Rapid determination of quinolones in cosmetic products by ultra high performance liquid chromatography with tandem mass spectrometry.

This study developed an improved analytical method for the simultaneous quantification of 13 quinolones in cosmetics by ultra high performance liquid chromatography combined with ESI triple quadrupole MS/MS under the multiple reaction monitoring mode. The analytes were extracted and purified by using an SPE cartridge. The limits of quantification ranged from 0.03 to 3.02 μg/kg. The precision for determining the quinolones was <19.39%. The proposed method was successfully developed for the determination of quinolones in real cosmetic samples.

[1]  Suyoung Lee,et al.  Development of isotope dilution-liquid chromatography tandem mass spectrometry for the accurate determination of fluoroquinolones in animal meat products: optimization of chromatographic separation for eliminating matrix effects on isotope ratio measurements. , 2013, Journal of chromatography. A.

[2]  V. Samanidou,et al.  HPLC confirmatory method development for the determination of seven quinolones in salmon tissue (Salmo salar L.) validated according to the European Union Decision 2002/657/EC. , 2013, Food chemistry.

[3]  Yan-Wen Li,et al.  Determination of Quinolones in Vegetables Using Ultra Performance Liquid Chromatography-Electrospray Ionization Tandem Mass Spectrometry , 2013 .

[4]  A. Zafra-Gómez,et al.  Simultaneous determination of 13 quinolone antibiotic derivatives in wastewater samples using solid‐phase extraction and ultra performance liquid chromatography–tandem mass spectrometry , 2013 .

[5]  M. Llompart,et al.  Determination of isothiazolinone preservatives in cosmetics and household products by matrix solid-phase dispersion followed by high-performance liquid chromatography-tandem mass spectrometry. , 2012, Journal of chromatography. A.

[6]  J. Guiteras,et al.  Analysis of quinolone antibiotics in eggs: preparation and characterization of a raw material for method validation and quality control. , 2012, Food chemistry.

[7]  M. Prat,et al.  Analysis of fluoroquinolones in animal feeds by liquid chromatography with fluorescence detection. , 2012, Journal of separation science.

[8]  I. Kwon,et al.  Quantitative monitoring of corticosteroids in cosmetic products manufactured in Korea using LC-MS/MS. , 2012, Forensic science international.

[9]  H. Hamdi,et al.  Assessment of the genotoxicity of quinolone and fluoroquinolones contaminated soil with the Vicia faba micronucleus test. , 2012, Ecotoxicology and environmental safety.

[10]  R. Burakham,et al.  Signal Derivatization for HPLC Analysis of Fluoroquinolone Antibiotic Residues in Milk Products , 2012, Chromatographia.

[11]  A. Leung,et al.  Residues of fluoroquinolones in marine aquaculture environment of the Pearl River Delta, South China , 2012, Environmental Geochemistry and Health.

[12]  J. I. Rader,et al.  Rapid and simultaneous determination of hexapeptides (Ac-EEMQRR-amide and H2N-EEMQRR-amide) in anti-wrinkle cosmetics by hydrophilic interaction liquid chromatography-solid phase extraction preparation and hydrophilic interaction liquid chromatography with tandem mass spectrometry. , 2011, Journal of chromatography. A.

[13]  Antonio V. Herrera-Herrera,et al.  Determination of quinolone residues in infant and young children powdered milk combining solid-phase extraction and ultra-performance liquid chromatography-tandem mass spectrometry. , 2011, Journal of chromatography. A.

[14]  Yan Liu,et al.  Trace detection of hormones and sulfonamides in viscous cosmetic products by neutral desorption extractive electrospray ionization tandem mass spectrometry. , 2011, Journal of mass spectrometry : JMS.

[15]  N. Leepipatpiboon,et al.  Simultaneous determination of multi-class antibiotic residues in water using carrier-mediated hollow-fiber liquid-phase microextraction coupled with ultra-high performance liquid chromatography tandem mass spectrometry , 2011 .

[16]  Y. Vásquez-Martínez,et al.  VALIDATION OF A LIQUID CHROMATOGRAPHY-FLUORESCENCE SPECTROMETRIC METHOD FOR THE QUANTIFICATION OF FOUR QUINOLONES IN PIG AND CHICKEN MUSCLE FOLLOWING THE EUROPEAN UNION GUIDELINE EC/657/2002 , 2011 .

[17]  R. Galarini,et al.  Simultaneous determination of eleven quinolones in animal feed by liquid chromatography with fluorescence and ultraviolet absorbance detection. , 2009, Journal of chromatography. A.

[18]  J A Lemus,et al.  Fatal embryo chondral damage associated with fluoroquinolones in eggs of threatened avian scavengers. , 2009, Environmental pollution.

[19]  T. Ding,et al.  Rapid determination of 19 quinolone residues in spiked fish and pig muscle by high-performance liquid chromatography (HPLC) tandem mass spectrometry , 2009, Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment.

[20]  Yiping Ren,et al.  Simultaneous determination of (fluoro)quinolones antibacterials residues in bovine milk using ultra performance liquid chromatography-tandem mass spectrometry. , 2009, Journal of pharmaceutical and biomedical analysis.

[21]  V. Zaragoza,et al.  Dermatitis alérgica de contacto por cosméticos , 2009 .

[22]  Jianying Hu,et al.  Trace analysis of quinolone and fluoroquinolone antibiotics from wastewaters by liquid chromatography-electrospray tandem mass spectrometry. , 2008, Journal of chromatography. A.

[23]  Jianying Hu,et al.  Multi-class confirmatory method for analyzing trace levels of tetracyline and quinolone antibiotics in pig tissues by ultra-performance liquid chromatography coupled with tandem mass spectrometry. , 2007, Rapid communications in mass spectrometry : RCM.

[24]  Jianying Hu,et al.  Quantitative structure-activity relationship model for prediction of genotoxic potential for quinolone antibacterials. , 2007, Environmental science & technology.

[25]  Sushil K. Khetan,et al.  Human pharmaceuticals in the aquatic environment: a challenge to Green Chemistry. , 2007, Chemical reviews.

[26]  I. Pecorelli,et al.  Simultaneous determination of 13 quinolones from feeds using accelerated solvent extraction and liquid chromatography , 2003 .

[27]  R. Stahlmann Children as a special population at risk – quinolones as an example for xenobiotics exhibiting skeletal toxicity , 2002, Archives of Toxicology.

[28]  D. Hooper Clinical applications of quinolones. , 1998, Biochimica et biophysica acta.

[29]  Alfredo C. Alder,et al.  Identification of fluoroquinolone antibiotics as the main source of umuC genotoxicity in native hospital wastewater , 1998 .

[30]  D. Volmer,et al.  Study of 4-quinolone antibiotics in biological samples by short-column liquid chromatography coupled with electrospray ionization tandem mass spectrometry. , 1997, Analytical chemistry.