Physicochemical Properties and Surfaces Morphologies Evaluation of MTA FillApex and AH Plus

The solubility, pH, electrical conductivity, and radiopacity of AH Plus and MTA FillApex were evaluated. In addition, the surfaces morphologies of the sealers were analyzed by using scanning electron microscopy. For pH test, the samples were immersed in distilled water at different periods of time. The same solution was used for electrical conductivity measurement. The solubility and radiopacity were evaluated according to ANSI/ADA. Statistical analyses were carried out at 5% level of significance. MTA FillApex presented higher mean value for solubility and electrical conductivity. No significant difference was observed in the mean values for pH reading. AH Plus presented higher radiopacity mean values. MTA FillApex presented an external surface with porosities and a wide range of sizes. In conclusion, the materials fulfill the ANSI/ADA requirements when considering the radiopacity and solubility. AH Plus revealed a compact and homogeneous surface with more regular aspects and equal particle sizes.

[1]  J. Guerreiro-Tanomaru,et al.  Physicochemical and mechanical properties of zirconium oxide and niobium oxide modified Portland cement-based experimental endodontic sealers. , 2014, International endodontic journal.

[2]  E. Piva,et al.  Chemical-physical properties of experimental root canal sealers based on butyl ethylene glycol disalicylate and MTA. , 2013, Dental materials : official publication of the Academy of Dental Materials.

[3]  Ya Shen,et al.  Physical properties of 5 root canal sealers. , 2013, Journal of endodontics.

[4]  Emmanuel João Nogueira Leal Silva,et al.  Physical properties of MTA Fillapex sealer. , 2013, Journal of endodontics.

[5]  N. Tani-Ishii,et al.  Evaluation of the biocompatibility of resin-based root canal sealers in rat periapical tissue. , 2013, Dental materials journal.

[6]  B. Gomes,et al.  Evaluation of cytotoxicity and physicochemical properties of calcium silicate-based endodontic sealer MTA Fillapex. , 2013, Journal of endodontics.

[7]  C. Bourauel,et al.  3D analyses of interface voids in root canals filled with different sealer materials in combination with warm gutta-percha technique , 2013, Clinical Oral Investigations.

[8]  C. R. Sipert,et al.  In vitro cytotoxicity of white MTA, MTA Fillapex® and Portland cement on human periodontal ligament fibroblasts. , 2013, Brazilian dental journal.

[9]  L. Â. Cintra,et al.  Rat tissue reaction to MTA FILLAPEX®. , 2012, Dental traumatology : official publication of International Association for Dental Traumatology.

[10]  J. V. Baldi,et al.  Variability of physicochemical properties of an epoxy resin sealer taken from different parts of the same tube. , 2012, International endodontic journal.

[11]  J. D. PÉcora,et al.  Characterization of calcium oxide in root perforation sealer materials. , 2012, Brazilian dental journal.

[12]  D. Grana,et al.  Reaction of rat subcutaneous connective tissue to a mineral trioxide aggregate-based and a zinc oxide and eugenol sealer. , 2012, Journal of endodontics.

[13]  S. Báo,et al.  Mineral trioxide aggregate-based endodontic sealer stimulates hydroxyapatite nucleation in human osteoblast-like cell culture. , 2012, Journal of endodontics.

[14]  K. Wrbas,et al.  Comparison between two thermoplastic root canal obturation techniques regarding extrusion of root canal filling—a retrospective in vivo study , 2012, Clinical Oral Investigations.

[15]  J. D. PÉcora,et al.  Changes in the surface of four calcium silicate-containing endodontic materials and an epoxy resin-based sealer after a solubility test. , 2012, International endodontic journal.

[16]  J. Granjeiro,et al.  A multiparametric assay to compare the cytotoxicity of endodontic sealers with primary human osteoblasts. , 2012, International endodontic journal.

[17]  R. D. Morgental,et al.  Antibacterial activity of two MTA-based root canal sealers. , 2011, International endodontic journal.

[18]  I. G. Moraes,et al.  Physical properties and interfacial adaptation of three epoxy resin-based sealers. , 2011, Journal of endodontics.

[19]  M. Sousa-Neto,et al.  Physicochemical properties of methacrylate resin-based root canal sealers. , 2010, Journal of endodontics.

[20]  Á. Borges,et al.  Evaluation of physico-chemical properties of Portland cements and MTA. , 2010, Brazilian oral research.

[21]  M. Sousa-Neto,et al.  Laboratory evaluation of the physicochemical properties of a new root canal sealer based on Copaifera multijuga oil-resin. , 2010, International endodontic journal.

[22]  D. Ørstavik,et al.  A laboratory assessment of coronal bacterial leakage in root canals filled with new and conventional sealers. , 2009, International endodontic journal.

[23]  L. Correr-Sobrinho,et al.  Solubility and dimensional change after setting of root canal sealers: a proposal for smaller dimensions of test samples. , 2007, Journal of endodontics.

[24]  F. Tay,et al.  Water sorption and solubility of methacrylate resin-based root canal sealers. , 2007, Journal of endodontics.

[25]  J. Camilleri Hydration mechanisms of mineral trioxide aggregate. , 2007, International endodontic journal.

[26]  M. Tanomaru-Filho,et al.  Radiopacity evaluation of new root canal filling materials by digitalization of images. , 2007, Journal of endodontics.

[27]  R. Frankenberger,et al.  Influence of moisture on the apical seal of root canal fillings with five different types of sealer. , 2007, Journal of endodontics.

[28]  E. Araújo,et al.  Physico-chemical properties of MTA and a novel experimental cement. , 2005, International endodontic journal.

[29]  M. Fridland,et al.  Mineral trioxide aggregate (MTA) solubility and porosity with different water-to-powder ratios. , 2003, Journal of endodontics.

[30]  M. Kuga,et al.  pH and calcium ion release of 2 root-end filling materials. , 2003, Oral surgery, oral medicine, oral pathology, oral radiology, and endodontics.

[31]  K. Safavi,et al.  Adhesion of human osteoblasts on root-end filling materials. , 2000, Journal of endodontics.

[32]  J. D. PÉcora,et al.  Evaluation of dentin root canal permeability after instrumentation and Er:YAG laser application , 2000, Lasers in surgery and medicine.