Investigating surface stress: Surface loss in ultrathin single-crystal silicon cantilevers

We investigated the effect of surface treatment in an ultrahigh-vacuum chamber on the Q factor of ultrathin single-crystal silicon cantilevers with different thicknesses (60, 170, and 500 nm) and different surface orientations. When the length is L>30 μm, the Q factor is proportional to the thickness and surface loss dominates, whereas when L<30 μm, support loss surpasses the surface loss. Heating can remove the SiO2 layer and absorbates and results in an increase of the Q factor. Hydrogen termination leads to a larger relative increase of the Q factor in thinner structures than in thicker ones. Heating and H exposure improve the Q values of Si(100)-oriented cantilevers more than Si(110)-oriented ones, and they result in the opposing resonance frequency response for these two surfaces.

[1]  Boland Structure of the H-saturated Si(100) surface. , 1990, Physical review letters.

[2]  J. Boland Scanning tunneling microscopy study of the adsorption and recombinative desorption of hydrogen from the Si(100)‐2×1 surface , 1992 .

[3]  Harald Ibach,et al.  The role of surface stress in reconstruction, epitaxial growth and stabilization of mesoscopic structures , 1997 .

[4]  Thomas Thundat,et al.  Adsorption-induced surface stress and its effects on resonance frequency of microcantilevers , 1995 .

[5]  Miura,et al.  Atomic configuration of hydrogenated and clean Si(110) surfaces. , 1986, Physical review. B, Condensed matter.

[6]  Schell-Sorokin Aj,et al.  Mechanical stresses in (sub)monolayer epitaxial films. , 1990 .

[7]  Harry C. Gatos,et al.  Surface stress and the normal mode of vibration of thin crystals :GaAs , 1975 .

[8]  N. C. MacDonald,et al.  Dissipation measurements of vacuum-operated single-crystal silicon microresonators , 1995 .

[9]  S. Jeng,et al.  Efficiency of oxygen plasma cleaning of reactive ion damaged silicon surfaces , 1988 .

[10]  H. Ibach,et al.  Adsorbate‐induced surface stress , 1994 .

[11]  J. Boland Role of bond-strain in the chemistry of hydrogen on the Si(100) surface , 1992 .

[12]  B. Anthony,et al.  Very low defect remote hydrogen plasma clean of Si (100) for homoepitaxy , 1990 .

[13]  Grossmann,et al.  Giant Surface Stress in Heteroepitaxial Films: Invalidation of a Classical Rule in Epitaxy. , 1996, Physical review letters.