Temperature effects on the ultrasonic separation of fat from natural whole milk.

This study showed that temperature influences the rate of separation of fat from natural whole milk during application of ultrasonic standing waves. In this study, natural whole milk was sonicated at 600kHz (583W/L) or 1MHz (311W/L) with a starting bulk temperature of 5, 25, or 40°C. Comparisons on separation efficiency were performed with and without sonication. Sonication using 1MHz for 5min at 25°C was shown to be more effective for fat separation than the other conditions tested with and without ultrasound, resulting in a relative change from 3.5±0.06% (w/v) fat initially, of -52.3±2.3% (reduction to 1.6±0.07% (w/v) fat) in the skimmed milk layer and 184.8±33.2% (increase to 9.9±1.0% (w/v) fat) in the top layer, at an average skimming rate of ∼5g fat/min. A shift in the volume weighted mean diameter (D[4,3]) of the milk samples obtained from the top and bottom of between 8% and 10% relative to an initial sample D[4,3] value of 4.5±0.06μm was also achieved under these conditions. In general, faster fat separation was seen in natural milk when natural creaming occurred at room temperature and this separation trend was enhanced after the application of high frequency ultrasound.

[1]  M. Villamiel,et al.  Influence of high-intensity ultrasound and heat treatment in continuous flow on fat, proteins, and native enzymes of milk. , 2000, Journal of agricultural and food chemistry.

[2]  Muthupandian Ashokkumar,et al.  Modification of food ingredients by ultrasound to improve functionality: A preliminary study on a model system , 2008 .

[3]  P. Walstra,et al.  The milk fat globule: Emulsion science as applied to milk products and comparable foods , 1974 .

[4]  T. Richardson,et al.  Antioxidant activity of skim milk: effect of sonication. , 1980, Journal of dairy science.

[5]  H. J.,et al.  Hydrodynamics , 1924, Nature.

[6]  Pablo Juliano,et al.  Impact of ultrasound treatment on lipid oxidation of Cheddar cheese whey. , 2014, Ultrasonics sonochemistry.

[7]  P. Juliano,et al.  Design parameters for the separation of fat from natural whole milk in an ultrasonic litre-scale vessel. , 2014, Ultrasonics sonochemistry.

[8]  Timothy J. Mason,et al.  Dosimetry in sonochemistry : The use of aqueous terephthalate ion as a fluorescence monitor , 1994 .

[9]  K. Yosioka,et al.  Acoustic radiation pressure on a compressible sphere , 1955 .

[10]  Aniruddha B. Pandit,et al.  Sonochemical reactors: important design and scale up considerations with a special emphasis on heterogeneous systems , 2011 .

[11]  D M Barbano,et al.  Gravity separation of fat, somatic cells, and bacteria in raw and pasteurized milks. , 2013, Journal of dairy science.

[12]  H. Lindmark-Månsson,et al.  Antioxidative factors in milk , 2000, British Journal of Nutrition.

[13]  Hideto Mitome,et al.  A standard method to calibrate sonochemical efficiency of an individual reaction system. , 2003, Ultrasonics sonochemistry.

[14]  P. Juliano,et al.  Ultrasonic Separation of Particulate Fluids in Small and Large Scale Systems: A Review , 2013 .

[15]  P. Juliano,et al.  Enhanced creaming of milk fat globules in milk emulsions by the application of ultrasound and detection by means of optical methods. , 2011, Ultrasonics sonochemistry.

[16]  T. Leighton The Acoustic Bubble , 1994 .

[17]  M. Michalski,et al.  Apparent ζ-potential as a tool to assess mechanical damages to the milk fat globule membrane , 2002 .

[18]  Jayani Chandrapala,et al.  Effects of ultrasound on the thermal and structural characteristics of proteins in reconstituted whey protein concentrate. , 2011, Ultrasonics sonochemistry.

[19]  D M Barbano,et al.  Gravity separation of raw bovine milk: fat globule size distribution and fat content of milk fractions. , 2000, Journal of dairy science.

[20]  Piotr Swiergon,et al.  Creaming enhancement in a liter scale ultrasonic reactor at selected transducer configurations and frequencies. , 2013, Ultrasonics sonochemistry.