Major advances in testing of dairy products: milk component and dairy product attribute testing.

Milk component analysis is relatively unusual in the field of quantitative analytical chemistry because an analytical test result determines the allocation of very large amounts of money between buyers and sellers of milk. Therefore, there is high incentive to develop and refine these methods to achieve a level of analytical performance rarely demanded of most methods or laboratory staff working in analytical chemistry. In the last 25 yr, well-defined statistical methods to characterize and validate analytical method performance combined with significant improvements in both the chemical and instrumental methods have allowed achievement of improved analytical performance for payment testing. A shift from marketing commodity dairy products to the development, manufacture, and marketing of value added dairy foods for specific market segments has created a need for instrumental and sensory approaches and quantitative data to support product development and marketing. Bringing together sensory data from quantitative descriptive analysis and analytical data from gas chromatography olfactometry for identification of odor-active compounds in complex natural dairy foods has enabled the sensory scientist and analytical chemist to work together to improve the consistency and quality of dairy food flavors.

[1]  P. Griffiths Fourier Transform Infrared Spectrometry , 2007 .

[2]  David M. Barbano,et al.  Crude and Protein Nitrogen Bases for Protein Measurement and Their Impact on Current Testing Accuracy , 1992 .

[3]  Harry T. Lawless,et al.  Sensory Evaluation of Food: Principles and Practices , 1998 .

[4]  M. Drake,et al.  Aroma-active Components of Liquid Cheddar Whey , 2003 .

[5]  W. Horwitz Official Methods of Analysis , 1980 .

[6]  H. Lawless,et al.  Validity of Descriptive and Defect‐oriented Terminology Systems for Sensory Analysis of Fluid Milk , 1993 .

[7]  D. Barbano,et al.  Kjeldahl method for determination of total nitrogen content of milk: collaborative study. , 1990 .

[8]  Leonard Steinborn,et al.  International Organization for Standardization ISO/IEC 17025 General Requirements for the Competence of Testing and Calibration Laboratories , 2004 .

[9]  D. Mckenna 4. Standardization in cheese plants. , 2000 .

[10]  Kenneth Helrick,et al.  Official methods of analysis , 1990 .

[11]  D. Barbano,et al.  Effectiveness of temperature modification in decreasing the bias in milk fat test results between the Babcock and Ether extraction methods. , 2003, Journal of AOAC International.

[12]  P. V. Soest,et al.  Composition and aroma compounds of Ragusano cheese: native pasture and total mixed rations. , 2004, Journal of dairy science.

[13]  D. Barbano,et al.  Direct determination of true protein content of milk by Kjeldahl analysis: collaborative study. , 1991 .

[14]  P. V. Soest,et al.  Contribution of native pasture to the sensory properties of Ragusano cheese. , 2004, Journal of dairy science.

[15]  Terry E. Acree,et al.  A Procedure for the Sensory Analysis of Gas Chromatographic Effluents , 1984 .

[16]  Patrick D. Gerard,et al.  Development of a Descriptive Language for Cheddar Cheese , 2001 .

[17]  D. Barbano,et al.  Kjeldahl nitrogen analysis as a reference method for protein determination in dairy products. , 1999, Journal of AOAC International.

[18]  D. Barbano,et al.  Comparison of Babcock and ether extraction methods for determination of fat content of milk: collaborative study. , 1988, Journal - Association of Official Analytical Chemists.

[19]  D. Barbano,et al.  Indirect and direct determination of the casein content of milk by Kjeldahl nitrogen analysis: collaborative study. , 1998, Journal of AOAC International.

[20]  J. L. Clark,et al.  Infrared Milk Analysis — Challenges for the Future , 1989 .

[21]  D. Barbano,et al.  Performance evaluation of direct forced-air total solids and Kjeldahl total nitrogen methods: 1990 through 1995. , 1997, Journal of AOAC International.