Investigating the dynamic behaviour of fluidized bed spray granulation processes applying numerical simulation tools

Abstract Particulate processes involve different kinetic processes such as formation of nuclei, their subsequent growth and breakage. In addition, external product classification can play a significant role. A reliable prediction and thorough understanding of potential sources for instability is not only of scientific interest but also an important issue for better process design and process control. The application of these nonlinear dynamics is concerned with fluidized bed spray granulation. Self-sustained oscillations may rise in processes with external product classification. Therefore, focus of this work is on process stability which can be influenced by classifying, milling and recycling of particles and by the production of internal and external seeds. First a brief introduction to the model is given, that couples the particle population state with thermodynamic-, fluiddynamic- and granulation process for a unit with non-classifying product discharge and a screening and milling unit in the seed recycle and builds the core of the software package AVA ® FB Sim ® , used for the experiments.

[1]  H. Klan,et al.  Wärmeübergang durch freie Konvektion an umströmten Körpern , 2002 .

[2]  K. Stephen,et al.  Wärmeübertragung n Festbetten, druchmischten Schüttgütern und Wirbelschichten. Von E.-U. Schlünder und E. Tsotsas. Georg Thieme Verlag, Stuttgart– New York 1988. XII, 259 S., 161 Abb., 33 Tab., kart., DM 58 , 1989 .

[3]  Daming Shi Fluiddynamik und Wärmeübergang in einer zirkulierenden Wirbelschicht , 1996 .

[4]  Doraiswami Ramkrishna,et al.  Population Balances: Theory and Applications to Particulate Systems in Engineering , 2000 .

[5]  D. Ramkrishna The Status of Population Balances , 1985 .

[6]  V. Gnielinski Wärme‐ und Stoffübertragung in Festbetten , 1980 .

[7]  Stefan Heinrich,et al.  Study of dynamic multi-dimensional temperature and concentration distributions in liquid-sprayed fluidized beds , 2003 .

[8]  Stefan Heinrich,et al.  Fluidized bed spray granulation—A new model for the description of particle wetting and of temperature and concentration distribution , 1999 .

[9]  Stefan Heinrich,et al.  Particle population modeling in fluidized bed-spray granulation—analysis of the steady state and unsteady behavior , 2003 .

[10]  M. Hounslow,et al.  Adjustable discretized population balance for growth and aggregation , 1995 .

[11]  Stefan Heinrich,et al.  Decay Behavior of Particles in a Fluidized Bed – Application of a Mass-Related Attrition Coefficient , 2002 .

[12]  Sotiris E. Pratsinis,et al.  Gas-phase manufacture of particulates: interplay of chemical reaction and aerosol coagulation in the free-molecular regime , 1989 .