Mechanical behavior of Ti3AlC2 prepared by pulse discharge sintering method

Almost single-phase ternary compound Ti3AlC2 was successfully synthesized by pulse discharge sintering (PDS) from Ti/Al/TiC powder mixtures with molar ratio of 2:2:3 . The typical microstructure of Ti3AlC2 was found to consist of plate-like grains with mean size of 9.5 mm in length. Four-point bending testing results revealed that the fracture behavior is brittle below 1200 � C, and some characteristics of plastic deformation were observed at higher testing temperatures. The polycrystalline Ti3AlC2 synthesized by PDS technique shows good strength at high temperatures. [doi:10.2320/matertrans.MAW200703]

[1]  Zhengming Sun,et al.  Synthesis of high-purity polycrystalline Ti3AlC2 through pulse discharge sintering Ti/Al/TiC powders , 2008 .

[2]  Zhengming Sun,et al.  Synthesis reactions for Ti3AlC2 through pulse discharge sintering Ti/Al4C3/TiC powder mixture , 2006 .

[3]  Jiaoqun Zhu,et al.  Synthesis of high-purity Ti3SiC2 and Ti3AlC2 by spark plasma sintering (SPS) technique , 2005 .

[4]  S. Kalidindi,et al.  Damage Mechanisms around Hardness Indentations in Ti3SiC2 , 2005 .

[5]  M. Barsoum,et al.  Synthesis and Characterization of Ti3AlC2 , 2004 .

[6]  E. Gutmanas,et al.  Pressure‐Assisted Combustion Synthesis of Dense Layered Ti3AlC2 and its Mechanical Properties , 2004 .

[7]  Zhengming Sun,et al.  Micron‐scale Deformation and Damage Mechanisms of Ti3SiC2 Crystals Induced by Indentation , 2004 .

[8]  Jiaoqun Zhu,et al.  Synthesis of single-phase polycrystalline Ti3SiC2 and Ti3AlC2 by hot pressing with the assistance of metallic Al or Si , 2004 .

[9]  Jiaoqun Zhu,et al.  Synthesis of high-purity Ti3SiC2 and Ti3AlC2 by hot-pressing (HP) , 2003 .

[10]  Chang-An Wang,et al.  Synthesis and mechanical properties of Ti3AlC2 by spark plasma sintering , 2003 .

[11]  J. Ferreira,et al.  Combustion synthesis of ternary carbide Ti3AlC2 in Ti–Al–C system , 2003 .

[12]  Zhengming Sun,et al.  Deformation and fracture behavior of ternary compound Ti3SiC2 at 25–1300 °C , 2003 .

[13]  Yanchun Zhou,et al.  Solid–liquid reaction synthesis of layered machinable Ti3AlC2 ceramic , 2002 .

[14]  W. Pan,et al.  Mechanical properties of polycrystalline Ti3SiC2 at ambient and elevated temperatures , 2001 .

[15]  Di Zhang,et al.  Dense Ti3SiC2 prepared by reactive HIP , 1999 .

[16]  K. Matsugi,et al.  Impact properties of spark sintered titanium aluminides at elevated temperatures , 1999 .

[17]  M. Komatsu,et al.  Mechanical properties of spark plasma sintered Nb–Al compacts strengthened by dispersion of Nb2N phase and additions of Mo and W , 1999 .

[18]  M. Barsoum,et al.  Layered machinable ceramics for high temperature applications , 1997 .

[19]  J. Schuster,et al.  Summary of constitutional data on the Aluminum-Carbon-Titanium system , 1994 .

[20]  M. Tokita Trends in Advanced SPS Spark Plasma Sintering Systems and Technology , 1993 .