass spectra
,
2016,
Nature Biotechnology.