Microstructural imaging techniques: a comparison between light and scanning electron microscopy

Abstract Both light microscopy and scanning electron microscopy are commonly used in microstructural studies of geological specimens. This contribution uses polished thin sections to analyse the same areas in two specimens using both microscopy techniques. The images from a quartz mylonite and a granodiorite are compared to quantitative crystallographic data obtained using electron backscatter diffraction (EBSD). The results indicate that light microscopy images pick out all high angle (>10° misorientation) boundaries but only some low angle and twin boundaries, therefore making it suitable for imaging more general microstructural trends. Orientation contrast imaging, using forescatter detectors in the SEM, images all types of crystallographic boundary: this can obscure the general microstructural trend but makes it more suitable for detailed microstructural analyses. Future studies are advised, wherever possible, to utilise the imaging advantages from a combination of both techniques.

[1]  Niels-Henrik Schmidt,et al.  Computer-aided determination of crystal-lattice orientation from electron channeling patterns in the SEM , 1989 .

[2]  Valerie Randle,et al.  Microtexture Determination and Its Applications , 2023 .

[3]  David C. Joy,et al.  Advanced Scanning Electron Microscopy and X-Ray Microanalysis , 1986, Springer US.

[4]  D. Prior,et al.  Grain boundary hierarchy development in a quartz mylonite , 1998 .

[5]  M. Heu,et al.  The SEM examination of geological samples with a semiconductor backscattered-electron detector: reply , 1983 .

[6]  H. Bunge Textures of geological materials , 1994 .

[7]  V. Randle,et al.  Microtexture determination by electron back-scatter diffraction , 1992 .

[8]  D. Coates Kikuchi-like reflection patterns obtained with the scanning electron microscope , 1967 .

[9]  S. Schmid,et al.  Simple shear deformation and quartz crystallographic fabrics: a possible natural example from the Torridon area of NW Scotland , 1990 .

[10]  Geoffrey E. Lloyd,et al.  Atomic number and crystallographic contrast images with the SEM: a review of backscattered electron techniques , 1987, Mineralogical Magazine.

[11]  H. Wenk,et al.  Local Microstructural Investigations in Recrystallized Quartzite Using Orientation Imaging Microscopy , 1994 .

[12]  A. Kearsley,et al.  Application of backscattered electron microscopy in shale petrology , 1983, Geological Magazine.

[13]  F. C. Phillips,et al.  An introduction to the study of fabrics of geological bodies , 1970 .

[14]  D. Prior,et al.  Orientation contrast imaging of microstructures in rocks using forescatter detectors in the scanning electron microscope , 1996, Mineralogical Magazine.

[15]  S. White Grain and sub-grain size variations across a mylonite zone , 1979 .

[16]  R. Heilbronner,et al.  Fabric domains in quartz mylonites: localized three dimensional analysis of microstructure and texture , 1996 .

[17]  Renée Heilbronner,et al.  Integrated spatial and orientation analysis of quartz c-axes by computer-aided microscopy , 1993 .

[18]  K. Kunze,et al.  Orientation imaging: The emergence of a new microscopy , 1993 .

[19]  G. Lloyd,et al.  The SEM examination of geological samples with a semiconductor back-scattered electron detector , 1981 .

[20]  Timothy K. Maugel,et al.  Quantitative scanning electron microscopy , 1976 .

[21]  Brent L. Adams,et al.  Orientation Imaging Microscopy: New Possibilities for Microstructural Investigations Using Automated BKD Analysis , 1994 .

[22]  Paul F. Williams,et al.  An Outline of Structural Geology , 1976 .

[23]  David C. Joy,et al.  Electron channeling patterns in the scanning electron microscope , 1982 .

[24]  G. Lloyd,et al.  Application of scanning electron microscopy to the study of deformed rocks , 1981 .

[25]  K. Lücke,et al.  Textures of Materials , 1978 .

[26]  W. Mader SCANNING ELECTRON MICROSCOPY AND X-RAY ANALYSIS , 1994 .

[27]  J. Huggett,et al.  The Use of Back-Scattered Electron Imaging for the Petrographic Study of Sandstones and Shales , 1984 .

[28]  G. Lloyd,et al.  Discriminatory petrofabric analysis of quartz rocks using SEM electron channelling , 1987 .

[29]  D. W. Pashley,et al.  High-angle Kikuchi patterns , 1954, Proceedings of the Royal Society of London. Series A. Mathematical and Physical Sciences.

[30]  J. Ramsay,et al.  Strain variation in shear belts , 1970 .

[31]  C. J. Harland,et al.  Electron back-scattering patterns—A new technique for obtaining crystallographic information in the scanning electron microscope , 1973 .

[32]  D. Davidson Uses of electron channelling in studying material deformation , 1984 .