Effect of high‐temperature, high‐pressure, and acidic conditions on the structure and properties of high‐performance fibers

High‐performance fibers such as carbon, aramid, and glass fiber generally have excellent mechanical, thermal, and chemical resistance and they have potential applications in oil and gas exploitation where high‐temperature and high‐pressure (HTHP) H2S/CO2 corrosive environments usually exist. To investigate the corrosion behavior of these fibers under such environments, two corrosion environments (HTHP water, HTHP H2S/CO2) were simulated in a high‐temperature high‐pressure reactor. Scanning electron microscope, X‐ray diffraction, density measurements, and single fiber tensile test were performed to study the surface morphology, crystal structure, and mechanical properties before and after corrosion. After exposure to the second corrosion environment, the carbon aramid fibers had no obvious mass loss and tensile strength retention of 70.28% and 49.66%, respectively. The surface of the aramid fiber and carbon fibers was significantly damaged which led to an increase in surface defects and a decrease in crystallinity. The glass fiber had clear weight loss due to a large number of defects being formed in the structure and the retention of tensile fracture strength was 48.18%. Corrosion under HTHP H2S/CO2 conditions caused more serious damage to the high‐performance fiber structures.

[1]  D. Harrison,et al.  Adhesively bonded CFRP/Al joints: Influence of the surface pretreatment on corrosion during salt spray test , 2021, Materials and Corrosion.

[2]  B. Ma,et al.  Durability Study on High-Performance Fiber-Reinforced Mortar under Simulated Wastewater Pipeline Environment , 2021, Materials.

[3]  Yudong Huang,et al.  Surface modification of aramid fibers by amino functionalized silane grafting to improve interfacial property of aramid fibers reinforced composite , 2020 .

[4]  P. Alaba,et al.  Unveiling Corrosion Behavior of Pipeline Steels in CO2-Containing Oilfield Produced Water: Towards Combating the Corrosion Curse , 2020, Critical Reviews in Solid State and Materials Sciences.

[5]  Zhishen Wu,et al.  Fatigue degradation and life prediction of basalt fiber-reinforced polymer composites after saltwater corrosion , 2019, Materials & Design.

[6]  D. Jiang,et al.  Effect of hydrothermal aging on the dynamic mechanical performance of the room temperature-cured epoxy adhesive , 2019, Rheologica Acta.

[7]  Changhong Cai,et al.  Effect of anodic T phase on surface micro-galvanic corrosion of biodegradable Mg-Zn-Zr-Nd alloys , 2018, Applied Surface Science.

[8]  B. Kandasubramanian,et al.  Functionalized Aramid Fibers and Composites for Protective Applications: A Review , 2018, Industrial & Engineering Chemistry Research.

[9]  Xu Wang,et al.  The novel high performance aramid fibers containing benzimidazole moieties and chloride substitutions , 2018, Materials & Design.

[10]  B. A. Patterson,et al.  Aramid nanofibers for multiscale fiber reinforcement of polymer composites , 2018 .

[11]  G. Grundmeier,et al.  Corrosive delamination processes of CFRP‐aluminum alloy hybrid components , 2018 .

[12]  Bin Wang,et al.  A facile method modified PBO fibers by polysiloxane microtube , 2017 .

[13]  J. Kaplan,et al.  The Neuropeptides FLP-2 and PDF-1 Act in Concert To Arouse Caenorhabditis elegans Locomotion , 2016, Genetics.

[14]  M. A. O. Ignacio,et al.  How to cite this article , 2016 .

[15]  M. Shokrieh,et al.  Corrosion behaviour and crack formation mechanism of basalt fibre in sulphuric acid , 2012 .

[16]  Houbu Li,et al.  Corrosion resistance of E6-glass fibre in simulated oilfield environments , 2012 .

[17]  H. Wang,et al.  Influence of corrosion on the interface between zinc phosphate steel fiber and cement , 2012 .

[18]  Robert L. Jones Chemical Corrosion of E‐Glass Fibers in Oxalic and Other Organic Acids , 2006 .

[19]  H. Lilholt,et al.  Tensile strength and fracture surface characterisation of sized and unsized glass fibers , 2005 .

[20]  T. Gierke,et al.  Morphology of poly(p‐phenylene terephthalamide) fibers , 1983 .

[21]  Roy W. Rice,et al.  Prediction of Fracture Energy and Flaw Size in Glasses from Measurements of Mirror Size , 1974 .