Umlagerungen der Phenylthiogruppe in Trimethylsilyl‐enoläthern von α,α‐dialkyl‐α‐phenylthio‐ketonen
暂无分享,去创建一个
Rearrangements of the Phenylthio Group of Trimethylsilyl-enolethers of α,α-Dialkylated α-Phenylthio-ketones
Trimethylsilyl-enolethers of α,α-dialkylated α-phenylthio-ketones undergo a photochemically induced 1,3-phenylthio shift leading to isomeric enolethers in high yields. The rearrangement can also be carried out under thermal conditions, but the results are less satisfying.
[1] H. Kwart,et al. Secondary deuterium isotope effects in the thia-allylic rearrangement , 1977 .
[2] B. Trost,et al. New synthetic reactions. Sulfenylations and dehydrosulfenylations of esters and ketones , 1976 .
[3] D. Seebach,et al. Herstellung α-thiolierter Carbonylverbindungen , 1976 .