Potential Use of Resorcinol-Formaldehyde and Zirconyl - Molybdo Pyrophosphate Ion - Exchange Materials for the Chromatographic Separation of Cesium, Cobalt and Europium Ions
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The distribution coefficient between 134 Cs(I), 60 Co(II) and 152,154 Eu(III) radioisotopes dissolved in HCl acid solution with Resorcinol-Formaldhyde (R-F) and Zirconyl-Molybdopyrophosphate (ZMPP) ion exchangers dried at 50 0 C have been studied using batch technique. The selectivity arrange was found to be Cs(I) Eu(III) Co(II). The capacity of R-F toward CS(I), Eu(III) and Co(II) was found to be 6.37, 2.86 and 1.66 meq/gm of the ion exchanger, respectively. A chromatographic column (0.6cm i.d) of 1 gm R-F exchanger was prepared and loaded with a mixture of (10 -3 M) 134 Cs, 60 Co and 152,154 Eu radioisotopes dissolved in 100 ml HCl acid solution pH = 2.5. Completely sorbent of Cs(I) and Eu(III) take place while only 35% of Co(II) was sorbed on the R-F exchanger. Successive elution of the 35% sorbedCo(II) take place using 12 ml of HCl acid solution pH = 1.2. Elution of Eu(III) required passing 15 ml HCl acid solution pH = 2.5, while removal of Cs(I) from the column need 24ml HCl acid solution (pH = 0.8). R-F ion exchanger is valuable in radioactive waste management and water treatment.
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