Phase Formation and Evaluation of Calcium Phosphate Ceramics Using Eggshell Waste

ALCIUM phosphate ceramics are considered as a family of the ……most important bio-inorganic materials used in biomedical applications. Calcium phosphates were prepared from eggshell waste and phosphoric acid after cleaning eggshell precursor and converting it to calcium oxide by calcination. The phases obtained from such reaction were dependent not only on the weight ratio of calcined eggshell powder and phosphoric acid (Ca/P) but also on the calcination temperature of the obtained mixture. Effects of Ca/P ratio and calcination temperature were studied and the phases obtained were evaluated using X-Ray Diffraction spectroscopy (XRD) and Scanning Electron Microscopy (SEM).

[1]  S. Ramesh,et al.  Sintering and mechanical properties of MgO-doped nanocrystalline hydroxyapatite , 2013 .

[2]  Hsueh-Chuan Hsu,et al.  A hydrothermal synthesis of eggshell and fruit waste extract to produce nanosized hydroxyapatite , 2013 .

[3]  E. Domashevskaya,et al.  Synthesis of nanocrystalline hydroxyapatite by precipitation using hen's eggshell , 2013 .

[4]  S. Prabu,et al.  Thermal stability of nano hydroxyapatite synthesized from sea shells through wet chemical synthesis , 2013 .

[5]  Jiang Chang,et al.  Fabrication of Dense Hydroxyapatite Nanobioceramics with Enhanced Mechanical Properties via Two-Step Sintering Process , 2012 .

[6]  S. Ramesh,et al.  Sintering behavior of hydroxyapatite prepared from different routes , 2012 .

[7]  M. Lavine,et al.  Biomaterials. Introduction. , 2012, Science.

[8]  Ya-Jun Guo,et al.  Fabrication of mesoporous carbonated hydroxyapatite microspheres by hydrothermal method , 2011 .

[9]  M. Chu,et al.  Sol–gel synthesis and characterization of hydroxyapatite nanorods , 2009 .

[10]  K. Zhou,et al.  Plate-like hydroxyapatite nanoparticles synthesized by the hydrothermal method , 2009 .

[11]  Y. Yoon,et al.  Highly sinterable β-tricalcium phosphate synthesized from eggshells , 2007 .

[12]  A. Rebelo,et al.  Novel synthesis and structural characterization of fluorine and chlorine co-substituted hydroxyapatites. , 2006, Journal of inorganic biochemistry.

[13]  T. Sakae Variations in Dental Enamel Crystallites and Micro-Structure , 2006 .

[14]  N. Mostafa Characterization, thermal stability and sintering of hydroxyapatite powders prepared by different routes , 2005 .

[15]  W. Feng,et al.  A simple sol–gel technique for preparing hydroxyapatite nanopowders , 2005 .

[16]  F. Driessens,et al.  Biological calcium phosphates and their role in the physiology of bone and dental tissues I. Composition and solubility of calcium phosphates , 1978, Calcified Tissue Research.

[17]  A. Shpak,et al.  Electronic structure of isomorphically substituted strontium apatite , 2004 .

[18]  Anna Tampieri,et al.  Carbonated hydroxyapatite as bone substitute , 2003 .

[19]  D S Metsger,et al.  Mechanical properties of sintered hydroxyapatite and tricalcium phosphate ceramic. , 1999, Journal of materials science. Materials in medicine.

[20]  A. Senos,et al.  Wet synthesis and characterization of modified hydroxyapatite powders , 1996 .

[21]  M. Glimcher Molecular Biology of Mineralized Tissues with Particular Reference to Bone , 1959 .