Advances in fabrication of X-ray waveguides

This paper reports on the fabrication of X-ray waveguides, manufactured by e-beam lithography, reactive ion etching and wafer bonding techniques. By combination of these processing steps, long empty (air) channels with cross-sections in the range of 10 to 100nm are obtained, forming a guiding layer, surrounded by a solid state cladding. Aside from silicon, we present also waveguide channels fabricated in germanium and quartz. The improved fabrication protocols lead to significantly enhanced exit flux for imaging applications. Finally, we address not only straight channels, but a large variety of various geometries, as required for different applications. Display Omitted X-ray waveguides were fabricated by e-beam lithography, reactive ion etching and wafer bonding techniquesThe fabrication process was optimized for Si, leading to an enhanced optical performance and then transferred to Ge and SiO2A variety of channel geometries was realized such as straight and curved channels, gratings, beamsplitters

[1]  Manuel Guizar-Sicairos,et al.  Kinoform diffractive lenses for efficient nano-focusing of hard X-rays. , 2014, Optics express.

[2]  C. Riekel,et al.  Submicrometer x‐ray beam production by a thin film waveguide , 1996 .

[3]  T. Salditt,et al.  Waveguide-based off-axis holography with hard X rays. , 2006, Physical review letters.

[4]  Coherent Propagation of X Rays in a Planar Waveguide with a Tunable Air Gap , 1999 .

[5]  T. Salditt,et al.  Miniaturized beamsplitters realized by X-ray waveguides. , 2016, Acta crystallographica. Section A, Foundations and advances.

[6]  G. Schmahl,et al.  High power zone plates as image forming systems for soft X-rays. , 1969 .

[7]  E. Spiller,et al.  Propagation of x rays in waveguides , 1974 .

[8]  I. Prudnikov X-ray waveguides based on Bragg scattering of multilayers , 2003 .

[9]  M. Reiche,et al.  Time‐Dependent Surface Properties and Wafer Bonding of O 2 ‐ Plasma ‐ Treated Silicon (100) Surfaces , 2000 .

[10]  Christian G. Schroer,et al.  Hard x-ray nanofocusing by refractive lenses of constant thickness , 2014 .

[11]  B. Lengeler,et al.  A compound refractive lens for focusing high-energy X-rays , 1996, Nature.

[12]  J. Raskin,et al.  Low-temperature wafer bonding: a study of void formation and influence on bonding strength , 2005, Journal of Microelectromechanical Systems.

[13]  Bryan M. Cord,et al.  Optimal temperature for development of poly(methylmethacrylate) , 2007 .

[14]  S. Kalbfleisch,et al.  High aspect ratio x-ray waveguide channels fabricated by e-beam lithography and wafer bonding , 2014 .

[15]  Tim Salditt,et al.  X-ray beam compression by tapered waveguides , 2015 .

[16]  D. Pelliccia,et al.  X-ray waveguides for laboratory sources , 2005 .

[17]  X-Ray Optics on a Chip: Guiding X Rays in Curved Channels. , 2015, Physical review letters.

[18]  F. Pfeiffer,et al.  X-ray waveguides with multiple guiding layers , 2000 .

[19]  Michael Curt Elwenspoek,et al.  Anisotropic reactive ion etching of silicon using SF6/02/CHF3 gas mixtures , 1995 .

[20]  U. Gosele,et al.  Bubble formation during silicon wafer bonding: causes and remedies , 1990, IEEE 4th Technical Digest on Solid-State Sensor and Actuator Workshop.

[21]  Tim Salditt,et al.  Phase-contrast zoom tomography reveals precise locations of macrophages in mouse lungs , 2015, Scientific Reports.

[22]  Werner Langheinrich,et al.  Application of oxygen plasma processing to silicon direct bonding , 1993 .

[23]  J. Golovchenko,et al.  Surface Trapped X Rays: Whispering-Gallery Modes at λ = 0.7 Å , 1997 .

[24]  Michael Sprung,et al.  Compound focusing mirror and X-ray waveguide optics for coherent imaging and nano-diffraction. , 2015, Journal of synchrotron radiation.

[25]  T Salditt,et al.  X-ray holographic imaging of hydrated biological cells in solution. , 2015, Physical review letters.

[26]  B. L. Henke,et al.  X-Ray Interactions: Photoabsorption, Scattering, Transmission, and Reflection at E = 50-30,000 eV, Z = 1-92 , 1993 .

[27]  C. Schroer Focusing hard x rays to nanometer dimensions using Fresnel zone plates , 2006 .

[28]  Tim Salditt,et al.  Real structure effects in X-ray waveguide optics: The influence of interfacial roughness and refractive index profile on the near-field and far-field distribution , 2009 .

[29]  Elina Färm,et al.  Ultra-high resolution zone-doubled diffractive X-ray optics for the multi-keV regime. , 2011, Optics express.

[30]  J. Bongaerts,et al.  Propagation of Coherent X Rays in a Multistep Index X-Ray Waveguide , 2001 .

[31]  M. Reiche,et al.  History and Future of Semiconductor Wafer Bonding , 1995 .

[32]  W. Jung,et al.  Characterization of silicon wafer bonding by observation in transmitted infrared radiation from an extended source , 2000 .