Process Sequence Development for Automated Progressive Freeze Concentration System

Nowadays there is a growing interest on Progressive Freeze Concentration (PFC) in solution concentration process due to its several significant advantages. The PFC process is proven to be able to be applied successfully in industrial application. PFC often exhibits a dynamic character and involves complex behavior and process. Even a slight change in the operating condition can cause unstable process behavior and lead to low performance of the system. Due to these reasons, the objective of this paper is to develop a sequence for conducting PFC process. In order to develop the process sequence, it has been divided into four major steps which are feeding process, crystallization process, Product 1 collection and Product 2 collection.  This system offers improved overall performance in conducting experiments as well as increased efficiency of the separation process.

[1]  Shigeru Sakashita,et al.  Ice crystallization in a pilot-scale freeze wastewater treatment system , 2001 .

[2]  O. Lorain,et al.  Potential of freezing in wastewater treatment: soluble pollutant applications. , 2001, Water research.

[3]  J. Sanchez,et al.  Review. Freeze Concentration in the Fruit Juices Industry , 2009 .

[4]  Kozo Nakamura,et al.  Effective partition constant of solute between ice and liquid phases in progressive freeze-concentration , 1998 .

[5]  M. Farid,et al.  Freeze concentration of milk and saline solutions in a liquid–solid fluidized bed: Part I. Experimental , 2007 .

[6]  D. K. Salunkhe,et al.  Freeze concentration of fruit juices. , 1984, Critical reviews in food science and nutrition.

[7]  P. Englezos,et al.  The Freeze Concentration Process and its Applications , 2008 .

[8]  A. Ibarz,et al.  Concentration of aqueous sugar solutions in a multi-plate cryoconcentrator , 2007 .

[9]  S. Veesler,et al.  Sea water desalination by dynamic layer melt crystallization: Parametric study of the freezing and sweating steps , 2012 .

[10]  Mohammed Aider,et al.  Cryoconcentration technology in the bio-food industry: principles and applications. , 2009 .

[11]  Rolf Halde Concentration of impurities by progressive freezing , 1980 .

[12]  J. R. Alvarez,et al.  A comparative study of reverse osmosis and freeze concentration for the removal of valeric acid from wastewaters , 2000 .

[13]  O. Miyawaki,et al.  Tubular ice system for scale-up of progressive freeze-concentration , 2005 .

[14]  E. Hernández,et al.  Calculation method for designing a multi-plate freeze-concentrator for concentration of fruit juices , 2011 .

[15]  F. Jona,et al.  Physics of Ice , 1972 .

[16]  Richard W. Hartel,et al.  Evaporation and Freeze Concentration , 2006, Handbook of Food Engineering.

[17]  N. Coggeshall,et al.  Concentration of Impurities from Organic Compounds by Progressive Freezing , 1959 .

[18]  K. Free,et al.  Solute inclusion in ice formed from sucrose solutions on a sub-cooled surface—an experimental study , 1998 .

[19]  K. Maeda,et al.  Freeze-thawing as a path to concentrate aqueous solution , 2010 .

[20]  J. Aguilera,et al.  Vacuum-assisted freeze concentration of sucrose solutions , 2013 .

[21]  Y. Shirai,et al.  Conditions of producing an ice layer with high purity for freeze wastewater treatment , 1998 .

[22]  C. Duque,et al.  Changes in volatiles with the application of progressive freeze-concentration to Andes berry (Rubus glaucus Benth) , 2005 .

[23]  J. Sanchez,et al.  Freeze concentration of whey in a falling-film based pilot plant: process and characterization , 2011 .

[24]  Kozo Nakamura,et al.  Progressive Freeze-Concentration of Model Liquid Food , 1997 .