Mechanical and Tribological Properties of 3D Printed Polyamide 12 and SiC/PA12 Composite by Selective Laser Sintering

Polymeric matrix composites are important to the advancement of industries such as the automobile and medicine industries. In this study, the silicon carbide (SiC) particle-reinforced polyamide12 (PA12) matrix composites were fabricated by selective laser sintering system as well as the pure PA12. The surface topographies, mechanical, and tribological properties were further examined. The results indicated that the friction and wear resistance of the composite were improved compared with the PA12 matrix. The compressive strength increased about 8.5%, shore D hardness increased about 6%. The friction coefficient decreased about 10%, the specific wear rate decreased 20% after adding silicon carbide 10% weight to PA12. The wear mechanisms were also discussed. The deformed asperities on the worn surface can withstand more tangential load, and therefore resulted in lower specific wear rate. It was found that the content of SiC particles on the surface were reduced after friction tests. According to the analysis of SEM, EDS, and FTIR results, the wear mechanisms were considered to be the abrasive and fatigue mode. This type of PA12 matrix composite might be a promising potential in marine and energy applications.

[1]  Mahmoud Yousry Mahmoud Zaghloul,et al.  Developments in polyester composite materials – An in-depth review on natural fibres and nano fillers , 2021, Composite Structures.

[2]  Feifei Yang,et al.  A combined theoretical and experimental approach to model polyamide 12 degradation in selective laser sintering additive manufacturing , 2021, Journal of Manufacturing Processes.

[3]  M. Heitzmann,et al.  Wear behaviour of polymeric materials reinforced with man-made fibres: A comprehensive review about fibre volume fraction influence on wear performance , 2021, Journal of Reinforced Plastics and Composites.

[4]  M. Kästner,et al.  Anisotropic and rate-dependent mechanical properties of 3D printed polyamide 12 - A comparison between selective laser sintering and multi jet fusion , 2021 .

[5]  K. Zhou,et al.  Comparative study on 3D printing of polyamide 12 by selective laser sintering and multi jet fusion , 2021 .

[6]  M. Schagerl,et al.  Thickness dependent anisotropy of mechanical properties and inhomogeneous porosity characteristics in laser-sintered polyamide 12 specimens , 2020 .

[7]  M.A. Hulsen,et al.  Numerical analysis of the crystallization kinetics in SLS , 2020 .

[8]  Wenfeng Hao,et al.  Failure analysis of 3D printed glass fiber/PA12 composite lattice structures using DIC , 2019, Composite Structures.

[9]  Jie Song,et al.  Tribological and mechanical properties of MoS2 enhanced polyamide 12 for selective laser sintering , 2019, Journal of Materials Processing Technology.

[10]  Jesús Rodríguez,et al.  Effect of temperature on the fracture behavior of polyamide 12 and glass-filled polyamide 12 processed by selective laser sintering , 2018, Engineering Fracture Mechanics.

[11]  M. Zaghloul Mechanical properties of linear low-density polyethylene fire-retarded with melamine polyphosphate , 2018, Journal of Applied Polymer Science.

[12]  D. Drummer,et al.  Tribological anisotropy of selective laser sintered PA12 parts , 2018, Polymer Testing.

[13]  Yasser S. Mohamed,et al.  Fatigue and tensile behaviors of fiber-reinforced thermosetting composites embedded with nanoparticles , 2018, Journal of Composite Materials.

[14]  K. Zhou,et al.  Electrical and thermal conductivities of MWCNT/polymer composites fabricated by selective laser sintering , 2018 .

[15]  D. Lin,et al.  A review on additive manufacturing of polymer-fiber composites , 2017 .

[16]  Paolo Ermanni,et al.  Continuous lattice fabrication of ultra-lightweight composite structures , 2017 .

[17]  M. Zaghloul,et al.  Experimental and modeling analysis of mechanical-electrical behaviors of polypropylene composites filled with graphite and MWCNT fillers , 2017 .

[18]  M. Zaghloul,et al.  Influence of flame retardant magnesium hydroxide on the mechanical properties of high density polyethylene composites , 2017 .

[19]  J. Kruth,et al.  Effect of PA12 powder reuse on coalescence behaviour and microstructure of SLS parts , 2017 .

[20]  Jianjun Guo,et al.  Thermal and mechanical properties of polyamide 12/graphene nanoplatelets nanocomposites and parts fabricated by fused deposition modeling , 2017 .

[21]  Liu Hongbo,et al.  Surface modification of carbon fibers and the selective laser sintering of modified carbon fiber/nylon 12 composite powder , 2017 .

[22]  Pulak M. Pandey,et al.  Fabrication of three dimensional open porous regular structure of PA-2200 for enhanced strength of scaffold using selective laser sintering , 2016 .

[23]  Chee Kai Chua,et al.  Effect of surface orientation on the tribological properties of laser sintered polyamide 12 , 2015 .

[24]  Shuping Peng,et al.  Selective laser sintering of β-TCP/nano-58S composite scaffolds with improved mechanical properties , 2015 .

[25]  Chee Kai Chua,et al.  Thermal Influence of CNT on the Polyamide 12 Nanocomposite for Selective Laser Sintering , 2015, Molecules.

[26]  Mo Song,et al.  Influence of carbon nanotubes on the rheology and dynamic mechanical properties of polyamide-12 for laser sintering , 2014 .

[27]  R. Seltzer,et al.  Fatigue crack growth of SLS polyamide 12: Effect of reinforcement and temperature , 2014 .

[28]  D. Marghitu,et al.  Statistical model of nearly complete elastic rough surface contact , 2014 .

[29]  V. E. Beal,et al.  Microstructural and mechanical characterization of PA12/MWCNTs nanocomposite manufactured by selective laser sintering , 2011 .

[30]  Javier Segurado,et al.  Effect of water conditioning on the fracture behavior of PA12 composites processed by selective laser sintering , 2011 .

[31]  Itzhak Green,et al.  On the Modeling of Elastic Contact between Rough Surfaces , 2011 .

[32]  Andrea Gatto,et al.  Mechanical characterisation of PA‐Al2O3 composites obtained by selective laser sintering , 2010 .

[33]  P. McHugh,et al.  Dependence of mechanical properties of polyamide components on build parameters in the SLS process , 2007 .

[34]  Neil Hopkinson,et al.  Investigating mechanical anisotropy and end-of-vector effect in laser-sintered nylon parts , 2006 .

[35]  I. Green,et al.  A Finite Element Study of Elasto-Plastic Hemispherical Contact Against a Rigid Flat , 2005 .

[36]  R. Jackson,et al.  Elasto-plastic hemispherical contact models for various mechanical properties , 2004 .

[37]  L. Kogut,et al.  Elastic-Plastic Contact Analysis of a Sphere and a Rigid Flat , 2002 .

[38]  J. Greenwood,et al.  Contact of nominally flat surfaces , 1966, Proceedings of the Royal Society of London. Series A. Mathematical and Physical Sciences.

[39]  Handbook of Polymers , 2022 .

[40]  R. Jackson,et al.  Statistical models of nearly complete elastic rough surface contact-comparison with numerical solutions , 2017 .

[41]  Lars Pejryd,et al.  Characterisation of carbon fibre-reinforced polyamide manufactured by selective laser sintering , 2016 .

[42]  Paolo Ermanni,et al.  Analysis of Processing Conditions for a Novel 3D-Composite Production Technique , 2015 .