Scanning near-field optical microscope based on double-resonant fiber probe montage and its operation in liquids

The operation of the scanning near-field optical microscope based on the double-resonant montage of a fiber probe onto the tuning fork (working frequency of the latter, that is 32 kHz, coincides with the second resonance frequency of the bending oscillations of the free standing part of a fiber beam) in liquid is reported. It is shown that due to the peculiarities of the probe montage (initially large, around 3,000 - 5,500 quality factor of the dithering and long projection of the fiber beam beyond the tuning fork body) and microscope electronics, this SNOM is very fit to work in liquids. Quality factor of the sensor drops down to the values around 300 - 600 when the probe tip is submerged on the depth of 0.2 - 0.3 mm, thus remaining large enough to enable high quality imaging with rather small acting force value laying in the subnanoNewton region. We also discuss the joint liquid recipient construction which connects the liquid cell containing a sample with the large water reservoir via a flexible tube. This reservoir is placed onto separate Z-stage and hence the water level in the cell can be regulated independently from the sample position which facilitates the SNOM operation a lot.

[1]  V. Letokhov,et al.  Direct measurement of the absolute value of the interaction force between the fiber probe and the sample in a scanning near-field optical microscope , 2002 .

[2]  Fabienne D. Marquis-Weible,et al.  Reduction of tip–sample interaction forces for scanning near-field optical microscopy in a liquid environment , 1998 .

[3]  D. V. SEREBRYAKOV,et al.  Scanning near‐field optical microscope based on a double resonant fibre probe montage and equipped with time‐gated photon detection , 2008, Journal of microscopy.

[4]  Ricardo Garcia,et al.  Dynamic atomic force microscopy methods , 2002 .

[5]  H.-J. Maas,et al.  Dynamic force distance control suited to various probes for scanning near-field optical microscopy , 1999 .

[6]  Kunio Nakajima,et al.  Near‐field optical microscopy in liquids , 1995 .

[7]  S. Kämmer,et al.  High‐resolution imaging using near‐field scanning optical microscopy and shear force feedback in water , 1996 .

[8]  N. F. van Hulst,et al.  Imaging soft samples in liquid with tuning fork based shear force microscopy , 2000 .

[9]  Din Ping Tsai,et al.  Tapping-mode tuning fork force sensing for near-field scanning optical microscopy , 1998 .

[10]  V. Letokhov,et al.  Double-resonance probe for near-field scanning optical microscopy , 2006 .

[11]  C. Höppener,et al.  High-resolution near-field optical imaging of single nuclear pore complexes under physiological conditions. , 2005, Biophysical journal.

[12]  N. F. van Hulst,et al.  Shear force imaging of soft samples in liquid using a diving bell concept , 2003 .