Measurement of temperature in the laser heated diamond anvil cell: comparison between reflective and refractive optics

ABSTRACT In this article we present a direct comparison between reflective (Schwarzschild mirrors) and refractive (achromatic doublets) optics commonly used in spectroradiometric temperature measurements in laser heated diamond anvil cells. Emission spectra are fitted with the Planck's law and are further analysed with the two-colour technique; theoretical simulations are used to compare the temperature measurement accuracy of the two optical systems. The first result obtained is that achromatic doublets with large numerical aperture () produce extensive accuracy errors in the full T range (1500–3000 K). When reduced apertures () are used a good agreement is found with measurements from reflective optics up to 2600 K while systematic differences (around 200 K) appear at higher temperatures. However, these temperature differences cannot explain the discrepancies between the iron melting curves obtained in the past years using laser heated diamond anvil cells.

[1]  O. Mathon,et al.  A laser heating facility for energy-dispersive X-ray absorption spectroscopy. , 2018, The Review of scientific instruments.

[2]  M. Mezouar,et al.  Methodology for in situ synchrotron X-ray studies in the laser-heated diamond anvil cell , 2017 .

[3]  G. Berruyer,et al.  The Time-resolved and Extreme-conditions XAS (TEXAS) facility at the European Synchrotron Radiation Facility: the energy-dispersive X-ray absorption spectroscopy beamline ID24 , 2016, Journal of synchrotron radiation.

[4]  A. Trapananti,et al.  Melting of iron determined by X-ray absorption spectroscopy to 100 GPa , 2015, Proceedings of the National Academy of Sciences.

[5]  Guoyin Shen,et al.  New developments in laser-heated diamond anvil cell with in situ synchrotron x-ray diffraction at High Pressure Collaborative Access Team. , 2015, The Review of scientific instruments.

[6]  A. Salamat,et al.  In situ synchrotron X-ray diffraction in the laser-heated diamond anvil cell: Melting phenomena and synthesis of new materials , 2014 .

[7]  G. Morard,et al.  Melting of Iron at Earth’s Inner Core Boundary Based on Fast X-ray Diffraction , 2013, Science.

[8]  F. Jing,et al.  Melting curves and entropy of fusion of body-centered cubic tungsten under pressure , 2012 .

[9]  H. Mao,et al.  Double-sided laser heating system at HPCAT for in situ x-ray diffraction at high pressures and high temperatures , 2006, Journal of physics. Condensed matter : an Institute of Physics journal.

[10]  M. Mezouar,et al.  Development of a new state-of-the-art beamline optimized for monochromatic single-crystal and powder X-ray diffraction under extreme conditions at the ESRF. , 2005, Journal of synchrotron radiation.

[11]  M. Mezouar,et al.  Double-sided laser heating system for in situ high pressure–high temperature monochromatic x-ray diffraction at the esrf , 2005 .

[12]  L. Benedetti,et al.  Temperature gradients, wavelength-dependent emissivity, and accuracy of high and very-high temperatures measured in the laser-heated diamond cell , 2004 .

[13]  H. Mao,et al.  Nuclear resonant scattering at high pressure and high temperature , 2004 .

[14]  M. Walter,et al.  The effects of chromatic dispersion on temperature measurement in the laser-heated diamond anvil cell , 2004 .

[15]  A. Kavner,et al.  Temperature gradients and evaluation of thermoelastic properties in the synchrotron-based laser-heated diamond cell , 2004 .

[16]  R. Ditz,et al.  Systematics of transition-metal melting , 2001 .

[17]  O. Shimomura,et al.  Construction of laser-heated diamond anvil cell system for in situ x-ray diffraction study at SPring-8 , 2001 .

[18]  S. Sutton,et al.  Laser heated diamond cell system at the Advanced Photon Source for in situ x-ray measurements at high pressure and temperature , 2001 .

[19]  R. Boehler High‐pressure experiments and the phase diagram of lower mantle and core materials , 2000 .

[20]  R. Jeanloz,et al.  Melting criteria and imaging spectroradiometry in laser-heated diamond-cell experiments , 1996, Philosophical Transactions of the Royal Society of London. Series A: Mathematical, Physical and Engineering Sciences.

[21]  Ross,et al.  High-pressure melting curves of alkali halides. , 1996, Physical review. B, Condensed matter.

[22]  J. S. Sweeney,et al.  A laser heating system that stabilizes and controls the temperature : diamond anvil cell applications , 1991 .

[23]  A. Miiller,et al.  Thermal expansion of tungsten in the range 1500–3600 K by a transient interferometric technique , 1990 .

[24]  P. Loubeyre,et al.  The membrane diamond anvil cell: A new device for generating continuous pressure and temperature variations , 1988 .

[25]  A. Jayaraman,et al.  Diamond anvil cell and high-pressure physical investigations , 1983 .

[26]  C. E. Weir,et al.  Infrared Studies in the 1- to 15-Micron Region to 30,000 Atmospheres , 1959, Journal of research of the National Bureau of Standards. Section A, Physics and chemistry.