Rigorous dynamics and control of continuous distillation systems—simulation and experimental results

Abstract The scope of this article is to focus the role of rigorous dynamic modeling and to present a simulation tool for multicomponent distillation columns. Comparisons between predicted dynamic profiles and available experimental results confirm that such kind of packages, based on rigorous dynamics, can nowadays be of real and practical value for engineering purposes. A short review of different applications of the DYCODIS program in a wide range of design and operating problems is also presented, namely: 1. — a general time domain approach to verify dynamic interactions among different control loops; 2. — the dynamic behavior of a superfractionator with a very large time delay; 3. — the dynamic stability analysis of multiple steady-states both for heterogeneous columns and interlinked distillation systems. In all these proposed examples, the program showed itself to be useful, reliable, robust and manageable with regard to both control synthesis or process analysis purposes.

[1]  Dale E. Seborg,et al.  Analysis of process interactions with applications to multiloop control system design , 1982 .

[2]  Thomas J. McAvoy,et al.  Some results on dynamic interaction analysis of complex control systems , 1983 .

[3]  Warren D. Seider,et al.  Feasible specifications in azeotropic distillation , 1983 .

[4]  Björn D. Tyréus Multivariable Control System Design for an Industrial Distillation Column , 1979 .

[5]  Angelo Lucia,et al.  Solving distillation problems by Newton-like methods , 1988 .

[6]  J. Gmehling Vapor-Liquid Equilibrium Data Collection , 1977 .

[7]  M. Rovaglio,et al.  Role of energy balances in dynamic simulation of multicomponent distillation columns , 1988 .

[8]  C. D. Holland,et al.  Development and comparison of a generalized semi-implicit Runge-Kutta method with Gear's method for systems of coupled differential and algebraic equations , 1984 .

[9]  T. L. Wayburn,et al.  Multiple steady-state solutions for interlinked separation systems , 1986 .

[10]  Rafiqul Gani,et al.  A generalized model for distillation columns—I: Model description and applications , 1986 .

[11]  F. Petlyuk Thermodynamically Optimal Method for Separating Multicomponent Mixtures , 1965 .

[12]  E. Bristol On a new measure of interaction for multivariable process control , 1966 .

[13]  C. D. Holland,et al.  Gear's procedure for the simultaneous solution of differential and algebraic equations with application to unsteady state distillation problems , 1982 .

[14]  Warren D. Seider,et al.  Heterogeneous azeotropic distillation: Experimental and simulation results , 1987 .

[15]  J. D. Seader,et al.  Computing multiple solutions to systems of interlinked separation columns , 1987 .

[16]  Michael F. Doherty,et al.  On the dynamics of distillation processes—I: The simple distillation of multicomponent non-reacting, homogeneous liquid mixtures , 1978 .