Identification of an atypical constitutent of a clandestine opiate
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An unusual morphine analog was extracted and separated from an opium-like sample. The high resolution mass spectrum of the unknown substance confirmed the empirical formula as C17H18O2NCl. Mass spectra and retention factor values in thin-layer chromatography of both unknown and authentic standards were compared, which lead to the identification of the unknown as β-chloromorphide.
[1] K. W. Bentley. The chemistry of the morphine alkaloids , 1954 .