2-(4-Bromobenzenesulfonamido)-2-phenylacetic acid monohydrate

In the title compound, C14H12BrNO4S·H2O, the phenyl and benzene rings are inclined at a dihedral angle of 39.5 (5)°. The crystal packing is stabilized by N—H⋯O, C—H⋯O and O—H⋯O hydrogen-bonding interactions.

[1]  G. G. Stokes.  "J." , 1890, The New Yale Book of Quotations.

[2]  Rui Wang,et al.  The Natural Amino Acid Derived Chiral Sulfonamide Ligands in the Catalytic Asymmetric Addition of Phenylacetylene to Aldehydes , 2006 .

[3]  Louis J. Farrugia,et al.  ORTEP-3 for Windows - a version of ORTEP-III with a Graphical User Interface (GUI) , 1997 .

[4]  H. Flack,et al.  On enantiomorph‐polarity estimation , 1983 .

[5]  Salman A. Khan,et al.  2-Benzenesulfonamidobenzoic acid , 2009, Acta crystallographica. Section E, Structure reports online.

[6]  E. Springman,et al.  Amino acid derived sulfonamide hydroxamates as inhibitors of procollagen C-proteinase. Part 2: Solid-phase optimization of side chains. , 2002, Bioorganic & medicinal chemistry letters.

[7]  Louis J. Farrugia,et al.  WinGX suite for small-molecule single-crystal crystallography , 1999 .

[8]  Xiaohu Deng,et al.  A facile, environmentally benign sulfonamide synthesis in water , 2006 .

[9]  D. Velmurugan,et al.  2-[1-(Phenylsulfonyl)ethyl]benzoic acid and 2-[1-(phenylsulfonyl)propyl]benzoic acid. , 2002, Acta crystallographica. Section C, Crystal structure communications.

[10]  Anthony L. Spek,et al.  Structure validation in chemical crystallography , 2009, Acta crystallographica. Section D, Biological crystallography.

[11]  Scott A. Erickson,et al.  Discovery and optimization of anthranilic acid sulfonamides as inhibitors of methionine aminopeptidase-2: a structural basis for the reduction of albumin binding. , 2006, Journal of medicinal chemistry.

[12]  Maria Cristina Burla,et al.  SIR97: a new tool for crystal structure determination and refinement , 1999 .

[13]  良二 上田.  J. Appl. Cryst.の発刊に際して , 1970 .

[14]  G. Sheldrick.  A short history of SHELX. , 2008, Acta crystallographica. Section A, Foundations of crystallography.

[15]  Olga Kennard,et al.  Tables of bond lengths determined by X-ray and neutron diffraction. Part 1. Bond lengths in organic compounds , 1987 .

[16]  Muhammad Nadeem Arshad,et al.  Methyl 3-hydroxy-4-oxo-3,4-dihydro-2H-1,2-benzothiazine-3-carboxylate 1,1-dioxide monohydrate , 2008, Acta crystallographica. Section E, Structure reports online.

[17]  Muhammad Nadeem Arshad,et al.  (2R)-2-Benzenesulfonamido-2-phenylethanoic acid , 2009, Acta crystallographica. Section E, Structure reports online.