Quick-EXAFS setup at the SuperXAS beamline for in situ X-ray absorption spectroscopy with 10 ms time resolution

A new quick-scanning EXAFS (QEXAFS) monochromator, ionization chambers and data acquisition system have been developed and installed at the SuperXAS beamline at the Swiss Light Source to reach a temporal resolution of 10 ms.

[1]  D Lützenkirchen-Hecht,et al.  Gridded Ionization Chambers for Time Resolved X-Ray Absorption Spectroscopy , 2013 .

[2]  T. Uruga,et al.  In situ observation of nucleation and growth process of gold nanoparticles by quick XAFS spectroscopy. , 2011, Chemphyschem : a European journal of chemical physics and physical chemistry.

[3]  Rakesh Agrawal,et al.  Fabrication of 7.2% efficient CZTSSe solar cells using CZTS nanocrystals. , 2010, Journal of the American Chemical Society.

[4]  D. Lützenkirchen-Hecht,et al.  QEXAFS and UV/Vis Simultaneous Monitoring of the TiO2-Nanoparticles Formation by Hydrolytic Sol−Gel Route , 2010 .

[5]  K. Ryan,et al.  Complete study of the composition and shape evolution in the synthesis of Cu2ZnSnS4 (CZTS) semiconductor nanocrystals , 2015 .

[6]  P. Eisenberger,et al.  Extended x-ray absorption fine structure—its strengths and limitations as a structural tool , 1981 .

[7]  D. Lützenkirchen-Hecht,et al.  A new flexible monochromator setup for quick scanning x-ray absorption spectroscopy. , 2010, The Review of scientific instruments.

[8]  D Lützenkirchen-Hecht,et al.  Quick scanning monochromator for millisecond in situ and in operando X-ray absorption spectroscopy. , 2015, The Review of scientific instruments.

[9]  Rommel Noufi,et al.  The state and future prospects of kesterite photovoltaics , 2013 .

[10]  H.W. Kraner,et al.  Radiation detection and measurement , 1981, Proceedings of the IEEE.

[11]  R. Frahm,et al.  Quick scanning exafs: First experiments , 1988 .

[12]  Uwe Bergmann,et al.  X-ray damage to the Mn4Ca complex in single crystals of photosystem II: a case study for metalloprotein crystallography. , 2005, Proceedings of the National Academy of Sciences of the United States of America.

[13]  J. Rehr,et al.  Theoretical approaches to x-ray absorption fine structure , 2000 .

[14]  J. Grunwaldt,et al.  Operando spatially and time-resolved X-ray absorption spectroscopy and infrared thermography during oscillatory CO oxidation , 2015 .

[15]  S. Belin,et al.  The SAMBA quick-EXAFS monochromator: XAS with edge jumping. , 2012, Journal of synchrotron radiation.

[16]  J. Grunwaldt,et al.  The dedicated QEXAFS facility at the SLS: Performance and Scientific Opportunities , 2010 .

[17]  John J. Rehr,et al.  Sensitivity of Pt x-ray absorption near edge structure to the morphology of small Pt clusters , 2002 .

[18]  R. Frahm.  New method for time dependent x-ray absorption studies , 1989 .

[19]  G. Knoll.  Radiation Detection And Measurement, 3rd Ed , 2009 .

[20]  Supratik Guha,et al.  Thin film solar cell with 8.4% power conversion efficiency using an earth‐abundant Cu2ZnSnS4 absorber , 2013 .

[21]  J. Szlachetko,et al.  High energy resolution off-resonant spectroscopy for x-ray absorption spectra free of self-absorption effects. , 2014, Physical review letters.

[22]  C. David,et al.  Communication: The electronic structure of matter probed with a single femtosecond hard x-ray pulse , 2014, Structural dynamics.

[23]  T Uruga,et al.  Quick-scanning x-ray absorption spectroscopy system with a servo-motor-driven channel-cut monochromator with a temporal resolution of 10 ms. , 2012, The Review of scientific instruments.

[24]  S. Ted Oyama,et al.  Transient Technique for Identification of True Reaction Intermediates: Hydroperoxide Species in Propylene Epoxidation on Gold/Titanosilicate Catalysts by X-ray Absorption Fine Structure Spectroscopy , 2008 .

[25]  Olivier Mathon,et al.  Advances in high brilliance energy dispersive X-ray absorption spectroscopy. , 2010, Physical chemistry chemical physics : PCCP.

[26]  K. Ryan,et al.  Colloidal synthesis of wurtzite Cu2ZnSnS4 nanorods and their perpendicular assembly. , 2012, Journal of the American Chemical Society.